scholarly journals Laser Powder Bed Fusion (PBF-LB/M) Process Strategies for In-Situ Alloy Formation with High-Melting Elements

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 336
Author(s):  
Florian Huber ◽  
Michael Rasch ◽  
Michael Schmidt
Keyword(s):  
Homogeneous Element ◽  
Alloying Elements ◽  
Complete Fusion ◽  
Alloy Formation ◽  
Powder Bed Fusion ◽  
High Melting ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Process Strategy

In-situ alloy formation by Laser Powder Bed Fusion (PBF-LB/M) from mixtures of easily available elemental powders is an appealing approach for developing and qualifying new alloys for laser based additive manufacturing of metals. However, especially when dealing with high-melting elements, like W, Ta, Mo, or Nb, it is difficult to achieve a homogeneous element distribution and a complete fusion of the powder particles. The aim of this work was to understand the effects of the PBF-LB/M process parameters (laser power, scan speed, laser spot diameter) and three different single- and double-exposure strategies on the fusion of high-melting W, Ta, Mo, and Nb particles in a Ti-matrix. For this purpose, 220 samples with 10 vol.% of the high-melting particle fraction were prepared and analyzed by optical light microscopy and automated image processing, as well as by scanning electron microscopy (SEM). The results are discussed in the context of current research on the process dynamics of PBF-LB/M. Based on that process strategies to support a complete fusion of high-melting particles during in-situ alloy formation are derived. It is shown that the number of unmolten particles can be at least decreased by a factor of ten compared to the most unfavorable parameter combination. For the lower melting elements, Nb and Mo, a complete fusion without any remaining particles visible in the microsections was achieved for certain parameter combinations. The results prove the feasibility of in-situ alloy formation with high-melting alloying elements, but they also demonstrate the necessity to adjust the PBF-LB/M process strategy to achieve a complete dissolution of the alloying elements.

scholarly journals In Situ Formation of a Metastable β-Ti Alloy by Laser Powder Bed Fusion (L-PBF) of Vanadium and Iron Modified Ti-6Al-4V

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1067 ◽  
Author(s):  
Florian Huber ◽  
Thomas Papke ◽  
Christian Scheitler ◽  
Lukas Hanrieder ◽  
Marion Merklein ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Homogeneous Element ◽  
Alloy Formation ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Β Phase ◽  
Stabilizing Effect

The aim of this work is to investigate the β-Ti-phase-stabilizing effect of vanadium and iron added to Ti-6Al-4V powder by means of heterogeneous powder mixtures and in situ alloy-formation during laser powder bed fusion (L-PBF). The resulting microstructure was analyzed by metallographic methods, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD). The mechanical properties were characterized by compression tests, both prior to and after heat-treating. Energy dispersive X-ray spectroscopy showed a homogeneous element distribution, proving the feasibility of in situ alloying by LPBF. Due to the β-phase-stabilizing effect of V and Fe added to Ti-6Al-4V, instead of an α’-martensitic microstructure, an α/β-microstructure containing at least 63.8% β-phase develops. Depending on the post L-PBF heat-treatment, either an increased upsetting at failure (33.9%) compared to unmodified Ti-6Al-4V (28.8%), or an exceptional high compressive yield strength (1857 ± 35 MPa compared to 1100 MPa) were measured. The hardness of the in situ alloyed material ranges from 336 ± 7 HV0.5, in as-built condition, to 543 ± 13 HV0.5 after precipitation-hardening. Hence, the range of achievable mechanical properties in dependence of the post-L-PBF heat-treatment can be significantly expanded in comparison to unmodified Ti-6Al-4V, thus providing increased flexibility for additive manufacturing of titanium parts.

scholarly journals In-Situ Alloy Formation of a WMoTaNbV Refractory Metal High Entropy Alloy by Laser Powder Bed Fusion (PBF-LB/M)

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 3095
Author(s):  
Florian Huber ◽  
Dominic Bartels ◽  
Michael Schmidt
Keyword(s):  
Electron Microscopy ◽  
Refractory Metal ◽  
High Entropy Alloy ◽  
Alloy Formation ◽  
High Entropy Alloys ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
High Entropy

High entropy or multi principal element alloys are a promising and relatively young concept for designing alloys. The idea of creating alloys without a single main alloying element opens up a wide space for possible new alloy compositions. High entropy alloys based on refractory metals such as W, Mo, Ta or Nb are of interest for future high temperature applications e.g., in the aerospace or chemical industry. However, producing refractory metal high entropy alloys by conventional metallurgical methods remains challenging. For this reason, the feasibility of laser-based additive manufacturing of the refractory metal high entropy alloy W20Mo20Ta20Nb20V20 by laser powder bed fusion (PBF-LB/M) is investigated in the present work. In-situ alloy formation from mixtures of easily available elemental powders is employed to avoid an expensive atomization of pre-alloyed powder. It is shown that PBF-LB/M of W20Mo20Ta20Nb20V20 is in general possible and that a complete fusion of the powder mixture without a significant number of undissolved particles is achievable by in-situ alloy formation during PBF-LB/M when selecting favorable process parameter combinations. The relative density of the samples with a dimension of 6 × 6 × 6 mm3 reaches, in dependence of the PBF-LB/M parameter set, 99.8%. Electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) measurements confirm the presence of a single bcc-phase. Scanning electron microscopy (SEM) images show a dendritic and/or cellular microstructure that can, to some extent, be controlled by the PBF-LB/M parameters.

On the use of spatter signature for in-situ monitoring of Laser Powder Bed Fusion

2017 ◽  
Vol 16 ◽  
pp. 35-48 ◽  
Author(s):  
Giulia Repossini ◽  
Vittorio Laguzza ◽  
Marco Grasso ◽  
Bianca Maria Colosimo
Keyword(s):  
In Situ Monitoring ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

Titanium Alloys Manufactured by In Situ Alloying During Laser Powder Bed Fusion

JOM ◽  
2017 ◽  
Vol 69 (12) ◽  
pp. 2725-2730 ◽  
Author(s):  
I. Yadroitsev ◽  
P. Krakhmalev ◽  
I. Yadroitsava
Keyword(s):  
Titanium Alloys ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

scholarly journals In Situ Analysis of Laser Powder Bed Fusion Using Simultaneous High-Speed Infrared and X-ray Imaging

JOM ◽  
2020 ◽  
Vol 73 (1) ◽  
pp. 201-211 ◽  
Author(s):  
Benjamin Gould ◽  
Sarah Wolff ◽  
Niranjan Parab ◽  
Cang Zhao ◽  
Maria Cinta Lorenzo-Martin ◽  
...  
Keyword(s):  
High Speed ◽  
In Situ Analysis ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
X Ray ◽  
X Ray Imaging

In-Situ Monitoring of Laser Powder Bed Fusion Process Anomalies via a Comprehensive Analysis of Off-Axis Camera Data

2020 ◽  
Author(s):  
Chaitanya Krishna Prasad Vallabh ◽  
Yubo Xiong ◽  
Xiayun Zhao
Keyword(s):  
Real Time ◽  
Network Architecture ◽  
Video Data ◽  
In Situ Monitoring ◽  
Process Efficiency ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Monitoring Method ◽  
Powder Bed

Abstract In-situ monitoring of a Laser Powder-Bed Fusion (LPBF) additive manufacturing process is crucial in enhancing the process efficiency and ensuring the built part integrity. In this work, we present an in-situ monitoring method using an off-axis camera for monitoring layer-wise process anomalies. The in-situ monitoring is performed with a spatial resolution of 512 × 512 pixels, with each pixel representing 250 × 250 μm and a relatively high data acquisition rate of 500 Hz. An experimental study is conducted by using the developed in-situ off-axis method for monitoring the build process for a standard tensile bar. Real-time video data is acquired for each printed layer. Data analytics methods are developed to identify layer-wise anomalies, observe powder bed characteristics, reconstruct 3D part structure, and track the spatter dynamics. A deep neural network architecture is trained using the acquired layer-wise images and tested by images embedded with artificial anomalies. The real-time video data is also used to perform a preliminary spatter analysis along the laser scan path. The developed methodology is aimed to extract as much information as possible from a single set of camera video data. It will provide the AM community with an efficient and capable process monitoring tool for process control and quality assurance while using LPBF to produce high-standard components in industrial (such as, aerospace and biomedical industries) applications.

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