scholarly journals Microstructure and Hardness Evolution of Solution Annealed Inconel 625/TiC Composite Processed by Laser Powder Bed Fusion

Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 929
Author(s):  
Giulio Marchese ◽  
Alberta Aversa ◽  
Emilio Bassini

This study deals with the Inconel 625 (IN625) alloy reinforced with micro-TiC particles processed by laser powder bed fusion. The microstructure and hardness in the as-built and solution-annealed states were investigated. The microstructures of the as-built IN625 and IN625/TiC states were primarily made up of columnar grains along the building direction. After the solution annealing at 1150 °C for 2 h, the IN625 alloy consisted of equiaxed grains due to recrystallization and grain growth. On the contrary, the solution-annealed IN625/TiC composite still presented columnar grains. Therefore, the TiC particles hinder the recrystallization, indicating higher microstructure stability for the composite. For the IN625/TiC composite, both the reduced alteration of the grains and the more intensive formation of carbides prevent a remarkable hardness reduction in the solution-annealed state.

Materialia ◽  
2021 ◽  
pp. 101243
Author(s):  
Leonardo Shoji Aota ◽  
Priyanshu Bajaj ◽  
Kahl Dick Zilnyk ◽  
Dirk Ponge ◽  
Hugo Ricardo Zschommler Sandim

2020 ◽  
Vol 769 ◽  
pp. 138500 ◽  
Author(s):  
Giulio Marchese ◽  
Simone Parizia ◽  
Masoud Rashidi ◽  
Abdollah Saboori ◽  
Diego Manfredi ◽  
...  

Author(s):  
Felix Schmeiser ◽  
Erwin Krohmer ◽  
Christian Wagner ◽  
Norbert Schell ◽  
Eckart Uhlmann ◽  
...  

AbstractLaser powder bed fusion is an additive manufacturing process that employs highly focused laser radiation for selective melting of a metal powder bed. This process entails a complex heat flow and thermal management that results in characteristic, often highly textured microstructures, which lead to mechanical anisotropy. In this study, high-energy X-ray diffraction experiments were carried out to illuminate the formation and evolution of microstructural features during LPBF. The nickel-base alloy Inconel 625 was used for in situ experiments using a custom LPBF system designed for these investigations. The diffraction patterns yielded results regarding texture, lattice defects, recrystallization, and chemical segregation. A combination of high laser power and scanning speed results in a strong preferred crystallographic orientation, while low laser power and scanning speed showed no clear texture. The observation of a constant gauge volume revealed solid-state texture changes without remelting. They were related to in situ recrystallization processes caused by the repeated laser scanning. After recrystallization, the formation and growth of segregations were deduced from an increasing diffraction peak asymmetry and confirmed by ex situ scanning transmission electron microscopy. Graphical Abstract


Author(s):  
Zhida Huang ◽  
Zongyue Fan ◽  
Hao Wang ◽  
Bo Li

Laser Powder Bed Fusion (LPBF) is an additive manufacturing method that manufactures high density and quality metal products. We present a coupled grain growth and heat transfer modeling technique to understand the materials microstructure evolution in metals during the cooling process of LPBF. The phase-field model is combined with a transient heat transfer equation to simulate the solidification and crystallization of the melt pool simultaneously. Specifically, the variable domain and driving force of the order parameters in the phase-field calculation are defined using current temperature distribution. Additionally, the latent heat generated by crystallization is introduced as a heat source to affect temperature evolution in the cooling process. The finite element method with a staggering strategy is employed to solve the coupled governing equations on an irregular computational domain. The computational framework is verified in a one-dimensional solidification problem by comparing the velocity of the fluid-solid interface. The two-way coupling solution of solidification and crystallization is studied in an example of LPBF of Aluminum alloys.


2017 ◽  
Vol 48 (11) ◽  
pp. 5547-5558 ◽  
Author(s):  
Eric A. Lass ◽  
Mark R. Stoudt ◽  
Maureen E. Williams ◽  
Michael B. Katz ◽  
Lyle E. Levine ◽  
...  

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