scholarly journals Optimization and Scale-Up for Polymer Extrusion

Polymers ◽  
2021 ◽  
Vol 13 (10) ◽  
pp. 1547
Author(s):  
Andrzej Nastaj ◽  
Krzysztof Wilczyński

A review paper is presented on optimization and scale-up for polymer extrusion, both single screw and twin screw extrusion. Optimization consists in obtaining a multidimensional space of process output variables (response surface) on the basis of an appropriate set of input data and searching for extreme values in this space. Scaling consists in changing the scale of the process according to specific criteria, that is, changing the process while maintaining the scaling parameters at a level that is as close to the reference process parameters as possible. It consists in minimizing the differences between the parameters characterizing the reference process and the resulting process. This may be obtained by using optimization techniques leading to the minimization of discrepancies between the parameters of scaled processes. In the paper, it was stated that optimization and scale-up based on process simulation are more effective than those based on experimentation which is time consuming and expensive. The state-of-the-art on extrusion process modeling which is the basis of optimization and scale-up has been presented. Various optimization techniques have been discussed, and the Genetic Algorithms have been identified as powerful and very efficient. Optimization and scale-up based on the process simulation using Genetic Algorithms have been broadly reviewed and discussed. It was concluded that, up to date, there is a lack of optimization studies on the counter-rotating twin screw extrusion, although the global models of this process are known. There is also a lack of process simulation-based scaling-up studies, both on the counter-rotating twin screw extrusion and on the starve fed single screw extrusion. Finally, development perspectives in this field have been discussed.

2014 ◽  
Vol 170 ◽  
pp. 235-249 ◽  
Author(s):  
Dominick Daurio ◽  
Karthik Nagapudi ◽  
Lan Li ◽  
Peter Quan ◽  
Fernando-Alvarez Nunez

The application of twin screw extrusion (TSE) in the scale-up of cocrystal production was investigated by using AMG 517–sorbic acid as a model system. Extrusion parameters that influenced conversion to the cocrystal such as temperature, feed rate and screw speed were investigated. Extent of conversion to the cocrystal was found to have a strong dependence on temperature and a moderate dependence on feed rate and screw speed. Cocrystals made by the TSE process were found to have superior mechanical properties than solution grown cocrystals. Additionally, moving to a TSE process eliminated the need for solvent.


Polymers ◽  
2022 ◽  
Vol 14 (2) ◽  
pp. 240
Author(s):  
Andrzej Nastaj ◽  
Krzysztof Wilczyński

A novel scaling-up computer system for single screw extrusion of polymers has been developed. This system makes it possible to scale-up extrusion process with both starve feeding and flood feeding. Each of the scale-up criteria can be an objective function to be minimized, represented by single values or functional dependencies over the screw length. The basis of scaling-up is process simulation made with the use of the GSEM program (Global Screw Extrusion Model). Scaling-up is performed using the GASES program (Genetic Algorithms Screw Extrusion Scaling) based on Genetic Algorithms. Scaling-up the extrusion process has been performed to increase extrusion output according to the scaling-up criteria defined by the single parameters of unit energy consumption, polymer plasticating rate and polymer temperature, as well as by the process parameters profiles of the temperature and plasticating. The global objective function reached the lowest value for the selected process parameters, and extrusion throughput was significantly increased.


Polymers ◽  
2021 ◽  
Vol 13 (13) ◽  
pp. 2128
Author(s):  
Paulo F. Teixeira ◽  
José A. Covas ◽  
Loïc Hilliou

The dispersion mechanisms in a clay-based polymer nanocomposite (CPNC) during twin-screw extrusion are studied by in-situ rheo-optical techniques, which relate the CPNC morphology with its viscosity. This methodology avoids the problems associated with post extrusion structural rearrangement. The polydimethylsiloxane (PDMS) matrix, which can be processed at ambient and low temperatures, is used to bypass any issues associated with thermal degradation. Local heating in the first part of the extruder allows testing of the usefulness of low matrix viscosity to enhance polymer intercalation before applying larger stresses for clay dispersion. The comparison of clay particle sizes measured in line with models for the kinetics of particle dispersion indicates that larger screw speeds promote the break-up of clay particles, whereas smaller screw speeds favor the erosion of the clay tactoids. Thus, different levels of clay dispersion are generated, which do not simply relate to a progressively better PDMS intercalation and higher clay exfoliation as screw speed is increased. Reducing the PDMS viscosity in the first mixing zone of the screw facilitates dispersion at lower screw speeds, but a complex interplay between stresses and residence times at larger screw speeds is observed. More importantly, the results underline that the use of larger stresses is inefficient per se in dispersing clay if sufficient time is not given for PDMS to intercalate the clay galleries and thus facilitate tactoid disruption or erosion.


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