scholarly journals Future-Oriented Experimental Characterization of 3D Printed and Conventional Elastomers Based on Their Swelling Behavior

Polymers ◽  
2021 ◽  
Vol 13 (24) ◽  
pp. 4402
Author(s):  
Klara Loos ◽  
Vivianne Marie Bruère ◽  
Benedikt Demmel ◽  
Yvonne Ilmberger ◽  
Alexander Lion ◽  
...  
Keyword(s):  
Tensile Tests ◽  
Swelling Behavior ◽  
Uniaxial Tensile ◽  
Stress And Strain ◽  
Experimental Characterization ◽  
Synthetic Fuels ◽  
Fuel Component ◽  
3D Printed ◽  
Fuel Components

The present study investigates different elastomers with regard to their behavior towards liquids such as moisture, fuels, or fuel components. First, four additively manufactured materials are examined in detail with respect to their swelling in the fuel component toluene as well as in water. The chemical nature of the materials is elucidated by means of infrared spectroscopy. The experimentally derived absorption curves of the materials in the liquids are described mathematically using Fick’s diffusion law. The mechanical behavior is determined by uniaxial tensile tests, which are evaluated on the basis of stress and strain at break. The results of the study allow for deriving valuable recommendations regarding the printing process and postprocessing. Second, this article investigates the swelling behavior of new as well as thermo-oxidatively aged elastomers in synthetic fuels. For this purpose, an analysis routine is presented using sorption experiments combined with gas chromatography and mass spectrometry and is thus capable of analyzing the swelling behavior multifacetted. The transition of elastomer constituents into the surrounding fuel at different aging and sorption times is determined precisely. The change in mechanical properties is quantified using density measurements, micro Shore A hardness measurements, and the parameters stress and strain at break from uniaxial tensile tests.

Inverse Mechanical Characterization of Tissue Engineered Heart Valves

2008 ◽  
Author(s):  
Martijn A. J. Cox ◽  
Jeroen Kortsmit ◽  
Niels J. B. Driessen ◽  
Carlijn V. C. Bouten ◽  
Frank P. T. Baaijens
Keyword(s):  
Heart Valves ◽  
Soft Tissues ◽  
Mechanical Characterization ◽  
Tensile Tests ◽  
Material Behavior ◽  
Uniaxial Tensile ◽  
Mechanical Conditioning ◽  
Indentation Tests ◽  
Tissue Engineered Heart Valves

Over the last few years, research interest in tissue engineering as an alternative for current treatment and replacement strategies for cardiovascular and heart valve diseases has significantly increased. In vitro mechanical conditioning is an essential tool for engineering strong implantable tissues [1]. Detailed knowledge of the mechanical properties of the native tissue as well as the properties of the developing engineered constructs is vital for a better understanding and control of the mechanical conditioning process. The nonlinear and anisotropic behavior of soft tissues puts high demands on their mechanical characterization. Current standards in mechanical testing of soft tissues include (multiaxial) tensile testing and indentation tests. Uniaxial tensile tests do not provide sufficient information for characterizing the full anisotropic material behavior, while biaxial tensile tests are difficult to perform, and boundary effects limit the test region to a small central portion of the tissue. In addition, characterization of the local tissue properties from a tensile test is non-trivial. Indentation tests may be used to overcome some of these limitations. Indentation tests are easy to perform and when indenter size is small relative to the tissue dimensions, local characterization is possible. We have demonstrated that by recording deformation gradients and indentation force during a spherical indentation test the anisotropic mechanical behavior of engineered cardiovascular constructs can be characterized [2]. In the current study this combined numerical-experimental approach is used on Tissue Engineered Heart Valves (TEHV).

Methods for the Experimental Evaluation of True Stress-Strain Curves After Necking of Conventional Tensile Specimens: Exploratory Investigation and Proposals

2012 ◽  
Author(s):  
Grace Kelly Q. Ganharul ◽  
Nick de Brangança Azevedo ◽  
Gustavo Henrique B. Donato
Keyword(s):  
Real Time ◽  
Weighted Average ◽  
Tensile Tests ◽  
Plastic Instability ◽  
True Stress ◽  
Experimental Results ◽  
Uniaxial Tensile ◽  
High Definition ◽  
Stress Strain

Numerical elastic-plastic simulations have undergone significant expansion during the last decades (e.g. refined fracture mechanics finite element models including ductile tearing). However, one limitation to increase the accuracy of such models is the reliable experimental characterization of true stress-strain curves from conventional uniaxial tensile tests after necking (plastic instability), which complicates the direct assessment of the true stress-strain curves until failure. As a step in this direction, this work presents four key activities: i) first, existing correction methods are presented, including Bridgman, power law, weighted average and others; ii) second, selected metals are tested to experimentally characterize loads and the geometric evolution of necking. High-definition images are used to obtain real-time measurements following a proposed methodology; iii) third, refined non-linear FEM models are developed to reproduce necking and assess stresses as a function of normalized neck geometry; iv) finally, existing correction methods are critically compared to experimental results and FEM predictions in terms of potential and accuracy. The experimental results evaluated using high-definition images presented an excellent geometrical characterization of instability. FEM models were able to describe stress-strain-displacement fields after necking, supporting the exploratory validations and proposals of this work. Classical methodologies could be adapted based on experiments to provide accurate stress-strain curves up to failure with less need for real-time measurements, thus giving further support to the determination of true material properties considering severe plasticity.

scholarly journals Design, Manufacture and Experimental Characterization of Magnetorheological Rotary Brake Based on an Peristaltic Pump System

2021 ◽  
Author(s):  
Tomasz Korona ◽  
Pawel Kowol ◽  
GRAZIA LO SCIUTO
Keyword(s):  
Magnetic Field ◽  
Experimental Tests ◽  
Stress And Strain ◽  
Peristaltic Pump ◽  
Experimental Characterization ◽  
Compression Force ◽  
Pump System ◽  
Concept Model ◽  
Design And Manufacture

Abstract In this article the design and manufacture of the innovative MR rotary brake based on peristaltic pump inspired by the concept model of the pliers and the Rochester Pean forceps are presented . For the calculation and analysis of created structure comprehensive of roller, housing and pliers, simulations concerning the stress and strain are conducted to investigate the deformation and possible failure of part or assembly. Experimental tests including measurements of compression force and magnetic field were conducted to evaluate the performance of proposed designed MR rotary brake based on peristaltic pump system constituted by tube containing MR fluid and pliers with arm responsible of the movement and arm completely hold on bench vise

scholarly journals Development, Fabrication, and Characterization of Composite Polycaprolactone Membranes Reinforced with TiO2 Nanoparticles

Polymers ◽  
2019 ◽  
Vol 11 (12) ◽  
pp. 1955 ◽  
Author(s):  
Karina del Ángel-Sánchez ◽  
César I. Borbolla-Torres ◽  
Luis M. Palacios-Pineda ◽  
Nicolás A. Ulloa-Castillo ◽  
Alex Elías-Zúñiga
Keyword(s):  
Acetic Acid ◽  
Titanium Dioxide Nanoparticles ◽  
Sol Gel ◽  
Tensile Tests ◽  
Experimental Characterization ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
The One

This paper focuses on developing, fabricating, and characterizing composite polycaprolactone (PCL) membranes reinforced with titanium dioxide nanoparticles (NPs) elaborated by using two solvents; acetic acid and a mixture of chloroform and N,N-dimethylformamide (DMF). The resulting physical, chemical, and mechanical properties of the composite materials are studied by using experimental characterization techniques such as scanning electron microscopy (SEM), differential scanning calorimetry (DSC), X-ray diffraction (XRD), Fourier-transform infrared (FTIR) analysis, contact angle (CA), uniaxial and biaxial tensile tests, and surface roughness measurements. Experimental results show that the composite material synthesized by sol-gel and chloroform-DMF has a better performance than the one obtained by using acetic acid as a solvent.

scholarly journals Optimization of Manufacturing Parameters and Tensile Specimen Geometry for Fused Deposition Modeling (FDM) 3D-Printed PETG

Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2556
Author(s):  
Arda Özen ◽  
Dietmar Auhl ◽  
Christina Völlmecke ◽  
Josef Kiendl ◽  
Bilen Emek Abali
Keyword(s):  
Mechanical Properties ◽  
Fused Deposition Modeling ◽  
Tensile Tests ◽  
Tensile Specimen ◽  
Careful Examination ◽  
Uniaxial Tensile ◽  
Fused Deposition ◽  
Design Flexibility ◽  
Deposition Modeling ◽  
3D Printed

Additive manufacturing provides high design flexibility, but its use is restricted by limited mechanical properties compared to conventional production methods. As technology is still emerging, several approaches exist in the literature for quantifying and improving mechanical properties. In this study, we investigate characterizing materials’ response of additive manufactured structures, specifically by fused deposition modeling (FDM). A comparative analysis is achieved for four different tensile test specimens for polymers based on ASTM D3039 and ISO 527-2 standards. Comparison of specimen geometries is studied with the aid of computations based on the Finite Element Method (FEM). Uniaxial tensile tests are carried out, after a careful examination of different slicing approaches for 3D printing. We emphasize the effects of the chosen slicer parameters on the position of failures in the specimens and propose a simple formalism for measuring effective mechanical properties of 3D-printed structures.

scholarly journals Experimental Study of Single-Lap, Hybrid Joints, Made of 3D Printed Polymer and Aluminium Adherends

Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7705
Author(s):  
Przemysław Golewski ◽  
Marek Nowicki ◽  
Tomasz Sadowski ◽  
Daniel Pietras
Keyword(s):  
Experimental Study ◽  
Tensile Tests ◽  
Lap Joints ◽  
Uniaxial Tensile ◽  
Adhesive Tape ◽  
Hybrid Joint ◽  
Multi Stage ◽  
3D Printed ◽  
Reference Specimens ◽  
Different Diameters

This paper presents the results of an experimental study into single-lap joints. One part of the joint was made as a 3D printed polymer and had cylindrical tenons, while the other part was made of an aluminium flat bar having mortises whose diameter and distribution corresponded to the polymer tenons. In addition to the mechanical joint, a layer of double-sided VHB (Very High Bond) adhesive tape was also placed in the lap, thus creating a hybrid joint. In total, 80 specimens were made, which were divided into four groups: A—specimens with one tenon of different diameters, B—specimens with different number of tenons of the same diameter, C—specimens characterised by multi-stage operation and R—reference specimens, connected only by double-sided adhesive tape. The joints were subjected to uniaxial tensile tests. The force–displacement characteristics obtained and the energy required, up to the point of the failure of the joints, have been analysed in this paper. The four and six-stage joints designed can significantly increase the safety of the structures in which they will be used.

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