scholarly journals Corrosion rate of Al-Si Alloy Reinforced with B4C Nanoparticle prepared by Powder Metallurgy Method using RSM

The current work aims to optimize the Al-Si alloy reinforced with B4C nanoparticles prepared through powder metallurgy technique. The sample was prepared with different weight percentage 0, 4 and 8; the size of the sample was 20 mm x 20mm and sintered in a furnace upto 500oC with argon gas and their by furnace cooled to room temperature. The samples were brushed to remove the slag present in it, and polished by emery paper. Then the samples were weighed in an electric balancing apparatus to measure the initial weight of the sample before dipping it into acid solution. The weight loss was measured to calibrate the corrosion rate of the samples for 9 days. Response surface methodology was designed for three factors at three levels with a response as corrosion rate. The Analysis of Variance (ANOVA) was used to identify the most influencing factor on corrosion rate. The normal probability plot, residual plot, and desirability plot demonstrates the influence of corrosion rate of the composites.

2017 ◽  
Vol 13 (10) ◽  
pp. 5905-5913
Author(s):  
S. Saravanan ◽  
P.Senthil Kumar ◽  
T. Palanisamy ◽  
M. Ravichandran ◽  
V. Anandakrishnan ◽  
...  

AA6063-TiC composites have several weight percentages up to 9 wt. % were fabricated by using stir casting route method. The effects of the weight percentage of TiC particles on the microstructures and corrosion behavior of AA6063-TiC composites were studied. The results revealed that the AA6063-TiC composites exhibited higher density than the AA6063 matrix. The accelerated corrosion tests of AA6063-TiC composites in 3.5 wt. % NaCl aqueous solution at room temperature, the AA6063-TiC composites have better corrosion resistance than the AA6063 matrix. Increasing the weight percentage of the TiC particles to reduces the corrosion rate of the AA6063-TiC composites. In this process corrosion rate of 0.4402 mm/year for AA6063 matrix, 0.3891 mm/year for 3 wt. % , 0.3568 mm/year for 6 wt. % and 0.3062 mm/year for 9 wt. % of TiC particles respectively. The poor corrosion resistance of the composites can be attributed to the galvanic effects between the AA6063 matrix and TiC reinforcement.


This research paper discuss about the wear loss behavior of Al-12Si-xB4C composites prepared through powder metallurgy method by varying the weight percentage of reinforcement (x = 2, 4, 6, 8, and 10) content. The samples were prepared by using die and punch assembly and the lubricant used to eject the sample from the die was molybdenum disulfide. The compaction was done by using compression testing machine by applying a pressure of 800MPa. The dry sliding wear loss behavior of the sample was conducted on Pin-on-Disc machine and the experimental values of wear loss were calibrated. Taguchi design experiment was done by applying L25 orthogonal array for 3 factors at 5 levels for the response parameter wear loss. Analysis of Variance demonstrated by Mean and S/N ratio table for wear loss was discussed and from the table it can be seen that the reinforcement plays a main role, when the compared with load and Sliding Distance (SD). The normal probability plot shows that the residuals falls near to the red line, it indicate that the error values were less in the model


2021 ◽  
Vol 900 ◽  
pp. 51-60
Author(s):  
Zainab Hassan ◽  
Mudhar Al-Obaidi

There has been a significant increase in the use of composite materials to reinforce metallic structures. Such an increase has been especially noted in marine and underground applications, where there is a higher corrosion impact. Whilst there have been several attempts to investigate the mechanical properties of several synthesized composite materials, few of these have analyzed the corrosion of such composite materials at different weight ratios. The aim of this paper is to explore the best weight ratios of a graphite/Zinc composite matrix that would yield the lowest corrosion rate for a variety of applications. The research is validated using experimentation based on six additives of graphite (1wt%, 2.5wt%, 4wt%, 6wt%, 8wt%, and 10wt%), which are used as reinforcements for a range of weight ratios. The additives were prepared using the powder metallurgy method. The corrosion rate for all specimens used was carried out at the room temperature of 27 °C. Analysis results showed that 1wt% of graphite additive has the highest corrosion resistance compared to other weight ratios tested. This has been verified by examining the microstructure of the composite using an optical microscope for 12h, 24h, and 48h of immersion time in a 1M HCl acid solution.


2011 ◽  
Vol 471-472 ◽  
pp. 420-425 ◽  
Author(s):  
Mohammad Moazami-Goudarzi ◽  
Farshad Akhlaghi

In the present study the effect of Mg addition on the characteristics of Al/SiC nanocomposite powder particles produced via a relatively new method called in situ powder metallurgy (IPM) is investigated. Commercially pure Al and Al-Mg alloy melts containing different amounts of Mg were used as the matrix alloy. Nano-sized SiC particles with the average size of 60 nm were used as the reinforcing material. The effect of Mg content on the fluidity of the melt as an influencing factor affecting both the process yield and wettability of SiC with molten metal was investigated. The size distribution of produced powders was characterized using a laser particle size analyzer. Scanning electron microscopy was utilized to investigate the possibility of embedding of SiC nanoparticles within the metallic matrix. Results of microhardness measurements together with SEM micrographs and EDS analysis showed that nano-sized SiC particles could be embedded in the relatively coarse Al-Mg powders containing at least 1 wt.% Mg.


2012 ◽  
Vol 626 ◽  
pp. 738-742
Author(s):  
M. Marina ◽  
K. Alir ◽  
W. Rahman ◽  
Z. Nooraizedfiza ◽  
Mohd Asri Selamat ◽  
...  

This study is focused on fabricating and characterizing iron (Fe) composites prepared by powder metallurgy route reinforced with varying weight of Yttria (Y2O3). Composites were prepared based on 5 wt. % to 15 wt. % of reinforcement powder with particle size ranging from 1-10µm. Pure Fe matrix composites were also prepared for comparison purpose. This paper will report the microstructure, bulk density and micro hardness values of the composites. Powder characterization and microstructures of the composites were examined using Scanning Electron Microscope (SEM) which indicated homogenous distribution of reinforcement particles in the metal matrix. Bulk density of the composites was calculated using standard Archimedean method showing decreasing values as the weight percentage of Y2O3 increases. Micro-hardness was measured using micro-Vickers hardness instrument. The data obtained shows that the Fe-Y2O3 composites samples possessed superior hardness value with the increasing quantity of reinforcement compared to the unreinforced Fe composite.


Materials ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 4090
Author(s):  
Negin Ashrafi ◽  
M. A. Azmah Hanim ◽  
Masoud Sarraf ◽  
S. Sulaiman ◽  
Tang Sai Hong

Hybrid reinforcement’s novel composite (Al-Fe3O4-SiC) via powder metallurgy method was successfully fabricated. In this study, the aim was to define the influence of SiC-Fe3O4 nanoparticles on microstructure, mechanical, tribology, and corrosion properties of the composite. Various researchers confirmed that aluminum matrix composite (AMC) is an excellent multifunctional lightweight material with remarkable properties. However, to improve the wear resistance in high-performance tribological application, hardening and developing corrosion resistance was needed; thus, an optimized hybrid reinforcement of particulates (SiC-Fe3O4) into an aluminum matrix was explored. Based on obtained results, the density and hardness were 2.69 g/cm3, 91 HV for Al-30Fe3O4-20SiC, after the sintering process. Coefficient of friction (COF) was decreased after adding Fe3O4 and SiC hybrid composite in tribology behaviors, and the lowest COF was 0.412 for Al-30Fe3O4-20SiC. The corrosion protection efficiency increased from 88.07%, 90.91%, and 99.83% for Al-30Fe3O4, Al-15Fe3O4-30SiC, and Al-30Fe3O4-20SiC samples, respectively. Hence, the addition of this reinforcement (Al-Fe3O4-SiC) to the composite shows a positive outcome toward corrosion resistance (lower corrosion rate), in order to increase the durability and life span of material during operation. The accomplished results indicated that, by increasing the weight percentage of SiC-Fe3O4, it had improved the mechanical properties, tribology, and corrosion resistance in aluminum matrix. After comparing all samples, we then selected Al-30Fe3O4-20SiC as an optimized composite.


Author(s):  
J. Alias

Much research on magnesium (Mg) emphasises creating good corrosion resistance of magnesium, due to its high reactivity in most environments. In this study, powder metallurgy (PM) technique is used to produce Mg samples with a variation of aluminium (Al) composition. The effect of aluminium composition on the microstructure development, including the phase analysis was characterised by optical microscope (OM), scanning electron microscopy (SEM) and x-ray diffraction (XRD). The mechanical property of Mg sample was performed through Vickers microhardness. The results showed that the addition of aluminium in the synthesised Mg sample formed distribution of Al-rich phases of Mg17Al12, with 50 wt.% of aluminium content in the Mg sample exhibited larger fraction and distribution of Al-rich phases as compared to the 20 wt.% and 10 wt.% of aluminium content. The microhardness values were also increased at 20 wt.% and 50 wt.% of aluminium content, comparable to the standard microhardness value of the annealed Mg. A similar trend in corrosion resistance of the Mg immersed in 3.5 wt.% NaCl solution was observed. The corrosion behaviour was evaluated based on potentiodynamic polarisation behaviour. The corrosion current density, icorr, is observed to decrease with the increase of Al composition in the Mg sample, corresponding to the increase in corrosion resistance due to the formation of aluminium oxide layer on the Al-rich surface that acted as the corrosion barrier. Overall, the inclusion of aluminium in this study demonstrates the promising development of high corrosion resistant Mg alloys.


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