Application of Coercive Field Measurements to the Evaluation of Recovery and Recrystallization in Cold Rolled Interstitial Free (IF) Steel

Author(s):  
Ane Martínez-de-Guereñu ◽  
M. Oyarzabal ◽  
F. Arizti ◽  
Isabel Gutiérrez
2005 ◽  
Vol 500-501 ◽  
pp. 647-654 ◽  
Author(s):  
Ane Martínez-de-Guereñu ◽  
M. Oyarzabal ◽  
F. Arizti ◽  
Isabel Gutiérrez

The recovery and recrystallization kinetics of a cold rolled interstitial free (IF) steel were studied during isothermal annealing. Magnetic methods based on coercive field measurements, hardness tests and metallography were applied so as to follow the kinetics experimentally. The coercive field measurement technique reveals a higher degree of resolution for monitoring recovery than conventional hardness determination and also allows the recrystallization progress to be monitored. The results obtained are compared to those previously determined for a non-stabilized extra low carbon (ELC) steel. The observed differences are discussed in terms of the presence of microalloying elements, Ti and Nb, which slow down recovery and delay recrystallization.


2014 ◽  
Vol 783-786 ◽  
pp. 1954-1960
Author(s):  
Toshiharu Morimoto ◽  
Y. Fuyuki ◽  
A. Yanagida ◽  
Jun Yanagimoto

T.M.C.P.(Thermo Mechanical Control Processing) has been widely used to improveplastic formability in steel strips. We have produced interstitial free steel(IF steel) strips and ferriticstainless-steel strips through T.M.C.P. rolling method. Optimizing conditions of hot rolling, hotrolled annealing, cold rolling and cold rolled annealing, we developed texture prediction model. Wecan predict rolling texture accurately using the conventional Taylor model. Moreover, we preciselypredict recrystallization texture classifying the total number of microscopic􀀁 slips which arecalculated using the Taylor model. We consider that these calculated results provednucleation-oriented model and two types of recrystallization and grain growth mechanisms exit inour studies. One mechanism is that grains which had the small total number of microscopic slips arepreferred orientation for the hot rolled and annealed ferritic stainless-steel strip. The othermechanism is that grains which had the high total number of microscopic slips are preferredorientation for the cold rolled and annealed IF steel strip.


2015 ◽  
Vol 651-653 ◽  
pp. 83-88 ◽  
Author(s):  
Satoshi Shirakami ◽  
Shigeru Yonemura ◽  
Tohru Yoshida ◽  
Noriyuki Suzuki ◽  
Toshihiko Kuwabara

In-plane tension/compression tests of a cold rolled interstitial-free (IF) steel and sheet a 980MPa dual phase high strength steel sheet (980DP) were carried out to investigate the work-hardening behavior under two-stage loading paths. The two-stage loading paths consist of the uniaxial tension/compression for the rolling direction (RD) followed by unloading and subsequent uniaxial tension/compression in the 0°, 45° and 90° directions from the first loading direction (0°-, 45°- and 90°-loading). The work hardening behavior in the second loading was different between the 980DP and the IF steel. It was found that the work hardening behaviors were significantly affected by the inner product of the strain rate mode tensors for the first and second loading and that the effect of the deformation mode (tension/compression) was small.


2010 ◽  
Vol 638-642 ◽  
pp. 2781-2786
Author(s):  
Chang Shu He ◽  
Sadahiro Tsurekawa ◽  
Hiroyuki Kokawa ◽  
Xiang Zhao ◽  
Liang Zuo

An AC magnetic field (0.5Tesla) is applied with the field direction perpendicular to the rolling direction during annealing of a 76% cold-rolled IF steel sheet. Microstructure and texture evolution in the as-annealed specimens were determined using SEM based OIM technique. It is found that the recrystallization is noticeably retarded by AC magnetic field annealing. At the early stage of recrystallization (annealing at 650°C for 30min), the development of (111) <123> orientations was favored by the AC magnetic field. With progress of recrystallization (annealing at 700°C and 750°C for 30min), the applied AC magnetic field suppressed the development of γ-fiber recrystallization textures to some extent.


2005 ◽  
Vol 495-497 ◽  
pp. 411-416
Author(s):  
Y.X. Cai ◽  
Y.D. Liu ◽  
Yi Nong Wang ◽  
Gang Wang ◽  
Yan Dong Wang ◽  
...  

The aim of this work is to investigate the relationship between the deformation microstructure and texture in cold rolled Interstitial Free (IF) steel sheets. In the present research, the cold rolled IF steel sheets with 10%-50% reductions are used to observe the characteristic microstructure and individual orientations by transmission electron microscopy (TEM) and SAED patterns. The experimental results on inter-granular strain homogeneity and dislocation wall formation are given in details in this paper. The results are explained by the analysis of crystallographic gliding and are helpful to improve the prediction of cold rolling textures.


2013 ◽  
Vol 753 ◽  
pp. 207-212 ◽  
Author(s):  
Xin Li Song ◽  
Kun Peng ◽  
Ze Xi Yuan ◽  
W.W. Zhu ◽  
J. Jia ◽  
...  

The effect of micro-alloying elements of niobium and boron and titanium on recrystallization behavior is researched after the cold rolled IF steels are annealed at high temperature. The results show that there is high density dislocation in the cold rolled steel and the microstructure is fibrous tissue. The recrystallization grains appear when the cold steel annealed at 655 °C and then the grains grow up with the annealing temperature increased to 840 °C. The recrystallization temperature and time of B-Ti-IF steel is lower than that of Nb-Ti-IF and Ti-IF steels. The recrystallization activation energy of Nb-Ti-IF steel is 181.7KJ/mol which is 56.6KJ/mol larger than that of B-Ti-IF steel.


2005 ◽  
Vol 495-497 ◽  
pp. 417-422
Author(s):  
T. He ◽  
Y.D. Liu ◽  
Yan Wu ◽  
Q.W. Jiang ◽  
Gang Wang ◽  
...  

An experimental setup was designed to study the recrystallization kinetics of Interstitial Free (IF) steel in this work. The 80% cold rolled IF steel foils are heated rapidly to 680°C, 730°C and 780°C by a salt bath. The recrystallization kinetic curves were obtained by the quantitative analysis of texture components, microstructures and EBSP (electron back-scattering patterns) measurements. With the help of EBSD, the orientations of the recrystallization nuclei are determined. The growth rule of the recrystallization nuclei was analyzed statistically. The effect of nucleus orientation on the formation of the recrystallization texture was investigated.


2008 ◽  
Vol 575-578 ◽  
pp. 972-977
Author(s):  
He Tong ◽  
Yan Dong Liu ◽  
Q.W. Jiang ◽  
Y. Ren ◽  
G. Wang ◽  
...  

High-energy synchrotron diffraction offers great potential for experimental study of recrystallization kinetics. A fine experimental design to study the recrystallization mechanism of Interstitial Free (IF) steel was implemented in this work. In-situ annealing process of cold-rolled IF steel with 80% reduction was observed using high-energy X-ray diffraction. Results show that, the diffraction intensity of {001}<110> and {112}<110> belong to α-fiber texture component decreased with the annealing temperature increased while {111}<110> did nearly not change and {111}<112> increased; the FMTH decreasing and d-space changing with annealing temperature increasing indicated that the residual stress relaxed completely during recovery.


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