Structure and Magnetostriction of PrxTb1-xFe1.9Ti0.1 Alloys

2013 ◽  
Vol 281 ◽  
pp. 413-416
Author(s):  
He Yan Liu ◽  
Guo Dong Liu ◽  
Ying Li ◽  
Hong Zhi Luo ◽  
Shao Ling Zhang ◽  
...  

The structure and magnetostriction have been investigated for PrxTb1-xFe1.9Ti0.1 alloys by means of the X-ray diffraction phase analysis, vibrating sample magnetometer, and standard strain gauge technique. Comparing the structure of bulk and annealed samples, it can be found that the annealing treatment is of benefit to the formation of single phase with MgCu2-type crystal structure when x0.3. The magnetization at the maximal magnetic field decreases rapidly with increasing Pr content. The magnetostriction for Pr0.2Tb0.8Fe1.9Ti0.1 annealed sample at 900kA/m is 1733ppm. The magnetostriction for PrxTb1-xFe1.9Ti0.1 alloys at 900kA/m also decreases with increasing Pr content.

2009 ◽  
Vol 152-153 ◽  
pp. 7-10 ◽  
Author(s):  
Irina S. Tereshina ◽  
S.A. Nikitin ◽  
G.A. Politova ◽  
A.S. Ilyushin ◽  
A.A. Opolenko ◽  
...  

In this work, the structural and magnetic properties of single-phase TbxDyyHoz(Fe,Co)2 (x + y + z = 1) alloys have been investigated by means of X-ray diffraction, 57Fe Mossbauer spectroscopy, magnetization measurements and a standard strain gage technique. The magnetostriction of TbxDyyHoz(Fe,Co)2 was examined against an applied magnetic field up to 10 kOe in 80 - 400 K temperature range. The Co-containing compounds are found to have high values of magnetostrictive susceptibility due to compensation of magnetic anisotropy in both the rare-earth and 3d transition metals sublattices.


2012 ◽  
Vol 476-478 ◽  
pp. 1370-1373
Author(s):  
X Liu ◽  
J.J Liu ◽  
R.R Lin ◽  
H.Y Yin ◽  
X.C Liu ◽  
...  

The magnetostrictive Pr(Fe0.4Co0.6)1.93alloy with MgCu2-type structure, and its 0-3 and pseudo 1-3 type epoxy-bonded composites were fabricated by curing without and with a magnetic field. The structural, magnetic and magnetoelastic properties were investigated by means of x-ray diffraction, a vibrating sample magnetometer and a standard strain technique. The 0-3 type composite has a larger magnetostriction than the 1-3 composite has, which can be ascribed to the easy magnetization direction (EMD) not lying along direction.


2021 ◽  
Vol 66 (1) ◽  
pp. 57-64
Author(s):  
Hang Pham Vu Bich ◽  
Yen Nguyen Hai ◽  
Mai Phung Thi Thanh ◽  
Dung Dang Duc ◽  
Hung Nguyen Manh ◽  
...  

In this study, we present the process of synthesis FexNi1-xMn2O4 (x = 0; 0.1; 0.3; 0.5; 0.7; 0.9; 1) by method sol-gel. Scanning electron microscope results shows that the particle size is about 50 nm. The X-ray diffraction diagram shows that the samples are single phase, changing structure clearly as the x ratio increases from 0 to 1. The lattice constant, the bond length also changes with x-value as shown on the Raman scattering spectrum. The results of the vibrating sample magnetometer show that the magnetism of the material FexNi1-xMn2O4 changes with the value of x and reaches a maximum in the range x from 0.5 to 0.7.


2013 ◽  
Vol 802 ◽  
pp. 119-123
Author(s):  
Supamas Wirunchit ◽  
Rangson Muanghlua ◽  
Supamas Wirunchit ◽  
Wanwilai Vittayakorn ◽  
Naratip Vittayakorn

Nanocrystalline barium zirconium titanate, BaZr0.4Ti0.6O3, was synthesized successfully via the sonochemical process. The effects of reaction time on the precipitation of Ba(Zr,Ti)O3 particles were investigated briefly. The crystal structure as well as molecular vibrations and morphology were investigated. X-ray diffraction indicated that the powders exhibited a single phase perovskite structure, without the presence of pyrochlore or unwanted phases at the reaction time of 60 min. Nanocrystals were formed before being oriented and aggregated into large particles in aqueous solution under ultrasonic irradiation. A scanning electron microscopy (SEM) photograph showed the BZT powder as spherical in shape with uniform nanosized features.


2007 ◽  
Vol 119 ◽  
pp. 71-74 ◽  
Author(s):  
Yan Li ◽  
Xiao Li Zhang ◽  
Young Hwan Kim ◽  
Young Soo Kang

Co nanoparticles were synthesized via a solventless thermal decomposition of Co2+-oleate2. The crystalline structure is strongly affected by the thermal treatment of the Co nanoparticles. Further, the annealing also results in the decomposition of surfactant around Co particles. The size of nanoparticles was confirmed by transmission electron microscopy (TEM). The crystal structure of nanoparticles was characterized by X-ray diffraction pattern (XRD). The magnetic properties were characterized by vibrating sample magnetometer (VSM).


2013 ◽  
Vol 802 ◽  
pp. 227-231
Author(s):  
Panida Pilasuta ◽  
Pennapa Muthitamongkol ◽  
Chanchana Thanachayanont ◽  
Tosawat Seetawan

Crystal structure of Zn0.96Al0.02Ga0.02O was analyzed by X-Ray diffraction (XRD) technique and the microstructure was observed by scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The XRD results showed single phase and hexagonal structure a = b = 3.24982 Å, and c = 5.20661 Å. The SEM and TEM results showed the grain size of material arrangement changed after sintering and TEM diffraction pattern confirmed hexagonal crystal structure of Zn0.96Al0.02Ga0.02O after sintering.


1990 ◽  
Vol 04 (12) ◽  
pp. 791-794 ◽  
Author(s):  
YANG JI-LIAN ◽  
YE CHUN-TANG ◽  
ZHANG BAI-SHENG ◽  
LI JI-ZHOU ◽  
KANG JIAN ◽  
...  

The polycrystalline sample of (Bi–Pb)2Sr2Ca2Cu3O10 with Tc=107 K was prepared. The X-ray diffraction proved that the sample is single phase. The crystal structure study on the sample has been carried out by neutron diffraction. The result shows that its structure is tetragonal body-centre structure with space group of I4/mmm, containing a few oxygen atoms at 4e site in Bi–Pb layers.


2004 ◽  
Vol 18 (05n06) ◽  
pp. 221-231 ◽  
Author(s):  
MANORANJAN KAR ◽  
S. RAVI

X-ray diffraction, electrical resistivity and ac susceptibility measurements have been carried out on La 1-x Ag x MnO 3 compounds for x=0.05 to 0.30. These samples are found to be in single phase form with [Formula: see text] space group and with typical lattice parameters a=b=5.524Å and c=13.349Å for x=0.05 sample. The Mn–O–Mn bond angles and variance, σ2 are found to increase with doping. Metal-insulator transitions in the temperature range 254 to 259 K have been observed. These materials exhibit paramagnetic to ferromagnetic transitions in the vicinity of metal-insulator transition temperatures. The paramagnetic susceptibility could be analyzed using Curie–Weiss law. All the above samples exhibit colossal magneto-resistivity and its maximum value is found to be 73% for x=0.15 sample at 50 kOe magnetic field.


2014 ◽  
Vol 602-603 ◽  
pp. 947-950
Author(s):  
Zhen Wang ◽  
Hai Yan Chen ◽  
Lin Qiang Gao ◽  
Xin Zou

BiFeO3 nanoparticles were successfully synthesized by a hydrothermal method by a mineralizer (KNO3). Structural characterization was performed by thermal analysis, powder X-ray diffraction (XRD) and scanning electron microscopy (TEM).The results showed that the products were perovskite structure BiFeO3 powders. Optimal conditions for the synthesis of single-phase BiFeO3 ceramics were obtained.


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