Preparation and Magnetostriction of Epoxy-Bonded Pr(Fe0.4Co0.6)1.93 Composites

2012 ◽  
Vol 476-478 ◽  
pp. 1370-1373
Author(s):  
X Liu ◽  
J.J Liu ◽  
R.R Lin ◽  
H.Y Yin ◽  
X.C Liu ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Vibrating Sample Magnetometer ◽  
X Ray Diffraction ◽  
Standard Strain ◽  
Easy Magnetization ◽  
Magnetization Direction ◽  
X Ray ◽  
Magnetoelastic Properties ◽  
Type Composite ◽  
Easy Magnetization Direction

The magnetostrictive Pr(Fe0.4Co0.6)1.93alloy with MgCu2-type structure, and its 0-3 and pseudo 1-3 type epoxy-bonded composites were fabricated by curing without and with a magnetic field. The structural, magnetic and magnetoelastic properties were investigated by means of x-ray diffraction, a vibrating sample magnetometer and a standard strain technique. The 0-3 type composite has a larger magnetostriction than the 1-3 composite has, which can be ascribed to the easy magnetization direction (EMD) not lying along direction.

Magnetostriction of Epoxy-Bonded Tb0.22Dy0.48Pr0.3(Fe0.9B0.1)1.93 Composites

2011 ◽  
Vol 295-297 ◽  
pp. 978-981
Author(s):  
Jin Jun Liu ◽  
Xiang Liu ◽  
Hong Yun Yin ◽  
Xin Cai Liu ◽  
Ping Zhan Si
Keyword(s):  
Magnetic Field ◽  
Room Temperature ◽  
Chain Structure ◽  
X Ray Diffraction ◽  
Standard Strain ◽  
Easy Magnetization ◽  
Magnetization Direction ◽  
X Ray ◽  
Magnetoelastic Properties ◽  
Easy Magnetization Direction

The magnetostrictive Tb0.22Dy0.48Pr0.3(Fe0.9B0.1)1.93 alloy, and its 0-3 and pseudo 1-3 type epoxy-bonded composites were fabricated by curing without and with a magnetic field. The structural, magnetic and magnetoelastic properties were in investigated by means of x-ray diffraction, an alternating gradient magnetometer and a standard strain technique. The easy magnetization direction (EMD) is lying along <111> direction at room temperature. The 1-3 type composites has a larger magnetostriction than the 0-3 composite has, which can be attributed to the <111>-textured orientation and the chain structure.

Structure and Magnetostriction of PrxTb1-xFe1.9Ti0.1 Alloys

2013 ◽  
Vol 281 ◽  
pp. 413-416
Author(s):  
He Yan Liu ◽  
Guo Dong Liu ◽  
Ying Li ◽  
Hong Zhi Luo ◽  
Shao Ling Zhang ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Crystal Structure ◽  
Single Phase ◽  
Annealing Treatment ◽  
Annealed Sample ◽  
Vibrating Sample Magnetometer ◽  
X Ray Diffraction ◽  
Standard Strain ◽  
X Ray ◽  
Type Crystal

The structure and magnetostriction have been investigated for PrxTb1-xFe1.9Ti0.1 alloys by means of the X-ray diffraction phase analysis, vibrating sample magnetometer, and standard strain gauge technique. Comparing the structure of bulk and annealed samples, it can be found that the annealing treatment is of benefit to the formation of single phase with MgCu2-type crystal structure when x0.3. The magnetization at the maximal magnetic field decreases rapidly with increasing Pr content. The magnetostriction for Pr0.2Tb0.8Fe1.9Ti0.1 annealed sample at 900kA/m is 1733ppm. The magnetostriction for PrxTb1-xFe1.9Ti0.1 alloys at 900kA/m also decreases with increasing Pr content.

scholarly journals Dynamic magnetoelastic properties of TbxHo0.9−xNd0.1(Fe0.8Co0.2)1.93/epoxy composites

2019 ◽  
Vol 37 (2) ◽  
pp. 257-264 ◽  
Author(s):  
W.C. Shen ◽  
L.L. Lin ◽  
C.Y. Shen ◽  
S. Xing ◽  
Z.B. Pan
Keyword(s):  
Room Temperature ◽  
Bias Field ◽  
Material System ◽  
Magnetic Bias ◽  
Easy Magnetization ◽  
Magnetization Direction ◽  
Magnetoelastic Properties ◽  
Type Composite ◽  
Easy Magnetization Direction ◽  
Orientation Structure

AbstractTbxHo0.9−xNd0.1(Fe0.8Co0.2)1.93/epoxy (0 ⩽ x ⩽ 0.40) composites are fabricated in the presence of a magnetic field. The structural and dynamic magnetoelastic properties are investigated as a function of both magnetic bias field Hbias and frequency f at room temperature. The composites are formed as textured orientation structure of 1–3 type with 〈1 0 0〉 preferred orientation for x ⩽ 0.10 and 〈1 1 1〉-orientation for x ⩾ 0.25. The composites generally possess insignificant eddy-current losses for frequency up to 50 kHz, and their dynamic magnetoelastic properties depend greatly on Hbias. The elastic modulus (E3H and E3B) shows a maximum negative ΔE effect, along with a maximum d33, at a relatively low Hbias ~ 80 kA/m, contributed by the maximum motion of non-180° domain-wall. The 1–3 type composite for x ⩾ 0.25 shows an enhanced magnetoelastic effect in comparison with 0 to 3 type one, which can be principally ascribed to its easy magnetization direction (EMD) towards 〈1 1 1〉 axis and the formation of 〈1 1 1〉-texture-oriented structure in the composite. These attractive dynamic magnetoelastic properties, e.g., the low magnetic anisotropy and d33,max as high as 2.0 nm/A at a low Hbias ~ 80 kA/m, along with the light rare-earth Nd element existing in insulating polymer matrix, would make it a promising magnetostrictive material system.

Study on the Preparation Technique and Magnetostriction of Sinter Tb0.7Pr0.3Fe1.80 Alloy

2012 ◽  
Vol 189 ◽  
pp. 152-156
Author(s):  
H.Y. Yin ◽  
X. Liu ◽  
R. Wang ◽  
Jin Jun Liu ◽  
R.R. Lin ◽  
...  
Keyword(s):  
Mechanical Alloying ◽  
Laves Phase ◽  
Type Structure ◽  
Preparation Technique ◽  
Sintering Process ◽  
X Ray Diffraction ◽  
Standard Strain ◽  
X Ray ◽  
Magnetoelastic Properties ◽  
Composite Samples

Mechanical alloying (MA) and subsequent solid sintering process was used to prepare the Pr-containing pseudobinary Tb0.7Pr0.3Fe1.80alloys. The structural and magnetoelastic properties were in comparative investigated by means of x-ray diffraction and a standard strain technique for sinter and composite samples. The high Pr-content (Tb,Pr)Fe2Laves phase with MgCu2-type structure for the composition Tb0.7Pr0.3Fe1.80 were synthesized by MA plus annealing at 500 °C.

Structure and Magnetostriction of Tb0.7Pr0.3FeX Prepared by Solid-State Synthesis

2012 ◽  
Vol 476-478 ◽  
pp. 1459-1462 ◽  
Author(s):  
H.Y Yin ◽  
J.J Liu ◽  
R Wang ◽  
X.C Liu ◽  
N.K Sun ◽  
...  
Keyword(s):  
Solid State ◽  
Mechanical Alloying ◽  
Annealing Process ◽  
Laves Phase ◽  
Type Structure ◽  
Solid State Synthesis ◽  
X Ray Diffraction ◽  
Standard Strain ◽  
X Ray ◽  
Magnetoelastic Properties

Mechanical alloying (MA) was used to prepare pseudobinary high Pr-content Tb0.7Pr0.3Fex alloys. The structural and magnetoelastic properties were in investigated by means of x-ray diffraction and a standard strain technique. A single (Tb,Pr)Fe2 Laves phase with MgCu2-type structure for the composition Tb0.7Pr0.3Fe1.80 was synthesized by MA and subsequent annealing process. The high magnetostriction of 600 ppm was achieved at 10 kOe for the epoxy-bonded Tb0.7Pr0.3Fe1.8 composite.

Crystal Structure and Magnetic Properties of Novel Compound PrFe8Ga3C

2009 ◽  
Vol 152-153 ◽  
pp. 75-78 ◽  
Author(s):  
V.S. Gaviko ◽  
A.G. Popov ◽  
G.V. Ivanova ◽  
N.V. Mushnikov ◽  
Y.V. Belozerov ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Room Temperature ◽  
Spontaneous Magnetization ◽  
Anisotropy Constant ◽  
X Ray Diffraction ◽  
Easy Magnetization ◽  
Magnetization Direction ◽  
X Ray ◽  
Powder Samples ◽  
Curie Temperature Tc

We have synthesized a novel intermetallic compound PrFe8Ga3C and studied its structure and magnetic properties. X-ray diffraction analysis revealed that the compound possesses a tetragonal BaCd11-type structure (space group I41/amd). In this structure Ga atoms occupy the same sites as Fe atoms with preferably filling the 4(b) site. Magnetization curves have been measured on the aligned powder samples. Below the Curie temperature TC = 400 K the easy magnetization direction was found to orient within the (100) plane. At 80 K the compound has a spontaneous magnetization of 97 emu/g and anisotropy constant of 4.2107 erg/cm3. At room temperature these values reduce to 78 emu/g and 4.7106 erg/cm3, respectively.

On magnetic domain configurations in single-crystal, (112)-orientation plates of iron-silicon alloy: some X-ray topographic observations and their interpretation

1993 ◽  
Vol 442 (1914) ◽  
pp. 161-175 ◽  
Keyword(s):  
Single Crystal ◽  
Reasonable Agreement ◽  
Minimum Energy ◽  
Magnetic Domain ◽  
Easy Magnetization ◽  
Magnetization Direction ◽  
X Ray ◽  
Ferromagnetic Crystal ◽  
Easy Magnetization Direction ◽  
Specimen Interior

Possible magnetization states of a cubic ferromagnetic crystal having easy magnetization directions parallel to the cube axes (as in Fe + 3 mass % Si alloy) can be represented using a regular octahedron, as first shown by Néel. This model is developed to derive rules that govern shapes and relative volumes of the differently magnetized domains needed to produce mean magnetization lying in a plane of any orientation. Single-crystal plates of Fe + 3 mass % Si alloy not containing an easy-magnetization direction, such as plates parallel to (112) studied in this work, are in general subdivided into a hierarchy of domains that in spatial scale diminish from specimen interior towards specimen surfaces. X-ray topography offers a non-contacting method of mapping domain configurations. Under appropriate diffraction conditions the strains associated with 90° Bloch walls generate strong diffraction contrast. In X-ray transmission topographs the superimposition of contrast from surface closure domains upon that of inner domains generally gives rise to highly complex images from (112) plates. However, with specimen thicknesses less than 20 μm the patterns can become sufficiently simplified to make possible the identification of shapes and magnetization axes of all domains present. A pattern in this class is illustrated, and interpreted with the aid of the octahedron. Reasonable agreement is found between the observed size scale of the domains and that calculated for minimum energy in the domain structure proposed.

Magnetic and Magnetostrictive Properties of Tb-Dy-Ho-Fe-Co Alloys

2009 ◽  
Vol 152-153 ◽  
pp. 7-10 ◽  
Author(s):  
Irina S. Tereshina ◽  
S.A. Nikitin ◽  
G.A. Politova ◽  
A.S. Ilyushin ◽  
A.A. Opolenko ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Magnetic Properties ◽  
Rare Earth ◽  
Applied Magnetic Field ◽  
Single Phase ◽  
X Ray Diffraction ◽  
Standard Strain ◽  
X Ray ◽  
Structural And Magnetic Properties ◽  
Co Alloys

In this work, the structural and magnetic properties of single-phase TbxDyyHoz(Fe,Co)2 (x + y + z = 1) alloys have been investigated by means of X-ray diffraction, 57Fe Mossbauer spectroscopy, magnetization measurements and a standard strain gage technique. The magnetostriction of TbxDyyHoz(Fe,Co)2 was examined against an applied magnetic field up to 10 kOe in 80 - 400 K temperature range. The Co-containing compounds are found to have high values of magnetostrictive susceptibility due to compensation of magnetic anisotropy in both the rare-earth and 3d transition metals sublattices.

scholarly journals Magnetoelastic properties of epoxy resin based TbxHo0.9−xNd0.1 (Fe0.8Co0.2)1.93 particulate composites

2017 ◽  
Vol 35 (1) ◽  
pp. 81-86 ◽  
Author(s):  
Z.R. Zhang ◽  
J.J. Liu ◽  
X.H. Song ◽  
F. Li ◽  
X.Y. Zhu ◽  
...  
Keyword(s):  
Magnetic Anisotropy ◽  
Volume Fraction ◽  
Particle Volume Fraction ◽  
Particulate Composites ◽  
Particle Volume ◽  
Easy Magnetization ◽  
Magnetization Direction ◽  
Alloy Particles ◽  
Magnetoelastic Properties ◽  
Easy Magnetization Direction

AbstractTbxHo0.9−xNd0.1 (Fe0.8Co0.2)1.93 (0 ⩽ x ⩽ 0.40) particulate composites were prepared by embedding and aligning alloy particles in an epoxy matrix with and without a magnetic curing field. The magnetoelastic properties were investigated as functions of composition, particle volume fraction and macroscopic structure of the composite. The magnetic anisotropy compensation point was found to be around x = 0.25, where the easy magnetization direction (EMD) at room temperature was detected lying along ⟨ 1 1 1 ⟩ axis. The composite with ⟨ 1 1 1 ⟩ preferred orientation and pseudo-1-3 type structure was prepared under an applied magnetic field of 12 kOe. An enhanced magnetoelastic effect and large low-field magnetostriction λa, as high as 430 ppm at 3 kOe, were obtained for Tb0.25Ho0.65Nd0.1 (Fe0.8Co0.2)1.93 composite rod. The value of λa was of 72 % of its polycrystalline alloy (~595 ppm/3 kOe) although it only contained 30 vol.% of the alloy particles. This enhanced effect can be attributed to the larger λ111 (as compared to λ100), low magnetic anisotropy, easy magnetization direction (EMD) along the ⟨ 1 1 1 ⟩ axis and ⟨ 1 1 1 ⟩-textured orientation of the alloy particles as well as the chain-like structure of the composite. The good magnetoelastic properties of the composite, in spite of the fact that it contained only 30 vol.% of the alloy particles with light rare-earth Nd element in the insulating epoxy, would make it a potential material for magnetostriction application.

SELF-ASSEMBLED COBALT CHAINS INDUCED BY MAGNETIC FIELD THROUGH HYDROTHERMALLY REDUCING COBALT IONS

2011 ◽  
Vol 25 (32) ◽  
pp. 4323-4329 ◽  
Author(s):  
FAN ZHAO ◽  
MIN YAO ◽  
JUN WANG
Keyword(s):  
Magnetic Field ◽  
Large Scale ◽  
Three Dimensional ◽  
Vibrating Sample Magnetometer ◽  
X Ray Diffraction ◽  
Cross Sectional ◽  
Cobalt Ions ◽  
X Ray ◽  
Hierarchical Microspheres ◽  
Potential Applications

Co uniform hierarchical microspheres were grown on a large scale at 200° by a simple hydrothermal method with the help of the surfactant polyvinylpyrrolidone (PVP). During the synthesis, the external magnetic field as a controlling factor assembled cobalt microspheres to form chain-like structures vertically on substrate. X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to characterize the product. The results indicate that three-dimensional (3D) Co microspheres are constructed by the cross-sectional nanoplatelets shape with a mean thickness of ~ 250 nm. The mechanism involved for the formation of the chain-like structures is discussed. The results of the vibrating sample magnetometer (VSM) show that the magnetic Co chains possess the saturation magnetization of 125.2 emu/g. Our work may shed some light on the design of other well-defined complex nanostructures, and as-grown architectures may have potential applications.

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