Study on Extraction Process of Technics of Litsea Cubeba Oil

2014 ◽  
Vol 602-605 ◽  
pp. 81-85 ◽  
Author(s):  
Zuo Ren Liu ◽  
Yan Fen Zhang ◽  
Yong Guang Bi ◽  
Hai Ling Li
Keyword(s):  
Visual Analysis ◽  
Extraction Process ◽  
Oil Extraction ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Litsea Cubeba ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

Litsea cubeba fruit as raw material in this experiment, the use of ultrasonic-assisted method of litsea cubeba oil extraction process are discussed. The effects of several ultrasonic processing parameters, such as ratio of liquid to solid, extraction temperature, ultrasonic power and extraction time on the extraction of litsea cubeba oil were investigated assisted by ultrasonic wave. And the L9 (34) orthogonal test was used to research this four factors, the result from the visual analysis indicated that the optimal extraction process was gotten when ratio of liquid to solid was 14:1 , ultrasonic time was 50min, ultrasonic power is 320W, ultrasonic temperature is 60 °C.Those experimental results showed that ultrasonic-assisted extraction of the Litsea cubeba oil is practicable, and this method is simple and efficient. With the preliminary investigation of the ultrasonic-assisted extraction of Litsea Cubeba oil, the oil yield reached up to 41.35%, this value is the highest of all the oil yields from the current oil extraction methods, and it is worthy of further exploration .

scholarly journals Ultrasonic-Assisted Extraction of Procyanidins Using Ionic Liquid Solution fromLarix gmeliniiBark

2013 ◽  
Vol 2013 ◽  
pp. 1-9 ◽  
Author(s):  
Xiaowei Sun ◽  
Zhimin Jin ◽  
Lei Yang ◽  
Jingwei Hao ◽  
Yuangang Zu ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Ionic Liquids ◽  
Extraction Efficiency ◽  
Liquid Solution ◽  
Extraction Process ◽  
Ultrasonic Power ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

An ionic liquid-based ultrasonic-assisted extraction method has been developed for the effective extraction of procyanidins fromLarix gmeliniibark. So as to evaluate the performance of ionic liquids in ultrasonic-assisted extraction process, the effects caused by changes in the anion and the alkyl chain length of the cation on the extraction efficiency were investigated in this paper. The results indicated that the characteristics of anions had remarkable effects on the extraction efficiency of procyanidins, and 1-butyl-3-methylimidazolium bromide ([Bmim]Br) aqueous solution was the best among the investigated ionic liquids. The optimum conditions for the extraction were as follows: [Bmim]Br concentration 1.25 M, soak time 3 h, solid-liquid ratio 1 : 10, ultrasonic power 150 W, and ultrasonic time 30 min. This work not only introduces a simple, green, and highly efficient sample preparation method for extraction of procyanidins fromL. gmeliniibark, but also reveals the tremendous application potential of ionic liquids.

scholarly journals Optimization of Ultrasonic-Assisted Extraction, Characterization, and Antioxidant Activities of Polysaccharides From Sojae Semen Praeparatum

2021 ◽  
Vol 16 (5) ◽  
pp. 1934578X2110206
Author(s):  
Yongshuai Jing ◽  
Ruijuan Zhang ◽  
Lan Li ◽  
Danshen Zhang ◽  
Yu Liu ◽  
...  
Keyword(s):  
Antioxidant Activities ◽  
Deae Cellulose ◽  
Chemical Compositions ◽  
Hydroxyl Groups ◽  
Ultrasonic Frequency ◽  
Ultrasonic Power ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

In this study, response surface methodology (RSM) was used to optimize the ultrasonic-assisted extraction parameters of Sojae Semen Praeparatum polysaccharides (SSPP-80), the optimum conditions were determined as follows: ultrasonic frequency of 100 W, ultrasonic power of 80 Hz, ultrasonic temperature of 52℃, ultrasonic time of 23 minutes, and liquid to raw material ratio of 40 mL/g. Based on these conditions, polysaccharides extraction rate was 7.72% ± 0.26%. Then, 2 novel polysaccharides (SSPP-80‐1, SSPP-80‐2) were isolated from SSPP by DEAE-cellulose 52 chromatography. The chemical compositions, physicochemical properties, and structure of SSPPs were investigated by simultaneous thermal analyzer (TGA), scanning electron microscopy (SEM), fourier transform infrared spectroscopy (FI-IR), and high-performance liquid chromatography (HPLC). The results showed that SSPP-80 and 2 fractions were mainly composed of mannose (Man), glucose (Glc), galactose (Gal), xylose (Xyl), and arabinose (Ara). In addition, the antioxidant activities were evaluated against the DPPH and hydroxyl radical in vitro, the IC50 of SSPP-80, SSPP-80‐1 and SSPP-80‐2 against DPPH free radical were 4.407, 8.267, and 5.204 mg/mL, respectively, whereas the IC50values for removing hydroxyl groups were 5.318, 3.516, and 4.016 mg/mL, respectively. It demonstrated that SSPP-80 and 2 fractions had certain antioxidant activity. Theoretical basis for use of Sojae Semen Praeparatum polysaccharides was provided by this study.

Optimization of Ultrasonic-Assisted Extraction of Total Saponins from Ophiopholis mirabilis Using Response Surface Methodology

2013 ◽  
Vol 781-784 ◽  
pp. 687-693
Author(s):  
Zhi Yang Shao ◽  
Jin Xia Fu ◽  
Yan Xia Qi ◽  
Qian Cheng Zhao ◽  
Zhi Bo Li
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Ethanol Concentration ◽  
Water Bath ◽  
Ultrasonic Power ◽  
Extraction Technology ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

Ultrasonic-Assisted extraction (UAE) was applied for saponins extraction from Ophiopholis mirabilis and response surface methodology (RSM) was used to optimize the extraction technology. A first set of experiments were designed to optimize water bath temperature, ethanol concentration, the ratio of liquid to solid, ultrasonic time (min) and ultrasonic power (W) as the main variables affecting the extraction effect. A Box-Behnken design consisting of 15 experimental runs was then applied and a second-order polynomial model was used to explain the interactions between the main factors and the yield of saponins. The developed mathematical model was found to fit well with the experimental data and the optimized conditions were ultrasonic pretreatment time 30.9 min, ethanol concentration 64%, liquid /solid ratio 35:1, ultrasonic power 300W and water bath 70°C. Corresponding saponins content was 0.574%.

ULTRASONIC-ASSISTED EXTRACTION OF OIL FROM CALOPHYLLUM INOPHYLLUM SEEDS: OPTIMIZATION OF PROCESS PARAMETERS

2016 ◽  
Vol 78 (10) ◽  
Author(s):  
Faiznur Mohd Fuad ◽  
Mashitah Mat Don
Keyword(s):  
Solvent Extraction ◽  
Extraction Time ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Calophyllum Inophyllum ◽  
Power Extraction ◽  
Optimization Of Process Parameters ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

Calophyllum inophyllum (C. inophyllum) is a plant known as “Penaga Laut” in Malaysia. Its seeds contain valuable oil that serve as a potential alternative sources for vegetable oil. In this study, C. inophyllum seeds oil was extracted using an ultrasonic-assisted extraction (UAE) technique. The optimization of extraction parameters namely different types of solvent, extraction time, ultrasonic power, extraction temperature and liquid to solid (L/S) ratio were performed using one-factor-at-a-time (OFAT) method. The optimum extraction conditions obtained were n-hexane as a solvent, extraction time 20 min, ultrasonic power 210 W, extraction temperature 40°C and L/S ratio 20 ml/g, with an oil yield 55.44 ± 0.53 %.

Optimization for the Process of Chlorophyll a Extraction by Orthogonal Method

2014 ◽  
Vol 1051 ◽  
pp. 423-427
Author(s):  
Jun Sen Wu ◽  
Chen Chen Liu ◽  
Bing Li ◽  
Xiu Zhi Wan
Keyword(s):  
Chlorophyll A ◽  
Orthogonal Experiment ◽  
Ultrasonic Power ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction ◽  
Extraction Agent ◽  
Optimum Extraction ◽  
Single Factor Experiment

The 90% acetone as extraction agent used in order to obtain the ultrasonic assisted extraction conditions of chlorophyll a. The ultrasonic power, ultrasonic time, centrifugation time and rotational speed as the four study factors and the chlorophyll a concentration as the target, here, the L9(34) orthogonal table of orthogonal experiment design are used in order to determine the optimum extraction contractions, basing on the single factor experiment. The experimental results shows the algae containing water can get better extraction effect, after ultrasonic 30 minutes in 225W and 6000r/min speed centrifugal 9 minutes and then mixing, repeat ultrasound centrifugation steps.

scholarly journals Study on the Optimization for the Extraction Process of Andrographolide by Ultrasonic Assisted Extraction

2021 ◽  
pp. 08-17
Author(s):  
KiBong Kim ◽  
IlJin Kim ◽  
SongLok Uh ◽  
YongIl Seo ◽  
CholKwang Li ◽  
...  
Keyword(s):  
Optimum Condition ◽  
Response Surface ◽  
Folk Medicine ◽  
Solution Concentration ◽  
Extraction Process ◽  
Extraction Temperature ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction ◽  
Medical Role

Because andrographis has a long history of folk medicine in Southeast Asian countries with antibacterial, antipyretic, antineoplastic, anti-inflammatory, cardioprotective effect and so on, the areas where andrographolia is introduced and cultivated are mainly concentrated. Espically andrographolide, neoandrographolide, andrographiside, homoandrographolide, andrographane, andrographanin, andrographone and andrographosterol that is concentrated in the leaves of the plant play the main medical role of andrographis. Of the above chemicals, andrographolide is the major bioactive constituent responsible for variety of activities. Leaves and stems of plant are used for extracting active phytochemicals; roots are used rarely. In this study, improved the extractability of andrographolide from the A. paniculata by ultrasonic assisted extraction, the optimum condition for extracted the andrographolide is determined by response surface experiment and detected the extractability of andrographolide under the optimum condition. By single factor analysis and response surface experiments, the optimum conditions for extracted the andrographolide were the extraction solution concentration 62.8%, the ultrasonic extraction time 59min, the ratio of solid to liquid 1:10.5 and the extraction temperature 62?. Investigate the andrographolide extractability in the optimun extraction condition by HPLC were increased from 2.27% to 3.28%.

Ultrasonic-Assisted Extraction and Antioxidant Activities of Polysaccharides from Radix astragali

2013 ◽  
Vol 864-867 ◽  
pp. 549-552 ◽  
Author(s):  
Ming Wu ◽  
Chuan Fu Ma ◽  
Jun Man Kan ◽  
Li Quan Guo
Keyword(s):  
Superoxide Anion ◽  
Antioxidant Activities ◽  
Radical Scavenging ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Radix Astragali ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction ◽  
Solid Liquid

Ultrasonic-assisted extraction (UAE) method was used to polysaccharides from Radix Astragali (RAP), and the orthogonal test was applied to optimize extraction conditions. Furthermore, the antioxidant activities of RAP were evaluated by DPPH and superoxide anion radical scavenging activities assay. The results indicated that the optimal conditions for RAP extraction as followings: solid/liquid ratios of 1:20, extraction time of 10 min, ultrasonic power of 65 W and extraction temperature of 60°C. Meanwhile, RAP had relatively higher scavenging activities on DPPH and superoxide anion radicals.

scholarly journals Ultrasonic-Assisted Extraction of Natural Yellow Pigment from Physalis pubescens L. and Its Antioxidant Activities

2018 ◽  
Vol 2018 ◽  
pp. 1-6
Author(s):  
Haitang Wang ◽  
Lin Shi ◽  
Xiaoyu Yang ◽  
Rui Hong ◽  
Liang Li
Keyword(s):  
Antioxidant Activities ◽  
Radical Scavenging Activity ◽  
Radical Scavenging ◽  
Yellow Pigment ◽  
Ultrasonic Power ◽  
Optimal Parameters ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

Physalis pubescens L. is rich in natural pigments but has not yet been fully utilized. Ultrasound-assisted extraction of yellow pigment from Physalis pubescens L. was investigated by response surface methodology in this study. Optimal parameters were ultrasonic power of 29.21%, ultrasonic time of 14.41 min, and ultrasonic interval time of 10.55 s. The yield was 0.193% under optimal parameters. FRAP, ABTS, and superoxide radical scavenging activity of the yellow pigment were 6.11 ± 0.22 mmol/g, 2.80 ± 0.27 mmol/g, and 57281.5 ± 2749.5 U/g, respectively. The results showed that the yield of yellow pigment could be improved by ultrasonic-assisted extraction and the yellow pigment extracted by ultrasound had antioxidant activity.

Extraction and Antioxidant Activity of Ultrasonic-Assisted Flavonoids from Suaeda salsa

2011 ◽  
Vol 140 ◽  
pp. 343-349 ◽  
Author(s):  
Lei Guo ◽  
Chao Liu
Keyword(s):  
Suaeda Salsa ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Dpph Radical ◽  
Liquid Ratio ◽  
Box Behnken Design ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction ◽  
Dose Dependent

The box-behnken design combined with response surface methodology was used to optimize ultrasonic-assisted extraction of flavonoids from Suaeda salsa (Linn.) Pall. The results indicate that the highest extraction rate of flavonoids by ultrasonic-assisted extraction could arrive 5.17% using 500W ultrasonic power, 69% ethanol as solvent, 77°C extraction temperature, 1:40 solid to liquid ratio for 58 min extraction. The flavonoids-enriched extracts exhibited quite strong reducing property and excellent inhibitions of DPPH radical, hydroxyl radical. Meanwhile, it was found that the bioactivities appeared to be dose-dependent of flavonoids.

scholarly journals Application of Ionic Liquid-Based Ultrasonic-Assisted Extraction of Flavonoids from Bamboo Leaves

Molecules ◽  
2018 ◽  
Vol 23 (9) ◽  
pp. 2309 ◽  
Author(s):  
Liling Wang ◽  
Minge Bai ◽  
Yuchuan Qin ◽  
Bentong Liu ◽  
Yanbin Wang ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Ionic Liquids ◽  
Large Scale ◽  
Ultrasonic Power ◽  
Solid Ratio ◽  
Bamboo Leaves ◽  
Assisted Extraction ◽  
Ultrasonic Time ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

Ionic liquids (ILs), known as environmentally benign “green” solvents, were developed as an optimal solvent for the green extraction and separation field. In this paper, an ionic liquid-based ultrasonic-assisted extraction (IL-UAE) of flavonoids (FVs) from bamboo leaves of Phyllostachys heterocycla was developed for the first time. First, 1-butyl-3-methylimidazolium bromide ([Bmim] Br), with the best extraction efficiency, was selected from fifteen ionic liquids with diverse structure, like carbon chains or anions. Then, the influencing parameters of ionic liquid (IL) concentration, liquid-solid ratio, ultrasonic time, and ultrasonic power, were investigated by single factor tests, and further optimized using response surface methodology (RSM). In the optimization experiment, the best conditions were 1.5 mol/L [BMIM]Br aqueous solution, liquid-solid ratio 41 mL/g, ultrasonic time 90 min, and ultrasonic power 300 W. Furthermore, the microstructures of bamboo leaves and the recovery of FVs and [BMIM]Br were also studied. Therefore, this simple, green and effective IL-UAE method has potentiality for the extraction of FVs from bamboo leaves for the large-scale operations.

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