Thermogravimetric Analysis of Different Calcination Temperature of Lemon Grass Ash

2014 ◽  
Vol 695 ◽  
pp. 232-234
Author(s):  
Nur Firdaus Mohamed Yusof ◽  
Hakimah Osman ◽  
Rozyanty Rahman
Keyword(s):  
Thermal Stability ◽  
High Temperature ◽  
Thermogravimetric Analysis ◽  
Calcination Temperature ◽  
Control Element ◽  
Calcination Temperatures ◽  
Lemon Grass ◽  
Thermal Stability Of

Lemon grass ash is produced at 0, 400, 525, 600 and 700°C calcination temperatures. The thermal stability of lemon grass ash calcination at various temperatures was examined by using a thermogravimetric analysis (TGA) instrument. The lemon grass ash calcinated at 700°C exhibit the highest thermal stability due to the highest combustion of high amount of minerals such as silica, potassium and calcium occur in the sample at high temperature. Besides, lemon grass calcinated at 0°C (as control element) showed the lowest thermal stability due to the present of carboneous substance such as hemicellulose and lignin. However, the thermal stability of lemon grass ash is increased at higher calcination temperatures.

The Ordered Phase Formation in Ti-Al-Ga Alloys

1970 ◽  
Vol 28 ◽  
pp. 440-441
Author(s):  
Shiro Fujishiro ◽  
Harold L. Gegel
Keyword(s):  
Thermal Stability ◽  
High Temperature ◽  
Titanium Alloys ◽  
Growth Kinetics ◽  
Stoichiometric Composition ◽  
Good Potential ◽  
Alpha Titanium ◽  
Cold Rolled ◽  
Kinetics Of ◽  
Thermal Stability Of

Ordered-alpha titanium alloys having a DO19 type structure have good potential for high temperature (600°C) applications, due to the thermal stability of the ordered phase and the inherent resistance to recrystallization of these alloys. Five different Ti-Al-Ga alloys consisting of equal atomic percents of aluminum and gallium solute additions up to the stoichiometric composition, Ti3(Al, Ga), were used to study the growth kinetics of the ordered phase and the nature of its interface.The alloys were homogenized in the beta region in a vacuum of about 5×10-7 torr, furnace cooled; reheated in air to 50°C below the alpha transus for hot working. The alloys were subsequently acid cleaned, annealed in vacuo, and cold rolled to about. 050 inch prior to additional homogenization

Thermal Stability of N-Heterocycle-Stabilized Iodanes – A Systematic Investigation

2019 ◽  
Author(s):  
Andreas Boelke ◽  
Yulia A. Vlasenko ◽  
Mekhman S. Yusubov ◽  
Boris Nachtsheim ◽  
Pavel Postnikov
Keyword(s):  
Thermal Stability ◽  
Differential Scanning Calorimetry ◽  
Thermogravimetric Analysis ◽  
Systematic Investigation ◽  
Scanning Calorimetry ◽  
Thermal Stability Of

<p>The thermal stability of pseudocyclic and cyclic <i>N</i>-heterocycle-stabilized (hydroxy)aryl- and mesityl(aryl)-l<sup>3</sup>-iodanes (NHIs) through thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) is investigated. NHIs bearing <i>N</i>-heterocycles with a high N/C-ratio such as triazoles show among the lowest descomposition temperatures and the highest decomposition energies. A comparison of NHIs with known (pseudo)cyclic benziodoxolones is made and we further correlated their thermal stability with reactivity in a model oxygenation. </p>

Increased Thermal Stability of Co-silicide Using Co-Ta Alloy Films

2001 ◽  
Vol 670 ◽  
Author(s):  
Min-Joo Kim ◽  
Hyo-Jick Choi ◽  
Dae-Hong Ko ◽  
Ja-Hum Ku ◽  
Siyoung Choi ◽  
...  
Keyword(s):  
Thermal Stability ◽  
High Temperature ◽  
Grain Boundary ◽  
Reaction Rate ◽  
Boundary Migration ◽  
Grain Boundary Migration ◽  
Alloy Films ◽  
Post Annealing ◽  
Alloy Process ◽  
Thermal Stability Of

ABSTRACTThe silicidation reactions and thermal stability of Co silicide formed from Co-Ta/Si systems have been investigated. In case of Co-Ta alloy process, the formation of low resistive CoSi2phase is delayed to about 660°C, as compared to conventional Co/Si system. Moreover, the presence of Ta in Co-Ta alloy films reduces the silicidation reaction rate, resulting in the strong preferential orientation in CoSi2 films. Upon high temperature post annealing in the furnace, the sheet resistance of Co-silicide formed from Co/Si systems increases significantly, while that of Co-Ta/Si systems maintains low. This is due to the formation of TaSi2 at the grain boundaries and surface of Co-silicide films, which prevents the grain boundary migration thereby slowing the agglomeration. Therefore, from our research, increased thermal stability of Co-silicide films was successfully obtained from Co-Ta alloy process.

Thermal stability of nickel-cobalt multilayer silicide

2005 ◽  
Vol 891 ◽  
Author(s):  
Kil Jin Han ◽  
Yu Jung Cho ◽  
Soon Young Oh ◽  
Yong Jin Kim ◽  
Won Jae Lee ◽  
...  
Keyword(s):  
Thermal Stability ◽  
High Temperature ◽  
Depth Profile ◽  
Ternary Phase ◽  
Nickel Silicide ◽  
Composition Gradient ◽  
Cobalt Silicide ◽  
Nickel Cobalt ◽  
Thermal Stability Of ◽  
Xps Depth Profile

ABSTRACTIn this study, we have investigated the structure of nickel-cobalt silicide to understand its behavior at high temperature. Nickel-cobalt silicide was formed after two-step RTP at 500°C and 700°C respectively. We could observe by TEM that nickel-cobalt silicide consists of a structure which seems to be a Ni-Co-Si ternary phase. No nickel silicide phases and cobalt silicide phases were detected in nickel-cobalt silicide by XRD. From XPS depth profile, we could confirm that there is a cobalt composition gradient along the silicide.

Study of Thermal Behaviour of EPDM/SBR Blends and Carbon Nanocoatings Deposited by Sputtering

2021 ◽  
Vol 875 ◽  
pp. 116-120
Author(s):  
Muhammad Alamgir ◽  
Faizan Ali Ghauri ◽  
Waheed Qamar Khan ◽  
Sajawal Rasheed ◽  
Muhammad Sarfraz Nawaz ◽  
...  
Keyword(s):  
Thermal Stability ◽  
Weight Loss ◽  
Thermogravimetric Analysis ◽  
Thermal Behavior ◽  
Thermal Behaviour ◽  
X Ray Diffraction ◽  
X Ray ◽  
Thermal Stability Of

In this study, the effect of SBR concentration (10 Phr, 20 Phr & 30 Phr ) on the thermal behavior of EPDM/SBR blends was studied. Thermogravimetric analysis (TGA) was used to check weight loss of samples as function of temperature by heating upto 600°C. X-ray diffraction (XRD) was performed to determine quality and % crystallinity of the elastomer blends. It was seen that % crystallinity improved with an increase in the content of SBR in EPDM/SBR blends. TGA revealed that the thermal stability of EPDM/SBR blends has improved by 17% than neat EPDM. Carbon nano-coatings produced by sputtering have no beneficial influence on thermal behaviour of elastomers.

scholarly journals ALUMINA PHASE TRANSFORMATION FROM THERMAL DECOMPOSITION OF AMMONIUM ALUM SYNTHESIZED FROM KANKARA KAOLIN

2017 ◽  
Vol 36 (3) ◽  
pp. 822-828
Author(s):  
SG Bawa ◽  
AS Ahmed ◽  
PC Okonkwo
Keyword(s):  
Thermal Stability ◽  
Phase Transformation ◽  
Calcination Temperature ◽  
Starting Material ◽  
Gamma Alumina ◽  
X Ray ◽  
Alumina Phase ◽  
Ammonium Alum ◽  
Alpha Alumina ◽  
Thermal Stability Of

Thermal stability of transitional alumina phases produced from ammonium alum using Kankara kaolin as starting material was studied. Wet beneficiation method was employed to purify the starting material, after which it was calcined and dealuminated with sulphuric acid. The elemental composition, mineralogical, and physiological analyses were carried out using X-ray fluorescence (XRF), X-ray diffraction (XRD) and Brunauer-Emmett-Teller (BET) techniques respectively. The ammonium alum was thermally treated by varying the calcination temperature from 700 to 1200°C and varying the time of calcination from 1 to 4 h. The formation of gamma alumina began at calcination temperature of 825°C for calcination time of 3 h, which was found to be lower than reported works of 900°C. It was found to be stable at higher temperature of 1125°C, above which phase transformation to alpha alumina was observed. The observed wide range of thermal stability of the gamma alumina phase gives it good advantage to be used for high temperature applications, such as support for catalyst promoters. Alpha alumina phase formation began at 1150°C and was fully formed at 1200°C. BET specific surface area of 166 m2/g was obtained for the gamma alumina phase which was high enough for it application as support for catalyst, catalyst and adsorbent. http://dx.doi.org/10.4314/njt.v36i3.23

Thermal stability of high-temperature materials. Part 1

2004 ◽  
Vol 45 (5) ◽  
pp. 327-332 ◽  
Author(s):  
V. V. Kolomeitsev ◽  
S. A. Suvorov ◽  
E. F. Kolomeitseva
Keyword(s):  
Thermal Stability ◽  
High Temperature ◽  
High Temperature Materials ◽  
Thermal Stability Of
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