Rheological Characterization of Water Atomised Stainless Steel SS316L for Micro MIM

2011 ◽  
Vol 264-265 ◽  
pp. 129-134 ◽  
Author(s):  
Mohd Halim Irwan Ibrahim ◽  
Norhamidi Muhamad ◽  
Abu Bakar Sulong

This paper investigates the performance of feedstock characteristics for micro metal injection molding (μMIM) by using optimum power loading variation and rheological characterization. The study has been emphasized on the powder and binder system in which stainless steel SS316L powder are mixed with composite binder, which consists of PEG (Polyethelena Glycol), PMMA (Polymethyl Methacrilate) and SA (Stearic Acid) by variation of powder loading concentration. The rheology properties are investigated using Shimadzu Flowtester CFT-500D capillary rheometer. As the geometry of water atomised stainless steel powder are irregular shape, therefore it is expected significant changes in the rheological results that can influence the microcomponent, surface quality, shape retention and resolution capabilities. The optimization of the μMIM rheological properties as a function of stainless steel powder loading concentration are evaluated by flow behavior exponent, activation energy and moldability index. From the results, it shows that 61.5%vol contributes a significant stability over a range of temperature and the best powder loading from a critical powder volume percentage (CPVP) and rheological point of view.

2013 ◽  
Vol 315 ◽  
pp. 992-996
Author(s):  
Mohd Halim Irwan Ibrahim ◽  
Norhamidi Muhamad ◽  
A.B. Sulong

Due to its versatility, micro metal injection molding has become an alternative method in powder metallurgy where it can produce small part with a minimal number of waste. The success of micro MIM is greatly influenced by feedstock characteristics. This paper investigated the characterization and optimization which both of them plays an important characteristic in determining the successful of micro MIM. In this paper, stainless steel SS 316L was used with composite binder, which consists of PEG (Polyethelena Glycol), PMMA (Polymethyl Methacrilate) and SA (Stearic Acid). The rheology properties are investigated using Shimadzu Flowtester CFT-500D capillary rheometer. The geometry of water atomised stainless steel powder are irregular shape, therefore it is expected significant changes in the rheological results that can influence the microcomponent, surface quality, shape retention and resolution capabilities. From rheological characteristics, feedstock with 61.5% shows a significant value with several injection parameters were optimized through screening experiment such as injection pressure (A), injection temperature (B), mold temperature (C), injection time (D) and holding time (E). Besides that, interaction effects between injection pressure, injection temperature and mold temperature were also considered to optimize in the Taguchis orthogonal array. Result shows that 61.5%vol contributes a significant stability over a range of temperature and the best powder loading from a critical powder volume percentage (CPVP) and rheological point of view. Furthermore interaction between injection temperature and mold temperature (BxC) give highest significant factor followed by interaction between injection pressure and mold temperature (AxC).


2010 ◽  
Vol 44-47 ◽  
pp. 2872-2876
Author(s):  
Pei Li Haw ◽  
Norhamidi Muhamad ◽  
Hadi Murthadha

The rheological behaviors of the Micro Metal Injection Molding feedstock are important for the stability of the feedstock during micro injection molding process and quality of the final micro-components. Homogeneous feedstocks are preferable for MIM process to ensure the dimensional consistency of molded components and prevent the defects of powder-binder separation or particle segregation. In this work, feedstocks with various formulations of 316L stainless steel and binder system were prepared by using Brabender Plastograph EC Plus mixer. The binder system comprises of palm stearin, polyethelene (PE) and stearic acid. In order to obtain the viscosity, activation energy, flow behavior and mold ability index, the rheological characterization of the feedstocks were investigated in numerous conditions by using Shimadzu 500-D capillary rheometer The study showed that all of the 316L stainless steel feedstocks are homogenous with pseudo-plastic behaviors.


2011 ◽  
Vol 471-472 ◽  
pp. 558-562 ◽  
Author(s):  
Muhammad Ilman Hakimi Chua Abdullah ◽  
Abu Bakar Sulong ◽  
Norhamidi Muhamad ◽  
Mohd Fazuri Abdullah ◽  
Che Hassan Che Haron

In this paper, injection molding parameters are optimized using the L18 Taguchi orthogonal array for mechanical strength and surface quality of the green part. The feedstock used consists of stainless steel powder (SS316L) with the powder loading of 63 vol. %, 63.5 vol. % & 64 vol. %. The binder compositions used are polyethelene glycol (PEG-73 wt.%), polymethyl methacrilate (PMMA-25 wt.%) and stearic acid (4 wt.%). Mould temperature, injection temperature, injection pressure, injection time, holding time and powder loading ware selected as signal factors using Taghuci’s method based on literature, where these parameters were significant in MIM. Results showed that the optimum parameters are: mold temperature at 650C, injection temperature at1450C, injection pressure at 650 bar, injection flow rate at 20 m3/s, holding time at 5 s and powder loading of 64 vol.%. Analysis of Variance (ANOVA) result shown that mold temperature is the most influence in order to produce good green part’s surface quality while powder loading give the best result for green part’s strength.


2017 ◽  
Vol 135 ◽  
pp. 00038 ◽  
Author(s):  
AM Amin ◽  
MHI Ibrahim ◽  
MY Hashim ◽  
OMF Marwah ◽  
MH Othman ◽  
...  

2012 ◽  
Vol 217-219 ◽  
pp. 483-486
Author(s):  
Mei Yuan Ke

Effects of Sintering atmosphere and temperature on properties of warm compacted 410L stainless steel powder were studied. Sintered density, hardness, tensile strength and elongation were measured. Results showed that in order to achieve high comprehensive properties, the optimal sintering temperature was 1230°C for 410L stainless steel powder. At the same sintering temperature, density and hardness sintered in vacuum were much higher than that sintered in cracked ammonia while tensile strength sintered in cracked ammonia were much higher than that in vacuum. When sintered in vacuum at 1230°C, sintered density was 7.45 g•cm-3, hardness was 65 HRB, tensile strength was 410 MPa and elongation was 29.5%. When sintered in cracked ammonia atmosphere at 1230°C, sintered density was 7.26 g•cm-3, hardness was 97 HRB, tensile strength was 515 MPa and elongation was 3.8%.


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