Optimization of Extraction Conditions of Active Constituents from Siraitia Grosvenorii

2011 ◽  
Vol 291-294 ◽  
pp. 2523-2528 ◽  
Author(s):  
Jing Liu ◽  
Long Rong ◽  
Can Liu ◽  
Yong Hai Rong
Keyword(s):  
Amino Acids ◽  
Extraction Process ◽  
Ultrasonic Extraction ◽  
Active Constituents ◽  
Siraitia Grosvenorii

The conditions of cascade extraction and isolation of some active constituents from Siraitia grosvenorii were optimized. The active constituents were extracted by ultrasonic extraction and isolated by chromatography; the obtained active constituents were determined by HPLC and/or spectrophotometry etc. The yields of the active constituents were as follows, mogroside 3.97% (purity 91.84%), polyphenol 3.45%, free polysaccharide 12.53%, free oligosaccharide 11.96%, combined polysaccharide 2.29%, combined oligosaccharide 2.88%, amino acids 6.54% and alkaloid 7.06%. This extraction process could be used as a guideline for the multi-utilization of Siraitia grosvenorii.

Extraction of Mogroside and Limonin with Different Extraction Methods and its Modeling

2012 ◽  
Vol 8 (2) ◽  
Author(s):  
Jing Liu ◽  
Can Liu ◽  
Yonghai Rong ◽  
Long Rong
Keyword(s):  
Thin Film ◽  
Natural Products ◽  
Mass Production ◽  
Extraction Process ◽  
Extraction Methods ◽  
Ultrasonic Extraction ◽  
Citrus Reticulata ◽  
Comparison Of Methods ◽  
Economical Method ◽  
Siraitia Grosvenorii

The extraction yields of mogroside from Siraitia grosvenorii fruits and limonin from orange (Citrus reticulata Blanco) seeds were compared with different extraction methods, respectively. Maceration extraction, stirring extraction, ultrasonic extraction and flash extraction were used for the extraction. The extraction process was modeled using the concept of thin film which provides the resistance to transfer. The results showed that the maximum yields of mogroside (4.11%) and limonin (0.65%) were obtained by ultrasonic extraction and flash extraction respectively. Owing to its shorter extraction time, flash extraction would be an economical method for the mass production of triterpenes from natural products. The model was found to be fit for the comparison of methods for the extraction and provided good correlation of the data. The model could be mainly used in the practical extraction process.

Kinetics on the Ultrasonic-Assisted Extraction of Polysaccharides from Limonium bicolor kunze (Bge.)

2014 ◽  
Vol 1003 ◽  
pp. 3-6
Author(s):  
Xiao Song ◽  
Peng Zhao ◽  
Qing Hua Meng ◽  
Zhi Shu Tang ◽  
Chang Li Wang
Keyword(s):  
Kinetic Equation ◽  
Extraction Process ◽  
Ultrasonic Extraction ◽  
Second Law ◽  
Technical Design ◽  
Kinetics Parameters ◽  
Limonium Bicolor ◽  
Assisted Extraction ◽  
Ultrasonic Assisted ◽  
Ultrasonic Assisted Extraction

To explore the kinetics parameters in the ultrasonic-assisted extraction from Limonium bicolor Kunze (Bge.) , the kinetic equation for polysaccharide ultrasonic extraction process was established with ball model. According to Fick’s second law of diffusion, extraction process was analysed. The results can provide the valuable theory basis for the technical design and further research of polysaccharide extraction process.

Ultrasonic Extraction Chuanxiong Polysaccharide of Influencing Factors

2012 ◽  
Vol 550-553 ◽  
pp. 1071-1075
Author(s):  
Yong Guang Bi ◽  
Chun Chun Liu
Keyword(s):  
Influencing Factors ◽  
Extraction Process ◽  
Extraction Rate ◽  
Ultrasonic Extraction ◽  
Ultrasonic Power ◽  
Extraction Temperature ◽  
Liquid Ratio ◽  
Ultrasonic Time ◽  
Solid Liquid

In order to study the the Chuanxiong polysaccharide ultrasonic extraction process, examine the ultrasonic time, ultrasonic power, solid-liquid ratio and extraction temperature on the Chuanxiong polysaccharide extract rate. The results show that the role of time at 30min Polysaccharide better, the extraction rate is 26.63%. when the ultrasonic power is 320W, Polysaccharide extraction rate is 26.15%.When the solid-liquid ratio is 1:20, polysaccharide extraction rate is 27.73%. When the extraction temperature is 60°C, the polysaccharide extraction rate is 27.73%.

scholarly journals Research on the Extraction Process in Aqueous Two-Phase System of Moringa Leaf Flavonoids

2021 ◽  
Vol 267 ◽  
pp. 02010
Author(s):  
Rui Wang ◽  
Xueqin Zhang ◽  
Qian Zhou
Keyword(s):  
Raw Materials ◽  
Extraction Process ◽  
Ultrasonic Extraction ◽  
Extraction Time ◽  
Phase System ◽  
Extraction Temperature ◽  
Liquid Ratio ◽  
Two Phase ◽  
Aqueous Two Phase System ◽  
Solid Liquid

Moringa leaves were used as raw materials, ethanol and ammonium sulfate were used to construct a aqueous two-phase system to extract the flavonoids from Moringa leaves. The solid-liquid ratio, ethanol content, ultrasonic extraction time, and ultrasonic extraction temperature were selected as single factors, and the extraction process of flavonoids was optimized through single-factor experiments and orthogonal experiments. The optimal process was: 1:110 of solid-liquid ratio, 45 % of ethanol concentration, 15 minutes of ultrasonic extraction time, 70 °C of ultrasonic extraction temperature. Under this condition, the extraction rate of Moringa leaf flavonoids reached 8.37 %.

scholarly journals Profiling of Collagens from Swim Bladder of Catfish (Pangasius sp.) by Acid Extraction

2019 ◽  
Vol 22 (2) ◽  
pp. 327-339
Author(s):  
Gressty Sari Br Sitepu ◽  
Joko Santoso ◽  
Wini Trilaksani
Keyword(s):  
Amino Acids ◽  
Acetic Acid ◽  
Triple Helix ◽  
Extraction Process ◽  
Raw Material ◽  
Acid Extraction ◽  
Swim Bladder ◽  
Acid Pretreatment ◽  
Randomized Design ◽  
Completely Randomized Design

Swim bladders of catfish contain high protein, therefore it is can be used as a raw material for collagen. The study aims to determine the chemical characteristics of swim bladders, the pretreatment of non-collagen, extraction of collagen dissolves acid and to evaluate the characteristics of collagen. The method of this study is KOH pretreatment with a concentration of 0,05; 0,1; and 0,15 for 12 hours. The extraction process is done by soaking the sample in a solution of acetic acid with a concentration of 0,25; 0,5 and 0,75 M (ratio 1:10; b/v) and extraction time for 24; 48; and 72 hours at 4oC. The experimental design used for alkaline and acetic acid pretreatment were factorial completely randomized design. The result showed that the protein content of swim bladder was 85,26% (db), the profile of amino acids were dominated by three amino acids namely glycine (56,85 mg/g), prolyne (31,03 mg/g), and alanyne (23,85 mg/g). Using 0,05 M KOH for 8 h was selected as the best pretreatment method for collagen extraction. Extraction method using 0,50 M acetic for 48 h resulted he best collagen which revealed the existence of a triple helix structure and had Tg 84oC.

scholarly journals Magnetic Field Extraction Techniques in Preparing High-Quality Tea Infusions

2018 ◽  
Vol 8 (10) ◽  
pp. 1876
Author(s):  
Maria Tarapatskyy ◽  
Grzegorz Zaguła ◽  
Marcin Bajcar ◽  
Czesław Puchalski ◽  
Bogdan Saletnik
Keyword(s):  
Magnetic Field ◽  
Amino Acids ◽  
Age Groups ◽  
Black Tea ◽  
Extraction Process ◽  
Extraction Methods ◽  
Variable Magnetic Field ◽  
Tea Leaves ◽  
Tea Infusions ◽  
Green And Black Tea

Tea is one of the most popular drinks in the world, commonly consumed by consumers from all age groups mainly due to its refreshing taste, attractive aroma, and potentially beneficial impact on health. The composition of a tea drink depends on numerous factors, such as time and brewing temperature, degree of crumbling of tea leaves, and degree of mixing. Diffusion of the polyphenolic compounds, minerals, caffeine or theanine typical of tea infusions have been the subject of studies conducted by numerous authors. Promoting the extraction of amino acids from tea leaves when preparing infusions through the induction of a magnetic field constitutes not only another step towards the optimisation of the extraction process, but is also one of the methods to improve the nutritional value of tea infusions. The purpose of this work was to verify a hypothesis concerning the improvement of the extraction of amino acids from dried tea during the preparation of infusions by applying a permanent or variable magnetic field induced under laboratory conditions. A variable magnetic field applied as a factor assisting extraction resulted in an increased concentration in the total number of amino acids in green and black tea infusions. A statistically significant improvement in the level of free amino acids was observed after application of extraction assisted by a variable magnetic field with induction at 100 mT and a frequency of 50 Hz. Extraction using a variable magnetic field for tea infusions may constitute a good solution to assist traditional water extraction methods for research purposes.

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