Preparation and Application of Polymer Dust Suppressants in Coal Transportation under Microwave Irradiation

2011 ◽  
Vol 396-398 ◽  
pp. 1632-1635 ◽  
Author(s):  
Shui Li Lai ◽  
Qiang Chai ◽  
Bin Wang ◽  
Ning Yang
Keyword(s):  
Electron Microscopy ◽  
Aqueous Solution ◽  
Corrosion Resistance ◽  
Microwave Irradiation ◽  
Solution Polymerization ◽  
Temperature Resistance ◽  
Oxidized Starch ◽  
Aqueous Solution Polymerization ◽  
Particle Pollution ◽  
Scanning Electron

The aqueous solution polymerization of acrylic acid, acryl amide and oxidized starch under microwave irradiation was studied, and a polymer dust suppressants was synthesized. It just needs 2 mins to preparation it. The polymer dust suppressants were characterized by IR and scanning electron microscopy (SEM). Prepared several coal models by polymer dust suppressants solution (2.0 g/L) was mixed with coal, and to determine compressive strength, temperature resistance, wind corrosion resistance and water corrosion resistance. The result showed that the polymer dust suppressant can effectively reduce the coal loss and particle pollution in transportation.

scholarly journals Manufacturing, Microstructure and Corrosion Resistance of Electrophoretically Deposited SiO2 and Ni/SiO2 Coatings On X2CrNiMo17–12–2 Steel

2016 ◽  
Vol 61 (2) ◽  
pp. 1221-1227
Author(s):  
T. Ratajski ◽  
I. Kalemba-Rec ◽  
B. Dubiel
Keyword(s):  
Electron Microscopy ◽  
Aqueous Solution ◽  
Scanning Electron Microscopy ◽  
Corrosion Resistance ◽  
Cross Sections ◽  
Deposition Time ◽  
Plan View ◽  
Uniform Microstructure ◽  
Scanning Electron

Abstract The SiO2 and Ni/SiO2 coatings were electrophoretically deposited on X2CrNiMo17-12-2 steel using ethanol-based suspensions of the SiO2 and Ni powders. The influence of the zeta potential and concentration of the suspensions, the applied voltage and deposition time on the quality of the coatings was studied. Microstructure of the plan-view and cross sections of the coatings was investigated using scanning electron microscopy. The plan-view images revealed the uniform microstructure of the coatings with sporadically observed cracks, pores as well SiO2 and Ni agglomerates. On the cross-sections, the Cr2O3 layer, resulted from oxidation of the substrate during sintering of the coatings was observed. The polarization tests have shown that SiO2 and Ni/SiO2 coatings improve the corrosion resistance of the X2CrNiMo17-12-2 steel in 3.5% NaCl aqueous solution.

Preparation of Polymer Suppressant in Coal Transportation under Single Mode Microwave Irradiation

2012 ◽  
Vol 198-199 ◽  
pp. 19-22
Author(s):  
Shui Li Lai ◽  
Ying Hua Gao ◽  
Qiang Chai
Keyword(s):  
Acrylic Acid ◽  
Microwave Irradiation ◽  
Irradiation Time ◽  
Weight Ratio ◽  
Single Mode ◽  
Solution Polymerization ◽  
Oxidized Starch ◽  
Irradiation Power ◽  
Aqueous Solution Polymerization ◽  
Radiation Time

The aqueous solution polymerization of acrylic acid, acrylamide and oxidized starch under single mode microwave irradiation was studied, and a polymer suppressant was synthesized. The factors that influence on performance of the polymer suppressant were discussed, including microwave irradiation time, neutralization degree of acrylic acid (AA), the dosage of oxidized starch. The polymer suppressant was characterized by IR and scanning electron microscopy (SEM). Results indicated that the optimal synthetic conditions are as follows: microwave irradiation power, 300 W; radiation time, 2 mins; 50% neutralization degree of the AA; m(AA) : m(AM) : m(oxidized starch)= 5.0 : 3.3 : 3.4, weight ratio initiator in the feed is 0.4%, respectively.

Corrosion Behaviour of Nanocrystalline Zn-Ni and Zn-Ni-Co Electrodeposits

2011 ◽  
Vol 409 ◽  
pp. 526-531 ◽  
Author(s):  
L. Monaco ◽  
J.L. McCrea ◽  
G. Palumbo ◽  
Uwe Erb
Keyword(s):  
Electron Microscopy ◽  
Aqueous Solution ◽  
Scanning Electron Microscopy ◽  
Corrosion Resistance ◽  
Surface Morphology ◽  
Corrosion Behaviour ◽  
High Strength ◽  
Corrosion Resistant ◽  
X Ray ◽  
Scanning Electron

In this study, alternatives to corrosion-resistant cadmium coatings on high strength steel fasteners are explored. Nanocrystalline Zn-Ni and Zn-Ni-Co electrodeposits, synthesized by electrochemical deposition, were analyzed by potentiodynamic polarization in a 1M NaCl aqueous solution, to determine the corrosion behaviour of the alloys. Sample coatings were characterized using scanning electron microscopy to examine differences in surface morphology that can affect corrosion resistance. Energy dispersive x-ray spectroscopy was used to relate composition to corrosion resistance and to characterize the corrosion behavior during polarization. All coatings showed corrosion potentials at equivalent, or lower values than that of cadmium, suggesting that both alloys are viable as cadmium replacements. Specific compositions showed slightly passivating regions, but the brittle film formed during polarization is unstable. Comparatively, Zn-Ni shows a better resistance to corrosion than Zn-Ni-Co. The effect of composition on the corrosion resistance can be explained on the basis of the sacrificial depletion of Zn over Ni.

Study on Morphologies of Palladium Coated Foam Nickel Cathodes for Dechlorination of 2,4-Dichlorophenol

2012 ◽  
Vol 571 ◽  
pp. 97-101 ◽  
Author(s):  
Jun Jing Li ◽  
Hui Ling Liu ◽  
Zhi Wei Wang ◽  
Xiu Wen Cheng
Keyword(s):  
Electron Microscopy ◽  
Aqueous Solution ◽  
Composite Electrode ◽  
Potential Temperature ◽  
Nickel Electrode ◽  
Polymerization Time ◽  
Applied Potential ◽  
Polypyrrole Films ◽  
Polypyrrole Film ◽  
Scanning Electron

Electrolytically deposited palladium on polypyrrole film, which is electropolymerized using potentiostatic method, covered foam nickel electrode as a support was used as cathode for the electrocatalytic hydrodechlorination of 2, 4-dichlorophenol in aqueous solution. It is well known that the morphologies of polypyrrole films have dramatic influences on the dispersion of metals and the performance of the composite electrode. The influence of applied potential, temperature and polymerization time on the morphology of the films was studied by scanning electron microscopy (SEM). The fundamental electrocatalytic hydrodechlorination (ECH) results indicated that the electrocatalytic activity of Pd loaded polypyrrole foam nickel electrode is excellent for dechlorination of 2,4-dichlorophenol. The present study shows a promising choice of this kind of composite electrode for ECH.

Influence of Fly Ash on Corrosion Resistance of Refractory Forsterite-Spinel Ceramics

2021 ◽  
Vol 325 ◽  
pp. 181-187
Author(s):  
Martin Nguyen ◽  
Radomír Sokolář
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Corrosion Resistance ◽  
Fly Ash ◽  
Raw Materials ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transition Zones ◽  
Refractory Ceramics ◽  
Scanning Electron

This article examines the influence of fly ash on corrosion resistance of refractory forsterite-spinel ceramics by molten iron as a corrosive medium. Fly ash in comparison with alumina were used as raw materials and sources of aluminium oxide for synthesis of forsterite-spinel refractory ceramics. Raw materials were milled, mixed in different ratios into two sets of mixtures and sintered at 1550°C for 2 hours. Samples were characterized by X-ray diffraction analysis and thermal dilatometric analysis. Crucibles were then made from the fired ceramic mixtures and fired together with iron at its melting point of 1535°C for 5 hours. The corrosion resistance was evaluated by scanning electron microscopy on the transition zones between iron and ceramics. Mixtures with increased amount of spinel had higher corrosion resistance and mixtures with fly ash were comparable to mixtures with alumina in terms of corrosion resistance and refractory properties.

scholarly journals Preparation, Characterization, and Photocatalytic Properties of Modified Red Mud

2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Mingjie Ma ◽  
Guanyu Wang ◽  
Zhengpeng Yang ◽  
Shanxiu Huang ◽  
Weijie Guo ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Aqueous Solution ◽  
Scanning Electron Microscopy ◽  
Uv Irradiation ◽  
Red Mud ◽  
Structure Property ◽  
X Ray Diffraction ◽  
X Ray ◽  
Xrf Scanning ◽  
Scanning Electron

Solid waste red mud was modified by HCl leaching. The structure property and composition of modified red mud were investigated by X-ray diffraction (XRD), X-ray fluorescence spectroscopy (XRF), scanning electron microscopy (SEM), and Brunauer-Emmett-Teller (BET). Under UV irradiation, methyl orange (MO) aqueous solution was photodegraded by modified red mud. The obtained results showed that the specific surface area of modified red mud was 317.14 m2/g, which was about 40 times higher than that of the normal red mud. After UV irradiation for 50 min, the removal percentage of MO reached 94.2%. The study provided a novel way for the application of red mud to the photocatalytic degradation of organic wastes.

OB-IV-1Exocrine Organs Imaged in Aqueous Solution by Atmospheric Scanning Electron Microscopy (ASEM)

Microscopy ◽  
2016 ◽  
Vol 65 (suppl 1) ◽  
pp. i17.1-i17
Author(s):  
Toshiko Yamazawa ◽  
Naotoshi Nakamura ◽  
Yoshinori Mikami ◽  
Hiroshi Sekiya ◽  
Mari Sato ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Aqueous Solution ◽  
Scanning Electron Microscopy ◽  
Scanning Electron

Properties and Synthesis of Kaolin / Potassium Polyacrylate / Acrylamide Composite Superabsorbent Resin

2011 ◽  
Vol 287-290 ◽  
pp. 1331-1334
Author(s):  
Hao Ren ◽  
Jie Li ◽  
Yu Fen Zhang ◽  
Tai Zhong Huang
Keyword(s):  
Aqueous Solution ◽  
Saline Water ◽  
Monomer Concentration ◽  
Water Absorbency ◽  
Solution Polymerization ◽  
Synthetic Resin ◽  
Polymer Molecules ◽  
Aqueous Solution Polymerization ◽  
Crosslinker Concentration ◽  
Superabsorbent Resin

The aqueous solution polymerization methods were used for the synthesis of superabsorbent resin. The effects of different experimental factors on synthetic resin water absorbency were investigated in this paper. The variables examined in this study included monomer concentration, neutralization degree, initiator and crosslinker concentration, reaction temperature and time, etc. The maximum absorbencies of distilled and 0.9% saline water are 919 times and 92 times respectively under optimum condition. Analysis from FTIR and SEM shown the polymer molecules can be firmly fixed with kaolin, the bonding of kaolin and polymer is good in CSR.

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