Graphene Based Ultrahin Composite Films Prepared by Layer-by-Layer Electrostatic Assembly and Spinning Coating

2012 ◽  
Vol 430-432 ◽  
pp. 79-82
Author(s):  
Yong Qiang He ◽  
Si Yao He ◽  
Qiao Juan Gong ◽  
Jian Ping Gao ◽  
Xiao Dong Wang
Keyword(s):  
Thin Films ◽  
Graphene Oxide ◽  
Polyvinyl Alcohol ◽  
Composite Films ◽  
Layer By Layer ◽  
Visible Absorption ◽  
Electrostatic Assembly ◽  
Potential Applications ◽  
Coating Methods ◽  
Electrochemical Devices

Ultra thin graphene oxide (GO)/polyvinyl alcohol and graphene-polyvinyl alcohol/gelatin composite films were fabricated by electrostatic layer-by-layer assembly and spinning coating methods. The assembling and coating process were traced with UV-visible absorption spectroscopy and the morphology of the formed ultra thin films was observed under scanning electron microscopy. The results show that the adsorption value of the GO based composite films linearly increased as the number of layers increased. The ultra thin graphene oxide/polyvinyl alcohol and graphene-polyvinyl alcohol/gelatin composite films have layered structure with high tensile strength because of the incorporation of GO. These strong ultra thin films have potential applications in coating, sensor and electrochemical devices.

scholarly journals Introduction of Chalcogenide Glasses to Additive Manufacturing: Nanoparticle Ink Formulation, Inkjet Printing, and Phase Change Devices Fabrication

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
A. Ahmed Simon ◽  
B. Badamchi ◽  
H. Subbaraman ◽  
Y. Sakaguchi ◽  
L. Jones ◽  
...  
Keyword(s):  
Thin Films ◽  
Phase Change ◽  
Inkjet Printing ◽  
Chalcogenide Glasses ◽  
Dip Coating ◽  
Potential Applications ◽  
Coating Methods ◽  
Report Data ◽  
Nanoparticle Ink ◽  
Ink Formulation

AbstractChalcogenide glasses are one of the most versatile materials that have been widely researched because of their flexible optical, chemical, electronic, and phase change properties. Their application is usually in the form of thin films, which work as active layers in sensors and memory devices. In this work, we investigate the formulation of nanoparticle ink of Ge–Se chalcogenide glasses and its potential applications. The process steps reported in this work describe nanoparticle ink formulation from chalcogenide glasses, its application via inkjet printing and dip-coating methods and sintering to manufacture phase change devices. We report data regarding nanoparticle production by ball milling and ultrasonication along with the essential characteristics of the formed inks, like contact angle and viscosity. The printed chalcogenide glass films were characterized by Raman spectroscopy, X-ray diffraction, energy dispersive spectroscopy and atomic force microscopy. The printed films exhibited similar compositional, structural, electronic and optical properties as the thermally evaporated thin films. The crystallization processes of the printed films are discussed compared to those obtained by vacuum thermal deposition. We demonstrate the formation of printed thin films using nanoparticle inks, low-temperature sintering and proof for the first time, their application in electronic and photonic temperature sensors utilizing their phase change property. This work adds chalcogenide glasses to the list of inkjet printable materials, thus offering an easy way to form arbitrary device structures for optical and electronic applications.

Photocatalytic Degradation of Humic Acid Using Fe3+ and N-Doped 3SnO2/TiO2 Thin Films Coated on Glass Fibers

2014 ◽  
Vol 608 ◽  
pp. 164-169
Author(s):  
Peerawas Kongsong ◽  
Lek Sikong ◽  
Sutham Niyomwas ◽  
Vishnu Rachpech
Keyword(s):  
Thin Films ◽  
Photocatalytic Activity ◽  
Humic Acid ◽  
Glass Fibers ◽  
Sol Gel ◽  
Composite Films ◽  
Dip Coating ◽  
High Photocatalytic Activity ◽  
Coating Methods ◽  
Uv Lamp

The Fe3+ and N–doped 3SnO2/TiO2 composite thin films and undoped films coated on glass fibers were prepared by sol–gel and dip–coating methods. The films were calcined at 600°C for 2 hour and characterized by XRD, SEM, EDS and XPS. The photocatalytic activity of the coated glass fibers was determined by means of degradation of a methylene blue (MB) solution and humic acid (HA). It was found that the optimized 20N/3SnO2/TiO2composite films exhibit a high photocatalytic activity and HA could be rapidly removed from water. The main factor affecting the HA degradation of 20N/3SnO2/TiO2 films is quantity of glass fibers loading, irradiation power of UV lamp and flow rate of water.

scholarly journals Graphene Oxide Reinforced Polycarbonate Nanocomposite Films with Antibacterial Properties

2016 ◽  
Vol 2016 ◽  
pp. 1-10 ◽  
Author(s):  
R. Mahendran ◽  
D. Sridharan ◽  
K. Santhakumar ◽  
T. A. Selvakumar ◽  
P. Rajasekar ◽  
...  
Keyword(s):  
Thin Films ◽  
Graphene Oxide ◽  
Low Cost ◽  
Thermal Studies ◽  
Composite Films ◽  
Antibacterial Properties ◽  
Antibacterial Activities ◽  
Nanocomposite Films ◽  
Matrix Microstructure ◽  
Phase Inversion Technique

The incorporation of carbonaceous nanofillers into polymers can result in significant materials with improved physicochemical properties and novel composite functionalities. In this study, we have fabricated antibacterial, lightweight, transparent, and flexible graphene oxide (GO) reinforced polycarbonate thin films by a facile and low-cost methodology. Solution blending is employed to get a homogeneous mixture of PC-GO composites at various loading of GO, and the thin films are prepared by dry-wet phase inversion technique. Thermal studies and micrographs of the films revealed the incorporation of GO in PC matrix. Microstructure of the thin films showed the homogeneous dispersion of GO at micro- and nanoscales; however, at higher loading of GO (0.7%), significant agglomeration is observed. More importantly, PC-GO composite films exhibited excellent antibacterial activities against E. coli and S. aureus, owing to the antibacterial nature of GO nanoparticles.

scholarly journals Laser Ablation Ceramic Target for 8YSZ High-k Dielectric Electrolyte thin Films Precessed by PLD on Si(100) and Pt/Si(111)

2020 ◽  
Vol 71 (7) ◽  
pp. 272-277
Author(s):  
Rovena Veronica Pascu
Keyword(s):  
Thin Films ◽  
X Ray Diffraction ◽  
Stabilized Zirconia ◽  
X Ray ◽  
Force Microscopy ◽  
Atomic Force ◽  
High K ◽  
Potential Applications ◽  
Electrochemical Devices ◽  
High K Dielectric

The cubic structure 8YSZ (8%Yttria-Stabilized Zirconia) thin films deposited by PLD(Pulsed Laser Deposition) on substrates Si (100) and Pt/Si (111) by identical control parameters have potential applications as electrolytes for planar micro electrochemical devices like Lambda oxygen sensors and IT-�SOFC. It appearance differences in polycrystalline structural and optical characterization by XRD (X-ray Diffraction), SEM (Scanning Electron Microscope), AFM (Atomic Force Microscopy) and V- VASE (Variable Angle Spectroscopic Ellipsometry. The differences are relating on crystalline dimensions, lattice parameters; surface roughness measured by V- VASE and AFM are presented synthetic to evidence the differences generated by substrates.

Bioinspired Layer-by-Layer Poly(vinyl alcohol) - Graphene Oxide Nanocomposites

2012 ◽  
Vol 1410 ◽  
Author(s):  
Charline Sellam ◽  
Zhi Zhai ◽  
Hediyeh Zahabi ◽  
Hua Deng ◽  
Emiliano Bilotti ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Vinyl Alcohol ◽  
Composite Films ◽  
Good Control ◽  
Layered Composite ◽  
Poly Vinyl Alcohol ◽  
Layer By Layer ◽  
Synergic Effect ◽  
Transparent Film ◽  
Spraying Method

ABSTRACTA bottom-up approach for poly(vinyl alcohol) (PVA) - graphene oxide (GO) nanocomposites using a spraying method is presented. Very simple and versatile, spraying allows to build-up uniform layered composite films with good control on the structure of each layer. 150 bi-layers were deposited to create a transparent film with improved mechanical properties at a loading of 5.4 wt.% GO. The Young’s modulus and strength of these films doubled or nearly doubled which is believed to be due to a synergic effect as a result of the nanoscale organization of the composite by the 2D nanofiller, and hydrogen bonding between the PVA and the GO.

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