Synthesis and Characterization of LiFePO4 Prepared by Sol-Gel Technique

LiFePO4 material was synthesized at 650°C in an N2 atmosphere using a sol-gel method. This material showed a well developed XRD pattern (orthorhombic structure, Pnma) without peaks at 2θ=41°, indicating the absence of FeP or metallic Fe2P impurities. The Li/LiFePO4 cell showed a high initial discharge capacity of more than 140mAh/g and no capacity decrease until the 50th cycle (>99.0%).

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Synthesis and characterization of new silica–titania mixed oxide in the presence of 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl) imide by sol–gel technique

Journal of Sol-Gel Science and Technology ◽

10.1007/s10971-014-3279-7 ◽

2014 ◽

Vol 70 (1) ◽

pp. 104-110 ◽

Cited By ~ 3

Author(s):

Tilagam Marimuthu ◽

Sharifah Mohamad ◽

Yatimah Alias

Keyword(s):

Mixed Oxide ◽

Sol Gel ◽

Synthesis And Characterization ◽

Gel Technique

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Synthesis and characterization of polyimide/silica hybrid waveguide materials via sol-gel technique

10.1117/12.569902 ◽

2005 ◽

Author(s):

Fengxian Qiu ◽

Yuming Zhou ◽

Juzheng Liu ◽

Xuping Zhang

Keyword(s):

Sol Gel ◽

Synthesis And Characterization ◽

Gel Technique ◽

Hybrid Waveguide ◽

Silica Hybrid

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Synthesis and characterization of nickel oxide nanoparticles by sol-gel technique

10.1063/5.0009740 ◽

2020 ◽

Author(s):

Infantiya Stephen Grace ◽

J. Vinola ◽

Shubramaniyan Deepapriya ◽

David Rodney John ◽

A. Aslinjensipriya ◽

...

Keyword(s):

Nickel Oxide ◽

Sol Gel ◽

Synthesis And Characterization ◽

Oxide Nanoparticles ◽

Nickel Oxide Nanoparticles ◽

Gel Technique

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Improved electrochemical properties of (1 − x)LiFePO4·xLi3V2(PO4)3/C composites prepared by a novel sol–gel method

New Journal of Chemistry ◽

10.1039/c5nj01328c ◽

2015 ◽

Vol 39 (11) ◽

pp. 8971-8977 ◽

Cited By ~ 8

Author(s):

Yuanchang Si ◽

Zhi Su ◽

Yingbo Wang ◽

Ting Ma ◽

Juan Ding

Keyword(s):

Electrochemical Properties ◽

Discharge Capacity ◽

Sol Gel ◽

Initial Discharge Capacity ◽

Gel Method ◽

Sol Gel Method ◽

Initial Discharge

0.8LiFePO4·0.2Li3V2(PO4)3/C composites were synthesized by a new sol–gel method, which delivered an initial discharge capacity of 158.7 mA h g−1 at 0.1C.

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Synthesis and Characterization of Fluoro- and Chloro-bimetallic Alkoxides as Precursors for Luminescent Metal Oxide Materials via Sol-Gel Technique

Chinese Journal of Chemistry ◽

10.1002/cjoc.200790194 ◽

2007 ◽

Vol 25 (7) ◽

pp. 998-1004 ◽

Cited By ~ 6

Author(s):

Taimur Athar ◽

Sang Il Seok ◽

Jeong Oh Kwon

Keyword(s):

Metal Oxide ◽

Sol Gel ◽

Synthesis And Characterization ◽

Oxide Materials ◽

Gel Technique ◽

Bimetallic Alkoxides

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Synthesis and Characterization of Nano Mn3O4 for Lithium-Ion Batteries

Applied Mechanics and Materials ◽

10.4028/www.scientific.net/amm.687-691.4331 ◽

2014 ◽

Vol 687-691 ◽

pp. 4331-4334

Author(s):

Han Ping Zhu ◽

Peng Ding ◽

Song Fang ◽

Hailin Liu

Keyword(s):

Discharge Capacity ◽

Current Density ◽

Solvothermal Method ◽

Lithium Ion ◽

Constant Current ◽

Initial Discharge Capacity ◽

Initial Discharge ◽

Structure Morphology ◽

Specific Discharge

nanoMn3O4was prepared by a simple solvothermal method. The structure, morphology and electrochemical properties of the products were investigated by XRD, SEM and constant current discharge-charge test. The results of XRD and SEM shows that nanoMn3O4is high-purity, and it’s diameter is about 30 nm. It could deliver an initial discharge capacity of 1324.4 mAh g-1at the current density of 25.5 mA g-1, and the specific discharge capacity is 586.9 mAh g-1after 30 cycles at the current density of 30.4 mA g-1.

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Synthesis and characterization of zinc titanate nano-crystal powders by sol–gel technique

Journal of Crystal Growth ◽

10.1016/s0022-0248(02)01490-2 ◽

2002 ◽

Vol 243 (2) ◽

pp. 319-326 ◽

Cited By ~ 109

Author(s):

Yee-Shin Chang ◽

Yen-Hwei Chang ◽

In-Gann Chen ◽

Guo-Ju Chen ◽

Yin-Lai Chai

Keyword(s):

Sol Gel ◽

Synthesis And Characterization ◽

Zinc Titanate ◽

Gel Technique ◽

Nano Crystal

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Preparation and Electrochemical Properties of LiMnPO4 Nanoparticles by Polyol Method

Key Engineering Materials ◽

10.4028/www.scientific.net/kem.566.95 ◽

2013 ◽

Vol 566 ◽

pp. 95-98 ◽

Cited By ~ 1

Author(s):

Takayuki Kodera ◽

Fuminari Isobe ◽

Takashi Ogihara

Keyword(s):

Physical Properties ◽

Electrochemical Properties ◽

Discharge Capacity ◽

Polyol Method ◽

Initial Discharge Capacity ◽

Xrd Pattern ◽

Initial Discharge ◽

Olivine Structure ◽

First Discharge Capacity ◽

Good Agreement

Plate-like LiMnPO4particles were prepared by polyol method. The chemical and physical properties of plate-like LiMnPO4particles were characterized by XRD and SEM. The thickness of plate-like LiMnPO4particles was approximately 35 nm. XRD pattern of plate-like LiMnPO4was good agreement with orthorhombic olivine structure. The first discharge capacity of C/LiMnPO4cathode was approximately 95 mAh/g. 99.9 % of initial discharge capacity was maintained after 100 cycles.

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