Role of Debinding to Control Mechanical Properties of Powder Injection Molded 316L Stainless Steel

2013 ◽  
Vol 699 ◽  
pp. 875-882 ◽  
Author(s):  
Muhammad Rafi Raza ◽  
Faiz Ahmad ◽  
M.A. Omar ◽  
R.M. German ◽  
Ali S. Muhsan

316L stainless steel is widely used in various industries due to low cost, ease of availability and exceptional combination of mechanical properties along with corrosion resistance as compared to the other available metal alloys. In powder injection molding, debinding is very critical step and improper debinding can change the final properties dramatically. In the present study, affects of debinding on mechanical properties of powder injection molded 316L stainless steel were studied. The prepared feedstocks were molded according to MPIF 50 standard using vertical injection molding machine (KSA100). The plastic binder was removed at 450°C from the molded test samples using two different furnaces i.e. commercial and laboratory furnace followed by the sintering in vacuum, hydrogen, mixture of H2 and N2 (9:1) and nitrogen at 1325°C for 2hr with post sintering cooling rate 3°C/min . Test samples debound in commercially available furnace showed 97% densification and higher mechanical properties. The corrosion resistance was reduced due to presence of residual carbon during thermal debinding. The presence of carbon and formation of carbides and nitrides were confirmed by XRD and microstructural analysis. The results showed that the test samples debound in commercial furnace showed brittle behavior due to the presence of carbides and nitrides. Test samples sintered in N2 showed 96.3% density and tensile strength 751MPa. This value of strength is twice as compared to the sample debound in laboratory furnace followed by the sintering in vacuum. The achieved mechanical properties in vacuum sintered samples were comparable to the wrought 316L stainless steel (according to ASTM standard).

2007 ◽  
Vol 26-28 ◽  
pp. 355-358
Author(s):  
Chang Kyu Kim ◽  
Chang Young Son ◽  
Dae Jin Ha ◽  
Tae Sik Yoon ◽  
Sung Hak Lee

Powder injection molding (PIM) process was applied to Fe-based metamorphic alloy powders, and microstructure, hardness, and wear resistance of the PIM products were analyzed and compared with those of conventional PIM stainless steel products. When Fe-based metamorphic powders were injection-molded and then sintered at 1200 oC, completely densified products with almost no pores were obtained. They contained 34 vol.% of (Cr,Fe)2B borides dispersed in the austenitic matrix without amorphous phases. Since these (Cr,Fe)2B borides were very hard and thermally stable, hardness, and wear resistance of the PIM products of Fe-based metamorphic powders were twice as high as those of conventional PIM stainless steel products. Such property improvement suggested new applicability of the PIM products of Fe-based metamorphic powders to structures and parts requiring excellent mechanical properties.


2012 ◽  
Vol 185 ◽  
pp. 102-105
Author(s):  
Muhammad Rafi Raza Malik ◽  
Faiz Ahmad ◽  
Othman Mamat ◽  
Mohd Afian Omar ◽  
R.M. German ◽  
...  

This research presents the effects of temperature and cooling rate on mechanical properties of powder injection molded 316L Stainless steel. Steel powder and binder were mixed together to produce the feedstock. The green samples were produced by injection molding and debinded. Brown test samples were sintered in vacuum at 1325°C, 1360°C and 1380°C for 2h with two heating and cooling rates 5°C/min and 10°C/ min. The test samples sintered at 1325°C achieved maximum sintered density. The higher cooling rate improved the strength of the sintered test samples. The maximum sintered density of 96% and tensile strength of 503MPa was achieved and these results are comparable to the wrought 316L stainless steel (according to ASTM standard).


2016 ◽  
Vol 1133 ◽  
pp. 324-328 ◽  
Author(s):  
Muhammad Aslam ◽  
Faiz Ahmad ◽  
P.S.M. Bm-Yousoff ◽  
Khurram Altaf ◽  
Afian Omar ◽  
...  

Optimization of solvent debinding process parameters for powder injection molded 316L stainless steel (SS) has been reported in this research work. Powder gas atomized (PGA) 316L SS was blended with a multicomponent binder in Z-blade mixer at 170°C ± 5°C for 90 minutes. Feedstock was successfully injected at temperature 170 ± 5°C. Injection molded samples were immersed in n-heptane for 2h, 4h, 6h and 8h at temperatures 50°C ,55°C and 60°C to extract the soluble binder components. Scanning electron microscope (SEM) results attested that soluble binder components were completely extracted from injection molded samples at temperature 55°C after 6h.


2011 ◽  
Vol 11 (11) ◽  
pp. 2042-2047 ◽  
Author(s):  
Muhammad Rafi Raza ◽  
Faiz Ahmad ◽  
M.A. Omar ◽  
R.M. German

Polymers ◽  
2020 ◽  
Vol 12 (6) ◽  
pp. 1296
Author(s):  
Berenika Hausnerova ◽  
Martin Novak

In this study, environmentally convenient highly metal powder filled feedstocks intended for powder injection molding is presented. The composition of 60 vol % 316L stainless steel gas atomized powder feedstocks containing semicrystalline waxes: acrawax or carnauba wax and paraffin wax, combined with polyethylene glycol and modifier, was optimized to provide defect-free parts. Rheological as well as thermogravimetric analyses supported with scanning electron microscopy and metallography were employed to set up optimum conditions for molding, debinding and sintering. The performance of the novel feedstock was compared with currently available polyolefines-based materials, and results showed an efficiency enhancement due to the substantially lower (about 100 °C) mixing and molding temperatures as well as a reduction of debinding and sintering times at the simultaneous achievement of better mechanical properties in terms of elongation and tensile strength, in comparison to the mass production feedstock.


2005 ◽  
Vol 498-499 ◽  
pp. 86-92 ◽  
Author(s):  
Isolda Costa ◽  
Sizue Ota Rogero ◽  
Olandir Vercino Correa ◽  
Clarice Terui Kunioshi ◽  
Mitiko Saiki

This study investigates the in vitro corrosion and cytotoxicity response of AISI 316L stainless steel produced by powder injection molding (PIM) technology in a solution that simulates physiological fluids (MEM) by electrochemical techniques and neutral red uptake cytotoxicity assay. The results were compared with those of AISI 316L produced by conventional metallurgy. Both steels showed high corrosion resistance and no toxic effect in the cytotoxicity test. The corrosion products were analyzed by instrumental neutron activation analysis (INAA). The surfaces of the alloys were evaluated before and after corrosion test by scanning electron microscopy and a passive behaviour was indicated supporting the results from other techniques.


2005 ◽  
Vol 54 (3) ◽  
pp. 230-238 ◽  
Author(s):  
L. Liu ◽  
N.H. Loh ◽  
B.Y. Tay ◽  
S.B. Tor ◽  
Y. Murakoshi ◽  
...  

2003 ◽  
Vol 43 (1) ◽  
pp. 119-126 ◽  
Author(s):  
Tae Shik Yoon ◽  
You Hwan Lee ◽  
Sang Ho Ahn ◽  
Jung Hwan Lee ◽  
Chong Soo Lee

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