Behavior of Heavy Plastic Deformation of Cu-15Cr-0.1Zr In Situ Composite

2009 ◽  
Vol 79-82 ◽  
pp. 2191-2194
Author(s):  
Yan Li ◽  
Xiao Hong Chen ◽  
Ping Liu ◽  
Lin Hua Gao ◽  
Bao Hong Tian
Keyword(s):  
Electron Microscopy ◽  
Plastic Deformation ◽  
Cold Drawing ◽  
Degree Of Deformation ◽  
Transmission Electron ◽  
Fibrous Morphology ◽  
Two Phases ◽  
Relationship Of ◽  
The Relationship

The behavior of plastic deformation of Cu-15Cr-0.1Zr in-situ composite under different degree of cold drawing deformation was analyzed by using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results show that both Cu and Cr phases are elongated along cold drawn direction and appear a fibrous morphology; However, Cu phase shows a thread-like fibrous morphology and Cr phase shows a band-like fibrous morphology. The two phases have a coherent relationship of (111)Cu //(011)Cr; When the degree of deformation(ε)is equal to 6.43, the relationship shows// [111]Cu // [110]Cr //cold drawn direction. Furthermore, forming two different morphologies of Cu and Cr phases during cold drawing is also analyzed.

Silica and Silane Coupling Agent for in Situ Reinforcement of Acrylonitrile-Butadiene Rubber

1999 ◽  
Vol 72 (1) ◽  
pp. 119-129 ◽  
Author(s):  
K. Murakami ◽  
S. Osanai ◽  
M. Shigekuni ◽  
S. Iio ◽  
H. Tanahashi ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Sol Gel ◽  
Silica Particles ◽  
Butadiene Rubber ◽  
Acrylonitrile Butadiene Rubber ◽  
In Situ Silica ◽  
Transmission Electron ◽  
Dispersion Agent ◽  
The Relationship

Abstract In situ silica reinforcement for the acrylonitrile-butadiene rubber (NBR) vulcanizates, which were premixed with a conventional silica (VN-3) and γ-mercaptopropyltrimethoxysilane (γ-MPS), was achieved by the sol-gel reaction of tetraethoxysilane (TEOS) using ethylenediamine. It was observed that the reinforcement efficiency tended to increase with the increase of mechanically premixed conventional silica. From the observations of transmission electron microscopy and scanning electron microscopy, the simultaneous use of VN-3 and γ-MPS was found to promote the formation of large silica particles and clusters with a relatively good dispersion by the sol-gel reaction of TEOS in the NBR vulcanizate. The results of hysteresis measurements supported this promotion. It was considered to be due to the surface modification of VN-3 by the sol-gel reaction of TEOS and the presence of γ-MPS which worked as a dispersion agent for silica particles. The relationship between the mechanical properties and the morphology of the in situ silica filled vulcanizates is discussed.

Crystalline and microstructure study of the AlN–Al2O3section in the Al–N–O system. II. φ′- and δ-AlON spinel phases

1999 ◽  
Vol 32 (2) ◽  
pp. 253-272 ◽  
Author(s):  
P. Tabary ◽  
C. Servant
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Structural Model ◽  
Spinel Phase ◽  
X Ray Diffraction ◽  
Transmission Electron ◽  
Spinel Phases ◽  
Two Phases ◽  
Microscopy Techniques ◽  
The Relationship

Results from the crystalline and microstructure study of the φ′- and δ-AlON spinel phases by X-ray diffraction, neutron diffraction and standard-resolution transmission electron microscopy techniques are reported. Several samples having different compositions in mol % AlN were considered. A structural model is proposed to account for the double modulation of composition and displacement of the cations and anions, which has been determined for these two phases and for the relationship with the γ-AlON spinel phase. Some high-resolution transmission electron microscopy experiments have confirmed the present structural model. A discussion with reference to previous data is presented.

Behaviors of TiN Nanoparticles in Mn18Cr2 Steel

2011 ◽  
Vol 117-119 ◽  
pp. 897-900
Author(s):  
Yan Li ◽  
Jing Pei Xie ◽  
Hui Wu Yu ◽  
Wen Yan Wang ◽  
Xin Hai Shao ◽  
...  
Keyword(s):  
Manganese Steel ◽  
High Manganese Steel ◽  
Tin Nanoparticles ◽  
Transmission Electron ◽  
Ε Martensite ◽  
Two Phases ◽  
Relationship Of ◽  
Existing Form ◽  
The Relationship

Mn18Cr2 steel is one of austenitic deformation strengthening steel. The existing form of TiN and its influence on the austenitic structure in the steel by adding small amounts of TiN nanoparticles are discussed in this study, which may provide some advices to explore new way to strengthen high manganese steel. The microstructures of Mn18Cr2 steel added small amounts of TiN nanoparticles are observed by Transmission Electron Microscopy (TEM). The results show that TiN nanoparticles exist in austenite and there have a very good match interface between the two phases, the crystal face relationship are {220}γ//{220}N, {422}γ//{422}N, (111)γ //(200)N , orientation relationship are <110>γ// <110>N, <211>γ//<211>N, [112]γ // [011]N, moreover, the relationship of (111)γ and (200)N is not only parallel but also coherent. Meanwhile, there are many high density dislocations, a small amount of stacking faults, twins and ε-martensite in the austenite due to the role of TiN nanoparticles.

Epitaxial Growth and Stability of C49 TiSi2 ON Si(111).

1990 ◽  
Vol 198 ◽  
Author(s):  
Hyeongtag Jeon ◽  
J. W. Honeycutt ◽  
C. A. Sukow ◽  
T. P. Humphreys ◽  
R. J. Nemanich ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Electron Diffraction ◽  
Metastable Phase ◽  
Plan View ◽  
Transmission Electron ◽  
Temperature Deposition ◽  
The Individual ◽  
Relationship Of

ABSTRACTEpitaxial TiSi2 films have been grown by molecular beam epitaxy (MBE) on atomically clean Si(111)-orientated substrates. The growth procedure involves the ambient temperature deposition of Ti films of 50Å thickness and annealing to 800°C. In situ low energy electron diffraction (LEED) and Auger electron spectroscopy (AES) techniques have been used to monitor the TiSi2 formation process. The epitaxial films have been identified as the C49 metastable phase by both Raman spectroscopy and electron diffraction. Plan view transmission electron microscopy shows three different connected island morphologies. The individual island structures are single crystal and are grown epitaxially with different crystallographic orientations. The orientational relationship of the largest islands is given by [3 1 1] C49 TiSi2//[112]Si and (130) C49 TiSi2//(l1 1)Si. High resolution transmission electron microscopy (HRTEM) cross-section shows a coherent interface extending over several hundred angstroms.

Epitaxial Gold in Au/Si Eutectic Reaction and Epitaxial Aluminum Spikes in Al-1%Si/Ti-W/Si System

1988 ◽  
Vol 116 ◽  
Author(s):  
Peng-Heng Chang
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Epitaxial Growth ◽  
Orientation Relationship ◽  
Gold Film ◽  
Eutectic Reaction ◽  
Orientation Relationships ◽  
Transmission Electron ◽  
Relationship Of ◽  
The Relationship

AbstractEpitaxial regrowth of gold film on Si as a result of Au/Si eutectic reaction and epitaxial aluminum spikes forming at IC contacts during sintering have been investigated by transmission electron microscopy (TEM). For gold film on Si, three types of epitaxy were observed: (1) the crystal structures of the two lattices are exactly the same, (2) the two structures have the orientation relationship of Au(111)//Si(111) and Au[132]//Si[231] and (3) 20° misorientation from the relationship in (2). Two orientation relationships were observed in the case of Al spike in Si: (1) Al[011]//Si[123] and Al(200)//Si(11), (2) Al[001]//Si[112] and 2° misorientation between Al(200) and Si(111). Possible mechanisms are proposed to explained the observed epitaxial growth.

Fine structure of mistletoe pollen. I. Eremolepidaceae, Lepidoceras, and Tupeia

1978 ◽  
Vol 56 (22) ◽  
pp. 2853-2864 ◽  
Author(s):  
Sylvia Feuer ◽  
Job Kuijt
Keyword(s):  
Electron Microscopy ◽  
Pollen Morphology ◽  
Spherical Shape ◽  
Oblate Spheroidal ◽  
Transmission Electron ◽  
Pollen Characters ◽  
The Family ◽  
Close Relationship ◽  
Relationship Of ◽  
The Relationship

An examination of pollen morphology and ultrastructure of Eremolepidaceae (Antidaphne, Ixidium, Eremolepis, Eubrachion) and Lepidoceras by light and scanning and transmission electron microscopy reveals a close relationship among the taxa. Pollen of Eremolepidaceae is typically echinate, tricolporate, and oblate-spheroidal. Eubrachion is unique within the family, exhibiting shallowly reticulate pollen. Ultrastructurally, all Eremolepidaceae exhibit a similar exine structure. The sculptural ektexinous elements (spines or 'muri') are never contiguous with the basal ektexine but rest on a thin granular zone. Pollen characters of Lepidoceras are particularly close to those of Ixidium and Eremolepis. The porate (por(or)ate) aperture type, completely spherical shape, and reduced granular ektexine of Lepidoceras pollen indicate an advanced position within the complex. The relationship of Tupeia to Eremolepidaceae is more obscure as pollen of the genus exhibits both eremolepidaceous (echinate sculpturing, shape in polar and equatorial views) as well as loranthaceous characters (simple apertures, ektexine organization). Palynologically Eremolepidaceae and related genera show no particular close relationship to Olacaceae or Santalaceae. Though Eremolepidaceae et al. do share a number of pollen features with Viscaceae (echinate sculpturing, compound apertures, exine organization) the strong nonpalynological differences between the two families suggest that these pollen features may have arisen independently.

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