Low-Frequency High-Temperature Internal Friction in Ti-13Nb-13Zr Alloy

2006 ◽  
Vol 319 ◽  
pp. 103-108
Author(s):  
Terlize Cristina Niemeyer ◽  
Carlos Roberto Grandini ◽  
Sandra G. Schneider

Recent studies have been done to achieve biomedical alloys containing non-toxic elements and presenting low elastic moduli. It has been reported that Ti-Nb-Zr alloys rich in beta phase, especially Ti-13Nb-13Zr, have potential characteristics for substituting conventional materials such as Ti-6Al-4V, stainless steel and Co alloys. The aim of this work is to study the internal friction (IF) of Ti-13Nb-13Zr (TNZ) alloy due to the importance of the absorption impacts in orthopedic applications. The internal friction of this alloy produced by arc melting was measured using an inverted torsion pendulum with the free decay method. The measurements were performed from 77 to 700 K with heating rate of 1 K/min, in a vacuum better than 10-5 mBar. The results show a relaxation structure at high temperature strongly dependent on microstructure of the material. Qualitative discussions are presented for the experimental results, and the possibility of using the TNZ as a high damping material is briefly mentioned.

2012 ◽  
Vol 535-537 ◽  
pp. 1027-1030
Author(s):  
Xiao Hui Cao ◽  
Yu Wang

By using a low frequency inverted torsion pendulum, the high temperature internal friction spectra of Al-0.02wt%Zr and Al-0.1wt%Zr alloys were investigated respectively. In Al-0.02wt%Zr alloy, the conventional grain boundary internal friction peak (Pg) is observed with some small unstable peaks. In Al-0.1wt%Zr alloy, the bamboo peak is observed to appear at the high temperature side of the conventional grain boundary internal friction peak. The conventional grain boundary internal friction peak decreased and moved to higher temperature. The bamboo peak owns an activation energy of 1.75eV. When average grain size exceeded the diameter of samples, Pb strength was reduced and its position was shifted to a lower temperature. Based on the grain boundary sliding model, Pg and Pb peaks were explained. Their dependence on annealing temperature and time was determined by considering the effects of contained Ce atoms and other impurities on the relaxation across grain boundary.


2015 ◽  
Vol 644 ◽  
pp. 171-174
Author(s):  
Dariusz Bochenek ◽  
Przemysław Niemiec ◽  
Radosław Zachariasz ◽  
Ryszard Skulski

Multicomponent PZT-type solid solution with composition: Pb0.975Ba0.01Ca0.01Sr0.005 (Zr0.52Ti0.48)O3+1.4wt.%Bi2O3+0.3wt.%GeO obtained by hot uniaxial pressing method is described in this paper. There are presented the results of studies of structural, dielectric and internal friction of obtained multicomponent PZT-type ceramics. It has been stated that the dielectric anomalies and internal friction anomalies are observed in similar temperature ranges. Obtained PZT-type ceramics have high value of the dielectric permittivity and low dielectric losses. The high temperature of phase transition and high value of electric permittivity allow considering this material as a base for low frequency and high temperature electromechanical transducers.


1978 ◽  
Vol 21 (85) ◽  
pp. 375-384 ◽  
Author(s):  
René Vassoille ◽  
Christian Maï ◽  
Joseph Perez

Abstract The inelastic behaviour of ice Ih single crystals has been investigated by an inverted torsional pendulum in the low-frequency range. Three features are distinguished: (i) a relaxation peak previously observed by several authors in the higher-frequency range, (ii) an internal friction increasing with temperature in the high-temperature range (230–273 K), (iii) within this high-temperature range, internal friction becomes amplitude dependent, and this dependence becomes greater the greater the temperature. In this case, the internal friction has been interpreted in terms of movements of dislocations. Hence, the experimental results are interpreted with a model of internal friction based on an empirical relation for the velocity of dislocations. This model of internal friction is in fair agreement with experimental data . It is possible then to get an estimate of dislocation density. Hence it is shown that internal friction experiments can be useful in the study of the plastic behaviour of ice single crystals.


2012 ◽  
Vol 78 ◽  
pp. 125-132 ◽  
Author(s):  
Vedamanickam Sampath ◽  
Prathap Chandran

Materials with high damping capacity for quelling noise and vibration in engineering structures have drawn increasing attention in recent times. Among the different materials that have been attempted so far, shape memory alloys (SMAs) have shown much promise since they exhibit much higher damping due to the occurrence of a thermoelastic martensitic transformation in them. Among the SMAs it is copper-based SMAs that have proved more attractive compared to Ni-Ti SMAs because of their lower cost, higher damping and better machining characteristics. In the present work, therefore, the damping properties of a Cu-Al-Mn-Zn alloy, a potential high damping material for high temperature turbomachinery rotor blades, are investigated. The internal friction was studied using a dynamic mechanical analyzer over a range of temperatures (25-300°C), frequencies (0.5-10Hz) and strain amplitudes (5×10-6 and 10-4). The analysis of the results reveals that the damping properties are more sensitive to variation in frequency and strain amplitude, pointing to the suitability of the material for the intended application. The results are presented and discussed in the paper.


2011 ◽  
Vol 197-198 ◽  
pp. 1573-1576
Author(s):  
Xiao Hui Cao ◽  
Shou Jing Wang

By using a low frequency inverted torsion pendulum, the high temperature internal friction spectra of Al-0.013wt%Ce alloy subjected to deformation at different tensile rates was measured, and three peaks, the conventional grain boundary peak (P1), the bamboo peak (P2) and the soild solution peak (P3) were found. Increases of annealing temperature and deformation rate make P1 and P2 lower with P1 shifting to higher temperature and P2 to lower temperature. P3 was only found in the as-received samples. The dependence of P1 and P2 on grain size indicates that the two peaks are originated from the grain boundary sliding, and P3 may be associated with the diffusion of Ce atoms or other impurities at grain boundaries.


1978 ◽  
Vol 21 (85) ◽  
pp. 375-384
Author(s):  
René Vassoille ◽  
Christian Maï ◽  
Joseph Perez

AbstractThe inelastic behaviour of ice Ih single crystals has been investigated by an inverted torsional pendulum in the low-frequency range. Three features are distinguished:(i) a relaxation peak previously observed by several authors in the higher-frequency range,(ii) an internal friction increasing with temperature in the high-temperature range (230–273 K),(iii) within this high-temperature range, internal friction becomes amplitude dependent, and this dependence becomes greater the greater the temperature.In this case, the internal friction has been interpreted in terms of movements of dislocations. Hence, the experimental results are interpreted with a model of internal friction based on an empirical relation for the velocity of dislocations. This model of internal friction is in fair agreement with experimental data . It is possible then to get an estimate of dislocation density. Hence it is shown that internal friction experiments can be useful in the study of the plastic behaviour of ice single crystals.


Author(s):  
A. Paulsen ◽  
H. Dumlu ◽  
D. Piorunek ◽  
D. Langenkämper ◽  
J. Frenzel ◽  
...  

AbstractTi75Ta25 high-temperature shape memory alloys exhibit a number of features which make it difficult to use them as spring actuators. These include the high melting point of Ta (close to 3000 °C), the affinity of Ti to oxygen which leads to the formation of brittle α-case layers and the tendency to precipitate the ω-phase, which suppresses the martensitic transformation. The present work represents a case study which shows how one can overcome these issues and manufacture high quality Ti75Ta25 tensile spring actuators. The work focusses on processing (arc melting, arc welding, wire drawing, surface treatments and actuator spring geometry setting) and on cyclic actuator testing. It is shown how one can minimize the detrimental effect of ω-phase formation and ensure stable high-temperature actuation by fast heating and cooling and by intermediate rejuvenation anneals. The results are discussed on the basis of fundamental Ti–Ta metallurgy and in the light of Ni–Ti spring actuator performance.


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