Ferroelectric Properties and Internal Friction in Doped PZT Ceramics

2015 ◽  
Vol 644 ◽  
pp. 171-174
Author(s):  
Dariusz Bochenek ◽  
Przemysław Niemiec ◽  
Radosław Zachariasz ◽  
Ryszard Skulski
Keyword(s):  
High Temperature ◽  
Internal Friction ◽  
Ferroelectric Properties ◽  
Low Frequency ◽  
Electric Permittivity ◽  
Pressing Method ◽  
Pzt Ceramics ◽  
Low Dielectric ◽  
Temperature Ranges ◽  
Similar Temperature

Multicomponent PZT-type solid solution with composition: Pb0.975Ba0.01Ca0.01Sr0.005 (Zr0.52Ti0.48)O3+1.4wt.%Bi2O3+0.3wt.%GeO obtained by hot uniaxial pressing method is described in this paper. There are presented the results of studies of structural, dielectric and internal friction of obtained multicomponent PZT-type ceramics. It has been stated that the dielectric anomalies and internal friction anomalies are observed in similar temperature ranges. Obtained PZT-type ceramics have high value of the dielectric permittivity and low dielectric losses. The high temperature of phase transition and high value of electric permittivity allow considering this material as a base for low frequency and high temperature electromechanical transducers.

scholarly journals The (1-x)BiFeO3-xBaTiO3-Bi(Zn0.5Ti0.5)O3 high temperature lead-free piezoelectric ceramics with strong piezoelectric properties

2021 ◽  
Author(s):  
Yuanyuan Sun ◽  
Huabin Yang ◽  
Jiwen Xu ◽  
Weiran Huang ◽  
Minhong Jiang ◽  
...  
Keyword(s):  
High Temperature ◽  
Curie Temperature ◽  
Piezoelectric Properties ◽  
Ferroelectric Properties ◽  
Temperature Fields ◽  
Depolarization Temperature ◽  
Ceramic Structure ◽  
Low Dielectric ◽  
Tan Δ ◽  
Piezoelectric Performance

Abstract The structure, microstructure, piezoelectric properties, ferroelectric properties and Curie temperature of (1- x )BiFeO 3 - x BaTiO 3 -Bi(Zn 0.5 Ti 0.5 )O 3 +MnO 2 +Li 2 CO 3 ceramics were investigated experimentally by improved solid-state reaction approach. The crystalline structures were examined by X-ray diffractometry. When x = 0.3, the rhombohedral and pseudocubic phases coexist in the ceramic structure. It is considered that the morphotropic phase boundary was formed here. At the same time, the piezoelectric performance d 33 , Curie temperature T C , and depolarization temperature are as high as 184 pC/N, 550°C, 530°C at x = 0.3, respectively. It is worth noting that when x = 0.24, the ceramics have a high T C = 580°C and low dielectric loss tan δ = 1.9%. These results show that the BFBT-BZT system ceramics are applicable ceramics with high piezoelectric properties in high temperature fields.

A Study on Influence of Annealing and Aging on High Temperature Internal Friction in Al-Zr Alloy

2012 ◽  
Vol 535-537 ◽  
pp. 1027-1030
Author(s):  
Xiao Hui Cao ◽  
Yu Wang
Keyword(s):  
High Temperature ◽  
Internal Friction ◽  
Grain Boundary ◽  
Low Frequency ◽  
Grain Boundary Sliding ◽  
High Temperature Side ◽  
Internal Friction Peak ◽  
Average Grain Size ◽  
Lower Temperature ◽  
Zr Alloy

By using a low frequency inverted torsion pendulum, the high temperature internal friction spectra of Al-0.02wt%Zr and Al-0.1wt%Zr alloys were investigated respectively. In Al-0.02wt%Zr alloy, the conventional grain boundary internal friction peak (Pg) is observed with some small unstable peaks. In Al-0.1wt%Zr alloy, the bamboo peak is observed to appear at the high temperature side of the conventional grain boundary internal friction peak. The conventional grain boundary internal friction peak decreased and moved to higher temperature. The bamboo peak owns an activation energy of 1.75eV. When average grain size exceeded the diameter of samples, Pb strength was reduced and its position was shifted to a lower temperature. Based on the grain boundary sliding model, Pg and Pb peaks were explained. Their dependence on annealing temperature and time was determined by considering the effects of contained Ce atoms and other impurities on the relaxation across grain boundary.

scholarly journals Internal Friction and Dynamic Modulus in Ultra-High Temperature Ru-Nb Functional Intermetallics / Tarcie Wewnętrzne I Moduł Dynamiczny W Bardzo Wysoko Temperaturowych Funkcjonalnych Związkach Międzymetalicznych Z Układu Ru-Nb

2015 ◽  
Vol 60 (4) ◽  
pp. 3069-3072
Author(s):  
M.L. Nó ◽  
L. Dirand ◽  
A. Denquin ◽  
J. San Juan
Keyword(s):  
High Temperature ◽  
Internal Friction ◽  
Martensitic Transformations ◽  
Time Dependent ◽  
Structural Defects ◽  
Complete Analysis ◽  
Internal Friction Peak ◽  
Thermally Activated ◽  
Temperature Ranges ◽  
Lower Temperature

In the present work we have studied the high-temperature shape memory alloys based on the Ru-Nb system by using two mechanical spectrometers working in temperature ranges from 200 to 1450ºC and -150 to 900ºC. We have studied internal friction peaks linked to the martensitic transformations in the range from 300 to 1200ºC. In addition, we have evidenced another internal friction peak at lower temperature than the transformations peaks, which apparently exhibits the behaviour of a thermally activated relaxation peak, but in fact is a strongly time-dependent peak. We have carefully studied this peak and discussed its microscopic origin, concluding that it is related to the interaction of some structural defects with martensite interfaces. Finally, we perform a complete analysis of the whole internal friction spectrum, taking into account the possible relationship between the time-dependent peak and the martensitic transformation behaviour.

scholarly journals Inelastic Behaviour of Ice Ih Single Crystals in the Low-Frequency Range Due to Dislocations

1978 ◽  
Vol 21 (85) ◽  
pp. 375-384 ◽  
Author(s):  
René Vassoille ◽  
Christian Maï ◽  
Joseph Perez
Keyword(s):  
High Temperature ◽  
Internal Friction ◽  
Single Crystals ◽  
Empirical Relation ◽  
Low Frequency ◽  
Frequency Range ◽  
High Temperature Range ◽  
Temperature Range ◽  
Inelastic Behaviour ◽  
Torsional Pendulum

Abstract The inelastic behaviour of ice Ih single crystals has been investigated by an inverted torsional pendulum in the low-frequency range. Three features are distinguished: (i) a relaxation peak previously observed by several authors in the higher-frequency range, (ii) an internal friction increasing with temperature in the high-temperature range (230–273 K), (iii) within this high-temperature range, internal friction becomes amplitude dependent, and this dependence becomes greater the greater the temperature. In this case, the internal friction has been interpreted in terms of movements of dislocations. Hence, the experimental results are interpreted with a model of internal friction based on an empirical relation for the velocity of dislocations. This model of internal friction is in fair agreement with experimental data . It is possible then to get an estimate of dislocation density. Hence it is shown that internal friction experiments can be useful in the study of the plastic behaviour of ice single crystals.

Low-Frequency High-Temperature Internal Friction in Ti-13Nb-13Zr Alloy

2006 ◽  
Vol 319 ◽  
pp. 103-108
Author(s):  
Terlize Cristina Niemeyer ◽  
Carlos Roberto Grandini ◽  
Sandra G. Schneider
Keyword(s):  
High Temperature ◽  
Internal Friction ◽  
Low Frequency ◽  
Beta Phase ◽  
Arc Melting ◽  
Damping Material ◽  
Free Decay ◽  
Orthopedic Applications ◽  
Relaxation Structure ◽  
Microstructure Of The Material

Recent studies have been done to achieve biomedical alloys containing non-toxic elements and presenting low elastic moduli. It has been reported that Ti-Nb-Zr alloys rich in beta phase, especially Ti-13Nb-13Zr, have potential characteristics for substituting conventional materials such as Ti-6Al-4V, stainless steel and Co alloys. The aim of this work is to study the internal friction (IF) of Ti-13Nb-13Zr (TNZ) alloy due to the importance of the absorption impacts in orthopedic applications. The internal friction of this alloy produced by arc melting was measured using an inverted torsion pendulum with the free decay method. The measurements were performed from 77 to 700 K with heating rate of 1 K/min, in a vacuum better than 10-5 mBar. The results show a relaxation structure at high temperature strongly dependent on microstructure of the material. Qualitative discussions are presented for the experimental results, and the possibility of using the TNZ as a high damping material is briefly mentioned.

Influences of Annealing and Deformation on the High Temperature Internal Friction Spectra of Al-0.013%Wt Ce Alloy

2011 ◽  
Vol 197-198 ◽  
pp. 1573-1576
Author(s):  
Xiao Hui Cao ◽  
Shou Jing Wang
Keyword(s):  
High Temperature ◽  
Internal Friction ◽  
Grain Boundary ◽  
Low Frequency ◽  
Grain Boundary Sliding ◽  
Boundary Sliding ◽  
Higher Temperature ◽  
Lower Temperature ◽  
Two Peaks ◽  
Internal Friction Spectra

By using a low frequency inverted torsion pendulum, the high temperature internal friction spectra of Al-0.013wt%Ce alloy subjected to deformation at different tensile rates was measured, and three peaks, the conventional grain boundary peak (P1), the bamboo peak (P2) and the soild solution peak (P3) were found. Increases of annealing temperature and deformation rate make P1 and P2 lower with P1 shifting to higher temperature and P2 to lower temperature. P3 was only found in the as-received samples. The dependence of P1 and P2 on grain size indicates that the two peaks are originated from the grain boundary sliding, and P3 may be associated with the diffusion of Ce atoms or other impurities at grain boundaries.

scholarly journals Inelastic Behaviour of Ice Ih Single Crystals in the Low-Frequency Range Due to Dislocations

1978 ◽  
Vol 21 (85) ◽  
pp. 375-384
Author(s):  
René Vassoille ◽  
Christian Maï ◽  
Joseph Perez
Keyword(s):  
High Temperature ◽  
Internal Friction ◽  
Single Crystals ◽  
Empirical Relation ◽  
Low Frequency ◽  
Frequency Range ◽  
High Temperature Range ◽  
Temperature Range ◽  
Inelastic Behaviour ◽  
Torsional Pendulum

AbstractThe inelastic behaviour of ice Ih single crystals has been investigated by an inverted torsional pendulum in the low-frequency range. Three features are distinguished:(i) a relaxation peak previously observed by several authors in the higher-frequency range,(ii) an internal friction increasing with temperature in the high-temperature range (230–273 K),(iii) within this high-temperature range, internal friction becomes amplitude dependent, and this dependence becomes greater the greater the temperature.In this case, the internal friction has been interpreted in terms of movements of dislocations. Hence, the experimental results are interpreted with a model of internal friction based on an empirical relation for the velocity of dislocations. This model of internal friction is in fair agreement with experimental data . It is possible then to get an estimate of dislocation density. Hence it is shown that internal friction experiments can be useful in the study of the plastic behaviour of ice single crystals.

Sign in / Sign up

Export Citation Format

Share Document