Fourier Transformation Infrared Spectrum Characteristics of Synthetic Zeolite A

2013 ◽  
Vol 591 ◽  
pp. 12-15
Author(s):  
Xiao Hu Zhang ◽  
Chun Ying Zhang ◽  
Feng Zhan ◽  
Nan Chun Chen
Keyword(s):  
Infrared Spectrum ◽  
Fourier Transformation ◽  
Synthetic Zeolite ◽  
Raw Material ◽  
Zeolite A ◽  
X Ray Diffraction ◽  
Natural Materials ◽  
X Ray ◽  
Ft Ir ◽  
Spectrum Characteristics

Synthesis of zeolite A by the use of natural materials (naturally stellerite) has been achieved without template agent. The final product was tested with X-ray diffraction, which was identified as the zeolite A. Then, the raw material and each step product were tested with Fourier Transformation Infrared (FT-IR). Comparing their FT-IR, we analyzed their spectrum characteristics, differences and reasons.

scholarly journals Sorption of oil products on the synthetic zeolite granules

Mineralogia ◽  
2020 ◽  
Vol 51 (1) ◽  
pp. 1-7
Author(s):  
Magdalena Król ◽  
Piotr Rożek
Keyword(s):  
Phase Composition ◽  
Infrared Spectroscopy ◽  
Silicone Oil ◽  
Synthetic Zeolite ◽  
Oil Products ◽  
Zeolite A ◽  
X Ray Diffraction ◽  
X Ray ◽  
Mineral Sorbent

Abstract In this work, lightweight granules of zeolite Na-P1 based on expanded glass aggregates were synthesized for the application in oil products’ sorption. The sorption of gasoline, diesel and silicone oil tests were also conducted for raw expanded glass, zeolite A, clinoptilolite and mineral sorbent available at a fuel station. All sorbents were also characterized in terms of the phase composition (X-ray diffraction) and structure (infrared spectroscopy). The zeolite Na-P1 granules achieved the highest values of sorption capacities (1.8, 2.1 and 2.6 g/g, respectively), which makes them promising materials for oils’ removal.

Preparation and Analysis of Kaolinite Intercalated by Potassium Acetate

2010 ◽  
Vol 150-151 ◽  
pp. 1220-1224
Author(s):  
Xiao Man Du ◽  
Qin Fu Liu ◽  
Hong Fei Cheng
Keyword(s):  
Thermal Analysis ◽  
Electron Microscope ◽  
Fourier Transformation ◽  
Potassium Acetate ◽  
Basal Spacing ◽  
X Ray Diffraction ◽  
Immersion Method ◽  
X Ray ◽  
Ft Ir ◽  
Scanning Electron

The kaolinite-potassium acetate composite was prepared by the immersion method. The intercalation composites were characterized by means of Scanning Electron Microscope (SEM), X-ray diffraction (XRD), Fourier transformation infrared (FT-IR) and High-resolution thermogravimetric analysis (HRTG). The results of XRD show that the intercalation of kaolinite by potassium acetate causes an increase of the basal spacing from 0.718 to 1.42nm. Thermal analysis shows the dehydroxylation of kaolinite decreased from 464 °C to 459.5 °C after intercalation of potassium acetate and three endotherms at 280, 323 and 459.5 °C attributed to the loss of water in the composite, potassium acetate and hydroxyl in the composite.

Preparation of Conducting Polypyrrole in Gelatin Solution

2011 ◽  
Vol 306-307 ◽  
pp. 717-721
Author(s):  
Hui Rong Ma ◽  
Mei Li ◽  
Cong De Qiao ◽  
Jin Shui Yao
Keyword(s):  
Fourier Transformation ◽  
Polymerization Process ◽  
Gelatin Solution ◽  
X Ray Diffraction ◽  
X Ray ◽  
Preparation Conditions ◽  
Ft Ir ◽  
Gelatin Concentration ◽  
Size And Morphology ◽  
Conducting Polypyrrole

Polypyrrole (PPy) nanoparticles were successfully synthesized from the gelatin solution. PPy nanoparticles with different size and morphology are prepared by changing the preparation conditions including the gelatin concentrations, with surfactant or not. The characteristics of the obtained PPy particles was collected by scanning electron microscopy (SEM), The X-ray diffraction(XRD), Fourier transformation infrared(FT-IR) spectra and Four-probe conductivity meter. The results indicated PPy could form nanoparticles, whereas some bigger spheres occurred when the gelatin concentration is 0.05g/L and the conductivity of the PPy is 0.05S/cm. The possible mechanism was proposed that the gelatin is used as a morphology-directing agent in the polymerization process.

Characterization the Raw Material of Filler in Cellulose Film

2016 ◽  
Vol 675-676 ◽  
pp. 482-485
Author(s):  
Anusorn Montree ◽  
Kanyakorn Teanchai ◽  
Wichian Siriprom
Keyword(s):  
Organic Compound ◽  
Major Element ◽  
Raw Material ◽  
Natural Material ◽  
X Ray Diffraction ◽  
X Ray ◽  
Conventional Analysis ◽  
Chicken Eggshell ◽  
Ft Ir ◽  
Ft Ir Spectroscopy

The aim of this study is preliminary survey the natural material and investigates physicochemical properties of cellulose and chicken eggshell. The chickeneggshell as natural material which used as film filler in the cellulose/CaCO3 biocomposite. The potential and the possibilities of chicken eggshell to use as filler were studied with three conventional analysis techniques, X-ray Diffraction (XRD), Energy Dispersive X-ray Fluorescence (EDXRF) and Fourier transform infrared (FT-IR) spectroscopy. It was found that the structural of chicken eggshell have calcites phase and the structural of cellulose have amorphous crystalline phase while the chemical composition of both material were investigated by EDXRF which show the organic compound as major element in cellulose but in chicken eggshell the major element is organic compound and calcium (Ca) element. The deeply investigate molecular composition by FT-IR which show the characteristic feature have been studied.

Preparation of Zeolite A from Natural Stellerite

2012 ◽  
Vol 624 ◽  
pp. 287-290
Author(s):  
Chun Ying Zhang ◽  
Nan Chun Chen ◽  
Xiao Hu Zhang ◽  
Quan Tang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Hydrochloric Acid ◽  
Crystallization Time ◽  
Zeolite A ◽  
X Ray Diffraction ◽  
X Ray ◽  
End Products ◽  
Ft Ir ◽  
Scanning Electron

Zeolite A was prepared from natural stellerite under hydrothermal conditions.The experiments were carried at different crystallization temperatures and times，the experimental results and synthetical factors were analyzed and researched. The end products have been characterized by using FT–IR, X–ray diffraction (XRD) and scanning electron microscopy (SEM). The results indicate that zeolite A was synthesized on the condition of the crystallization temperature at 90~100°C and the crystallization time for 6 hours with 15% hydrochloric acid of stellerite modifying，according to certain proportion of stellerite.

scholarly journals Synthesis of Zeolite A From Coal Fly Ash with Variation of Si/Al Molar Ratio

2018 ◽  
Vol 19 (2) ◽  
pp. 105
Author(s):  
Novita Andarini ◽  
Tanti Haryati ◽  
Zuhrotul Lutfia
Keyword(s):  
Fly Ash ◽  
Hydrothermal Treatment ◽  
Coal Fly Ash ◽  
Synthetic Zeolite ◽  
Raw Material ◽  
Molar Ratio ◽  
Zeolite A ◽  
X Ray ◽  
Molar Ratios ◽  
Aluminosilicate Mineral

Fly ash containing 30-36% silica and 14,52-23,78% alumina can be potentially as raw material for synthetic zeolite such as zeolite A. Zeolite A is an aluminosilicate mineral which is rich in alumina so that this zeolite has a good cation exchange capability. Zeolite A has been synthesized by hydrothermal treatment after NaOH fusion. Fly ash has been fused with NaOH at 550 0C for 40 minutes and hydrothermally treated at 1000C for 5 hours. The hydrothermal treatment was conducted in some various Si/Al molar ratios from 0.90; 1.00.; 1.05; to 1.24. The zeolite A was then analyzed using XRD and XRF. The best zeolite A based on XRD result is zeolite with Si/Al molar ratio of 1.1 with crystallinity of 96,80%. The x-ray fluorescence result showed that the Si/Al molar ratios of the four zeolite samples were close to of Si/Al molar ratios of 1, 1.1, 1.21.3 respectively.Keywords: Fly ash, Zeolite A, Hydrothermal Fusion

scholarly journals 3-Mercaptopropyltrimethoxysilane Modified Diatomite: Preparation and Application for Voltammetric Determination of Lead (II) and Cadmium (II)

2017 ◽  
Vol 2017 ◽  
pp. 1-10 ◽  
Author(s):  
Dinh Quang Khieu ◽  
Bui Hai Dang Son ◽  
Vo Thi Thanh Chau ◽  
Pham Dinh Du ◽  
Nguyen Hai Phong ◽  
...  
Keyword(s):  
Thermal Treatment ◽  
Fourier Transformation ◽  
Treatment Temperature ◽  
Carbon Paste ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ft Ir ◽  
Paste Electrode ◽  
Modified Diatomite

In this study, functionalized diatomite was prepared by grafting of 3-mercaptopropyltrimethoxysilane (MPTMS) to diatomite (MPTMS-diatomite). The diatomite with thermal treatment from 100 to 700°C was functionalized by MPTMS under dry and humid conditions. The obtained MPTMS-diatomite was characterized by X-ray diffraction (XRD), thermal gravity-differential scanning calorimeter (TG-DSC), and Fourier transformation infrared (FT-IR). The results showed that an increase in treatment temperature seems to reduce the loading of MPTMS onto diatomite. The humidity of diatomite was favorable for the grafting of functional groups on the surface. The possible mechanisms of MPTMS loading to diatomite (MPTMS-diatomite) were also proposed. The performance of a carbon paste electrode (CPE) modified with MPTMS-diatomite in the simultaneous determination of Cd(II) and Pb(II) ions was addressed.

Comparation Trace Element and Structural of Filler Materials in Chitosan Films

2016 ◽  
Vol 675-676 ◽  
pp. 213-216
Author(s):  
Noppadon Chamchoi ◽  
Narong Sangwaranatee ◽  
Jakrapong Kaewkhao ◽  
A. Montree ◽  
K. Teanchai ◽  
...  
Keyword(s):  
Trace Element ◽  
Functional Group ◽  
Raw Material ◽  
Filler Materials ◽  
X Ray Diffraction ◽  
X Ray ◽  
Biocomposite Films ◽  
Result Show ◽  
Chicken Eggshell ◽  
Ft Ir

In present study, the structural and trace element were preliminary survey the potentiality to use as filler material for produced the biocomposite films. The first raw material is chitosan and the second raw material is chicken eggshell. Both raw material were investigated the structural and morphological with X-ray Diffraction (XRD) and Scaning Electron Microscope (SEM), respectively. While, Fourier transform infrared spectroscopy (FT-IR) the Energy Dispersive X-ray Fluorescence (EDXRF) were used to investigate functional group and trace element, respectively. The result show that, both material have crystalline structural. The chicken eggshell have calcite structure while the chitosan have amorphos-crystalline structure. The chemical composition in both material compose of P, Ca, Fe similarly but the concentration have been different.

Synthesis and Characterization of Novel PCA-PEG-PCA Triblock Copolymer

2012 ◽  
Vol 499 ◽  
pp. 95-98
Author(s):  
Jun Chang ◽  
Cheng Wu Li ◽  
Gang Li
Keyword(s):  
Polyethylene Glycol ◽  
Triblock Copolymer ◽  
Chloroacetic Acid ◽  
Raw Material ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ft Ir ◽  
Solution Polycondensation ◽  
Ft Ir Spectroscopy

Using chloroacetic acid(CA) and polyethylene glycol(PEG) as raw material, polyacetic acid-polyethylene glycol-polyacetic acid(PCA-PEG-PCA) triblock copolymer was synthesized by solution polycondensation. The triblock copolymer was characterized by FT-IR spectroscopy、X-Ray Diffraction and DSC. The structure of copolymer was confirmed by FT-IR. The crystallinity of compolymer was 51.24% investigated by XRD, and the result of DSC showed the PCA and PEG was homogeneous with a good compatibility.

scholarly journals First Report on the Geologic Occurrence of Natural Na–A Zeolite and Associated Minerals in Cretaceous Mudstones of the Paja Formation of Vélez (Santander), Colombia

Crystals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 218
Author(s):  
Carlos Alberto Ríos-Reyes ◽  
German Alfonso Reyes-Mendoza ◽  
José Antonio Henao-Martínez ◽  
Craig Williams ◽  
Alan Dyer
Keyword(s):  
Natural Zeolite ◽  
Scanning Electron Micrographs ◽  
Total Sulfur ◽  
Zeolite A ◽  
X Ray Diffraction ◽  
X Ray ◽  
Mineral Phases ◽  
The World ◽  
Porosity And Permeability ◽  
First Time

This study reports for the first time the geologic occurrence of natural zeolite A and associated minerals in mudstones from the Cretaceous Paja Formation in the urban area of the municipality of Vélez (Santander), Colombia. These rocks are mainly composed of quartz, muscovite, pyrophyllite, kaolinite and chlorite group minerals, framboidal and cubic pyrite, as well as marcasite, with minor feldspar, sulphates, and phosphates. Total organic carbon (TOC), total sulfur (TS), and millimeter fragments of algae are high, whereas few centimeters and not biodiverse small ammonite fossils, and other allochemical components are subordinated. Na–A zeolite and associated mineral phases as sodalite occur just beside the interparticle micropores (honeycomb from framboidal, cube molds, and amorphous cavities). It is facilitated by petrophysical properties alterations, due to processes of high diagenesis, temperatures up to 80–100 °C, with weathering contributions, which increase the porosity and permeability, as well as the transmissivity (fluid flow), allowing the geochemistry remobilization and/or recrystallization of pre-existing silica, muscovite, kaolinite minerals group, salts, carbonates, oxides and peroxides. X-ray diffraction analyses reveal the mineral composition of the mudstones and scanning electron micrographs show the typical cubic morphology of Na–A zeolite of approximately 0.45 mμ in particle size. Our data show that the sequence of the transformation of phases is: Poorly crystalline aluminosilicate → sodalite → Na–A zeolite. A literature review shows that this is an unusual example of the occurrence of natural zeolites in sedimentary marine rocks recognized around the world.

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