scholarly journals Hydrothermal Transformation of Microporous Lithium Zinc Phosphates: A Kinetic Study Using in situ Synchrotron Radiation Powder Diffraction

1998 ◽  
Vol 278-281 ◽  
pp. 414-417
Author(s):  
T.R. Jensen ◽  
P. Norby ◽  
J.C. Hanson
Keyword(s):  
Synchrotron Radiation ◽  
Kinetic Study ◽  
Powder Diffraction ◽  
Zinc Phosphates ◽  
Hydrothermal Transformation

Applications of High-Resolution Powder X-Ray Diffraction

2007 ◽  
Vol 130 ◽  
pp. 7-14 ◽  
Author(s):  
Andrew N. Fitch
Keyword(s):  
High Resolution ◽  
Synchrotron Radiation ◽  
Powder Diffraction ◽  
X Rays ◽  
X Ray Diffraction ◽  
Crystalline Materials ◽  
X Ray ◽  
Structural Characterisation ◽  
Pdf Analysis

The highly-collimated, intense X-rays produced by a synchrotron radiation source can be harnessed to build high-resolution powder diffraction instruments with a wide variety of applications. The general advantages of using synchrotron radiation for powder diffraction are discussed and illustrated with reference to the structural characterisation of crystalline materials, atomic PDF analysis, in-situ and high-throughput studies where the structure is evolving between successive scans, and the measurement of residual strain in engineering components.

Apparatus for the in situ kinetic study of reactions involving air sensitive materials using energy‐dispersive powder diffraction

1994 ◽  
Vol 65 (7) ◽  
pp. 2210-2213 ◽  
Author(s):  
S. M. Clark ◽  
P. Irvin ◽  
J. Flaherty ◽  
T. Rathbone ◽  
H. V. Wong ◽  
...  
Keyword(s):  
Kinetic Study ◽  
Powder Diffraction ◽  
Energy Dispersive

Crystallization of Bulk Zr48Nb8Cu14Ni12Be18Metallic Glass

2000 ◽  
Vol 644 ◽  
Author(s):  
Y.X. Zhuang ◽  
L. Gerward ◽  
J.Z. Jiang ◽  
J.S. Olsen ◽  
Y. Zhang ◽  
...  
Keyword(s):  
Differential Scanning Calorimetry ◽  
High Pressure ◽  
Glass Transition ◽  
High Temperature ◽  
Synchrotron Radiation ◽  
Powder Diffraction ◽  
Applied Pressure ◽  
Scanning Calorimetry ◽  
X Ray

AbstractThe crystallization of bulk Zr48Nb8Cu14Ni12Be18metallic glass has been investigated by differential scanning calorimetry (DSC) and X-ray powder diffraction. The activation energies of glass transition and crystallization for the glass obtained using Kissinger analysis from the shift of the peak temperature in the DSC curve are 470 and 235 kJ/mol, respectively. The effect of applied pressure on crystallization is studied by in situ high-pressure and high-temperature X-ray powder diffraction using synchrotron radiation. It is found that the crystallization temperature increases with pressure having a slope of 9.5 K/GPa in the range of 0-4.4 GPa.

A new gas system for automatedin situpowder diffraction studies at the European Synchrotron Radiation Facility

2013 ◽  
Vol 46 (2) ◽  
pp. 570-572 ◽  
Author(s):  
Adrian H. Hill
Keyword(s):  
High Resolution ◽  
Synchrotron Radiation ◽  
Powder Diffraction ◽  
European Synchrotron Radiation Facility ◽  
Structural Studies ◽  
Control Software ◽  
Gas System

A new gas dosing rig built for the high-resolution powder diffraction beamline (ID31) at the ESRF is described. The rig is fully controlled and monitored by the beamline control software, enabling automated absorption and desorption of fixed pressures of gases up to 100 bar (107 Pa) forin situstructural studies. The rig has successfully been used on ID31 as well as other beamlines at the ESRF.

A Kinetic Study of Thermal Decomposition of Limestone Using In Situ High Temperature X-Ray Powder Diffraction

2012 ◽  
Vol 95 (8) ◽  
pp. 2491-2498 ◽  
Author(s):  
Nicoletta Marinoni ◽  
Stefano Allevi ◽  
Maurizio Marchi ◽  
Monica Dapiaggi
Keyword(s):  
Thermal Decomposition ◽  
High Temperature ◽  
Kinetic Study ◽  
Powder Diffraction ◽  
X Ray
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