Dynamic Recrystallization of Dense Polycrystalline NaCl: Dependence of Grain Size Distribution on Stress and Temperature

2004 ◽  
Vol 467-470 ◽  
pp. 1187-1192 ◽  
Author(s):  
J.H. ter Heege ◽  
J.H.P. de Bresser ◽  
C.J. Spiers

Only few models explain the development of a steady state grain size during dynamic recrystallization, and their microphysical basis is poorly understood. In this study, we investigate mechanical and microstructural data on dry and wet NaCl, deformed at a range of stresses and temperatures at elevated pressure, with the aim to evaluate the different models. The results show that dry NaCl continuously work hardens and shows evidence for recrystallization dominated by progressive subgrain rotation, while the wet material shows, at similar conditions, oscillating stressstrain behaviour and recrystallization dominated by grain boundary migration. Taking into account the distribution of grain size, deformation of wet NaCl is best described by flow laws based on composite grain size sensitive (GSS) solution-precipitation creep and grain size insensitive (GSI) dislocation creep. The recrystallized grain size data in wet NaCl can be modeled with the hypothesis that recrystallized grain size organises itself in the boundary between the GSS and GSS creep domains.

2021 ◽  
Author(s):  
Mark Coleman ◽  
Bernhard Grasemann ◽  
David Schneider ◽  
Konstantinos Soukis ◽  
Riccardo Graziani

<p>Microstructures may be used to determine the processes, conditions and kinematics under which deformation occurred. For a given set of these variables, different microstructures are observed in various materials due to the material’s physical properties. Dolomite is a major rock forming mineral, yet the mechanics of dolomite are understudied compared to other ubiquitous minerals such as quartz, feldspar, and calcite. Our new study uses petrographic, structural and electron back scatter diffraction analyses on a series of dolomitic and calcitic mylonites to document differences in deformation styles under similar metamorphic conditions. The Attic-Cycladic Crystalline Complex, Greece, comprises a series of core complexes wherein Miocene low-angle detachment systems offset and juxtapose a footwall of high-pressure metamorphosed rocks against a low-grade hanging wall. This recent tectonic history renders the region an excellent natural laboratory for studying the interplay of the processes that accommodate deformation. The bedrock of Mt. Hymittos, Attica, preserves a pair of ductile-then-brittle normal faults dividing a tripartite tectonostratigraphy. Field observations, mineral assemblages and observable microstructures suggests the tectonic packages decrease in metamorphic grade from upper greenschist facies (~470 °C at 0.8 GPa) in the stratigraphically lowest package to sub-greenschist facies in the stratigraphically highest package. Both low-angle normal faults exhibit cataclastic fault cores that grade into the schists and marbles of their respective hanging walls. The middle and lower tectonostratigraphic packages exhibit dolomitic and calcitic marbles that experienced similar geologic histories of subduction and exhumation. The mineralogically distinct units (calcite vs. dolomite) of the middle package deformed via different mechanisms under the same conditions within the same package and may be contrasted with mineralogically similar units that deformed under higher pressure and temperature conditions in the lower package. In the middle unit, dolomitic rocks are brittlely deformed. Middle unit calcitic marble are mylonitic to ultramylonitic with average grain sizes ranging from 30 to 8 μm. These mylonites evince grain-boundary migration and grain size reduction facilitated by subgrain rotation. Within the lower package, dolomitic and calcitic rocks are both mylonitic to ultramylonitic with grain sizes ranging from 28 to 5 μm and preserve clear crystallographic preferred orientation fabrics. Calcitic mylonites exhibit deformation microstructures similar to those of the middle unit. Distinctively, the dolomitic mylonites of the lower unit reveal ultramylonite bands cross-cutting and overprinting an older coarser mylonitic fabric. Correlated missorientation angles suggest these ultramylonites show evidence for grain size reduction accommodated by microfracturing and subgrain rotation. In other samples the dolomitic ultramylonite is the dominant fabric and is overprinting and causing boudinage of veins and relict coarse mylonite zones. Isolated interstitial calcite grains within dolomite ultramylonites are signatures of localized creep-cavitation processes. Following grain size reduction, grain boundary sliding dominantly accommodated further deformation in the ultramylonitic portions of the samples as indicated by randomly distributed correlated misorientation angles. This study finds that natural deformation of dolomitic rocks may occur by different mechanisms than those identified by published experiments; notably that grain-boundary migration and subgrain rotation may be active in dolomite at much lower temperatures than previously suggested.</p>


Minerals ◽  
2018 ◽  
Vol 9 (1) ◽  
pp. 17
Author(s):  
Caroline Bollinger ◽  
Billy Nzogang ◽  
Alexandre Mussi ◽  
Jérémie Bouquerel ◽  
Dmitri Molodov ◽  
...  

Plastic deformation of peridotites in the mantle involves large strains. Orthorhombic olivine does not have enough slip systems to satisfy the von Mises criterion, leading to strong hardening when polycrystals are deformed at rather low temperatures (i.e., below 1200 °C). In this study, we focused on the recovery mechanisms involving grain boundaries and recrystallization. We investigated forsterite samples deformed at large strains at 1100 °C. The deformed microstructures were characterized by transmission electron microscopy using orientation mapping techniques (ACOM-TEM). With this technique, we increased the spatial resolution of characterization compared to standard electron backscatter diffraction (EBSD) maps to further decipher the microstructures at nanoscale. After a plastic strain of 25%, we found pervasive evidence for serrated grain and subgrain boundaries. We interpreted these microstructural features as evidence of occurrences of grain boundary migration mechanisms. Evaluating the driving forces for grain/subgrain boundary motion, we found that the surface tension driving forces were often greater than the strain energy driving force. At larger strains (40%), we found pervasive evidence for discontinuous dynamic recrystallization (dDRX), with nucleation of new grains at grain boundaries. The observations reveal that subgrain migration and grain boundary bulging contribute to the nucleation of new grains. These mechanisms are probably critical to allow peridotitic rocks to achieve large strains under a steady-state regime in the lithospheric mantle.


2007 ◽  
Vol 550 ◽  
pp. 393-398 ◽  
Author(s):  
D.T. McDonald ◽  
John F. Humphreys ◽  
Pete S. Bate

The microstructure and texture in dynamically recrystallized copper and two copper – tin alloys (2wt% and 4.5wt% tin) has been investigated. Specimens were deformed in channel-die plane strain compression to true strains from 0.1 to 1.22 within the temperature range 200°C to 700°C, and the resulting microstructures were investigated with the use of high resolution electron backscatter diffraction (EBSD). Dynamic recrystallization was initiated by the bulging of preexisting high angle grain boundaries (HAGB), and occurred primarily by strain induced boundary migration (SIBM) and twinning. The addition of tin led to an increase in the temperature at which dynamic recrystallization initiated, and furthermore to a smaller dynamically recrystallized grain size. This was attributed to the effects of solute drag causing lower HAGB mobility. Dynamic recrystallization was observed to weaken the deformation texture components of brass and Goss, as well as introduce a cube texture component which generally tended to strengthen with temperature but weaken with increasing tin additions.


Minerals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1038
Author(s):  
Toru Takeshita

The Sambagawa metamorphic rocks in central Shikoku, southwest Japan consist of an inverted metamorphic sequence from the upper chlorite to oligoclase-biotite zones at the lower structural level (LSL), which is overlain by a normal metamorphic sequence consisting of the albite-biotite and garnet zones at the upper structural level (USL). These sequences form a large-scale recumbent fold called the Besshi nappe. To unravel the mechanism of recrystallization and physical conditions in quartz, and their relation to exhumation tectonics, microstructures of recrystallized quartz grains in quartz schist from the Asemi-Saruta-Dozan River traverse were analyzed. The recrystallized quartz grain size increases with increasing structural level from 40 µm in the upper chlorite zone to 160 µm in the garnet zone of the USL. Further, the mechanism of dynamic recrystallization of quartz changes from subgrain rotation to grain boundary migration with increasing structural level across the uppermost garnet zone of the LSL. From these data, the deformation temperatures in quartz schist are calculated to increase with increasing structural level within the range between 300 and 450 °C using paleopiezometers and experimental flow laws. It could be interpreted that a rapid cooling of the Besshi nappe from above is responsible for the deformation temperatures recorded in quartz schist.


Solid Earth ◽  
2014 ◽  
Vol 5 (2) ◽  
pp. 805-819 ◽  
Author(s):  
D. Dorner ◽  
K. Röller ◽  
B. Stöckhert

Abstract. Indentation creep tests are established in materials engineering, providing information on rheology, deformation mechanisms, and related microstructures of materials. Here we explore the potential of this method on natural, polycrystalline anhydrite. The tests are run at atmospheric pressure, temperatures between 700 and 920 °C, and reference stresses between 7 and 30 MPa. An activation energy Q of 338 kJ mol−1 and a stress exponent n of 3.9 are derived. Deformation is localized into shear zones bounding a less deformed approximately conical plug underneath the indenter. Shear zone microstructures reveal inhomogeneous crystal–plastic deformation, subgrains, and extensive strain-induced grain boundary migration, while mechanical twinning appears not to be activated. Microstructure and mechanical data are consistent with deformation by dislocation creep.


2007 ◽  
Vol 26-28 ◽  
pp. 449-452 ◽  
Author(s):  
M. Honda ◽  
Tokuteru Uesugi ◽  
Yorinobu Takigawa ◽  
Hiroshi Mabuchi ◽  
Kenji Higashi

Dynamic recrystallization behavior that occurs during the hot extrusion was examined in two commercial Mg alloys, AZ31 and AZ80 alloys. The initial grain size, d0, and the dynamically recrystallized grain size, drec, after the extrusion was investigated using optical microscopy. The dynamically recrystallized grain size decreased with an increasing the Zener-Hollomon parameter.


2013 ◽  
Vol 5 (2) ◽  
pp. 2081-2118
Author(s):  
D. Dorner ◽  
K. Röller ◽  
B. Stöckhert

Abstract. Indentation creep tests are established in materials engineering, providing information on rheology, deformation mechanisms, and related microstructures of materials. Here we explore the potential of this method on natural, polycrystalline anhydrite. The tests are run at atmospheric pressure, temperatures between 700 °C and 920 °C, and reference stresses between 7 MPa and 30 MPa. An activation energy Q of 338 kJ mol−1 and a stress exponent n of 3.9 are derived. Deformation is localized into shear zones bounding a less deformed approximately conical plug underneath the indenter. Shear zone microstructures reveal inhomogeneous crystal plastic deformation, subgrains, and extensive strain induced grain boundary migration, while mechanical twinning appears not to be activated. Microstructure and mechanical data are consistent with deformation by dislocation creep. Extrapolated to slow natural strain rates, the flow law predicts a high flow strength of anhydrite compared to previous studies.


1999 ◽  
Vol 32 (1-4) ◽  
pp. 47-63 ◽  
Author(s):  
R. Kaibyshev ◽  
B. Sokolov ◽  
A. Galiyev

The influence of a crystallographic texture (CT) on Dynamic Recrystallization (DRX) was investigated at T= 300℃ and 2.8 x 10-3 s-1 in Mg–5.8% Zn–0.65% Zr in detail. It was shown that mechanics and kinetics of DRX are in strong dependence on location of basal planes. Initial texture effects recrystallized grain size too. Extensive recrystallization process was observed in cases when basal planes locate parallelly or at right angles to a compression axis. Almost full recrystallization structure was formed after moderate strains. If basal planes locate at 45° to the compression axis DRX occurs slowly and the formed grain size is less as compared to the other two cases. Microstructure evolution was considered in context of relationship between DRX and mechanisms of plastic deformation. It was established that the effect of initial texture on DRX is promoted by its influence on the character of dislocation slip. The reasons for the influence of the character of dislocation slip on DRX are discussed.


1994 ◽  
Vol 40 (134) ◽  
pp. 46-55
Author(s):  
C.J. L. Wilson ◽  
Y. Zhang

AbstractAn examination of both experiments and computer models of polycrystalline ice undergoing a simple shear suggests that there is good agreement. The model has correctly reproduced the deformational and microstructural features caused by glide on (0001) in the ice aggregates. This success is particularly prominent for those ice grains with a lattice orientation suitable for hard or easy glide or kinking, and where there is a sub-horizontal с axis and a larger grain-size. A limitation may be that the model cannot explicitly simulate recrystallization and grain-boundary migration, which are two other important processes operating jointly with glide in experimentally deformed ice. However, through the use of the models, it is possible to show how kinematic factors can control the processes of recrystallization. The localization of recrystallization in the polycrystalline ice aggregate is determined by the stress and strain variations between neighbouring grains.


1994 ◽  
Vol 40 (134) ◽  
pp. 46-55 ◽  
Author(s):  
C.J. L. Wilson ◽  
Y. Zhang

AbstractAn examination of both experiments and computer models of polycrystalline ice undergoing a simple shear suggests that there is good agreement. The model has correctly reproduced the deformational and microstructural features caused by glide on (0001) in the ice aggregates. This success is particularly prominent for those ice grains with a lattice orientation suitable for hard or easy glide or kinking, and where there is a sub-horizontalсaxis and a larger grain-size. A limitation may be that the model cannot explicitly simulate recrystallization and grain-boundary migration, which are two other important processes operating jointly with glide in experimentally deformed ice. However, through the use of the models, it is possible to show how kinematic factors can control the processes of recrystallization. The localization of recrystallization in the polycrystalline ice aggregate is determined by the stress and strain variations between neighbouring grains.


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