Analysis of the Fundamental Mechanisms and Efficiency of the Deformation Methods of Nanostructuring

2008 ◽  
Vol 584-586 ◽  
pp. 29-34 ◽  
Author(s):  
Radik R. Mulyukov ◽  
Ayrat A. Nazarov ◽  
Renat M. Imayev
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
High Pressure ◽  
High Temperature ◽  
Severe Plastic Deformation ◽  
Grain Refinement ◽  
Equal Channel Angular Pressing ◽  
Efficient Method ◽  
High Pressure Torsion ◽  
Angular Pressing

Deformation methods of nanostructuring (DMNs) of materials are proposed to classify into severe plastic deformation (SPD) and mild plastic deformation (MPD) methods according to fundamentally different low- and high-temperature grain refinement mechanisms they exploit. A general analysis of the fundamentals and nanostructuring efficiency of three most developed DMNs, high pressure torsion (HPT), equal-channel angular pressing (ECAP), and multiple isothermal forging (MIF) is done with a particular attention to ECAP and MIF. It is demonstrated that MIF is the most efficient method of DMNs allowing one to obtain the bulkiest nanostructured samples with enhanced mechanical properties.

Equal Channel Angular Pressing of Al Alloy AA2219

2009 ◽  
Vol 67 ◽  
pp. 53-58
Author(s):  
V. Anil Kumar ◽  
M.K. Karthikeyan ◽  
Rohit Kumar Gupta ◽  
P. Ramkumar ◽  
P.P. Sinha
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Grain Refinement ◽  
Equal Channel Angular Pressing ◽  
High Strength ◽  
Dark Field ◽  
Grain Structure ◽  
Al Alloy ◽  
Angular Pressing

Severe plastic deformation processes (SPD) are gaining importance as advanced materials processing techniques and hold immense potential in obtaining ultra fine-grained high strength materials. Among the SPD techniques, Equal channel angular pressing (ECAP) has its own merits to produce materials with ultra fine grains in bulk with better mechanical properties. The material deforms with high level of plastic strain inside the channel resulting in grain refinement of the output material with improvement in mechanical properties. A very viable die configuration was conceptualized and die was made with 1200 channel angle. Processing of 25 mm dia. of Al alloy AA2219 at room temperature was successfully carried out and grain refinement was observed. The mechanism of grain refinement has been studied using optical and transmission electron microscopy (TEM). It was observed that low energy dislocation structure (LEDS) forms concurrently with sub-grain structure due to dislocation rearrangements, which provide stability to the evolving sub-grain structure. Dislocation mobility is hindered by the presence of precipitates and / or intermetallic dispersoids present in the matrix and results in presence of dislocations in grain interiors. The pile up of dislocations at intermetallic dispersoids was confirmed from the dark field TEM micrographs. Present paper describes the experimental procedure and followed to attain severe plastic deformation through ECAP. Increase in hardness as well as refinement in the grain size after 5-passes have been discussed in light of extensive optical and TEM. The mechanisms of grain refinement to achieve nano-grained structure and strengthening accrued from the grain refinement through ECAP has been discussed.

Microstructure and Mechanical Properties of the SPD-Processed TiNi Alloys

2013 ◽  
Vol 738-739 ◽  
pp. 486-490 ◽  
Author(s):  
Dmitriy Gunderov ◽  
Alexandr Lukyanov ◽  
Egor Prokofiev ◽  
Anna Churakova ◽  
Vladimir Pushin ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Cold Rolling ◽  
High Pressure Torsion ◽  
Angular Pressing ◽  
Ultrafine Grained ◽  
First Results ◽  
Equal Channel Angular Pressure

The article represents results of influence of different severe plastic deformation (SPD) techniques on TiNi alloys. It is demonstrated that strength and shape memory effect (SME) of TiNi can be significantly enhanced due to formation of ultrafine-grained (UFG) and nanocrystalline (NC) structures by SPD. Influence of equal channel angular pressing (ECAP), high pressure torsion (HPT), multi-step SPD deformations (ECAP plus cold rolling) on structure, mechanical and functional properties of TiNi alloys is considered. There are represented first results of influence of equal channel angular pressure-Conform (ECAP-C) on TiNi alloys, which is a perspective technology for industrial fabrication of UFG metals and alloys.

Bulk Ultrafine and Nanostructured Materials from Consolidation of Particles by Severe Plastic Deformation

2008 ◽  
Vol 579 ◽  
pp. 61-74 ◽  
Author(s):  
Kenong Xia
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Nanostructured Materials ◽  
High Pressure Torsion ◽  
Processing Parameters ◽  
Back Pressure ◽  
Angular Pressing ◽  
Important Processing

The progress in bulk ultrafine and nanostructured materials through consolidation of particles by severe plastic deformation (SPD) is reviewed. The focus is on the processes of high pressure torsion (HPT) and equal channel angular pressing (ECAP) with or without the application of a back pressure. Various materials consolidated are described in terms of their densities, microstructures and mechanical properties. The important processing parameters and their effects on the resulting materials are discussed. It is shown that SPD consolidation of particles is an effective way of producing bulk nanostructured materials although much work is needed to understand the consolidation behaviour and to design the optimum compositions and microstructures.

Positron Annihilation Studies of Microstructure of Ultra Fine Grained Metals Prepared by Severe Plastic Deformation

2005 ◽  
Vol 482 ◽  
pp. 207-210 ◽  
Author(s):  
Jakub Čížek ◽  
Ivan Procházka ◽  
Bohumil Smola ◽  
Ivana Stulíková ◽  
Radomír Kužel ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Spatial Distribution ◽  
Severe Plastic Deformation ◽  
Positron Annihilation ◽  
Equal Channel Angular Pressing ◽  
High Pressure Torsion ◽  
Positron Annihilation Spectroscopy ◽  
Fine Grained ◽  
Angular Pressing

In the present work, positron annihilation spectroscopy (PAS) is employed for microstructure investigations of various ultra fine grained (UFG) metals (Cu, Ni, Fe) prepared by severe plastic deformation (SPD), namely high-pressure torsion (HPT) and equal channel angular pressing (ECAP). Generally, UFG metals prepared using both the techniques exhibit two kinds of defects introduced by SPD: dislocations and small microvoids. The size of the microvoids is determined from the PAS data. Significantly larger microvoids are found in HPT deformed Fe and Ni compared to HPT deformed Cu. The microstructure of UFG Cu prepared by HPT and ECAP is compared and the spatial distribution of defects in UFG Cu samples is characterized. In addition, the microstructure of a pure UFG Cu prepared by HPT and HPT deformed Cu+Al2O3 nanocomposite (GlidCop) is compared.

Role of Strain Gradient and Dynamic Transformation on the Formation of Nanocrystalline Structure Produced by Severe Plastic Deformation

2007 ◽  
Vol 539-543 ◽  
pp. 2787-2792 ◽  
Author(s):  
Minoru Umemoto ◽  
Yoshikazu Todaka ◽  
Jin Guo Li ◽  
Koichi Tsuchiya
Keyword(s):  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Grain Refinement ◽  
Strain Gradient ◽  
High Pressure Torsion ◽  
Large Strain ◽  
Nanocrystalline Structure ◽  
Angular Pressing ◽  
Dynamic Transformation ◽  
Fine Grained Structure

Formation of nanocrystalline structure by severe plastic deformation has studied extensively. Although ultra fine grained structure (grain size larger than 100 nm) had been obtained in many processes such as heavy cold rolling, equal channel angular pressing (ECAP) or accumulative roll bonding (ARB), the formation of nano grained structure (< 100 nm) is limited to processes such as ball milling, shot peening or drilling. In the present study, high pressure torsion (HPT) deformation and drilling were carried out to understand the conditions necessary to obtain nano grained structure in steels. The results of HPT experiments in pure Fe showed that HPT has superior ability of strengthening and grain refinement probably due to a strain gradient but the saturation of grain refinement occurs before reaching nano grained structure. Drilling experiments in high carbon martensitic steel revelaed that nano grained ferrite forms at the drilled hole surface only when the transformation from ferrite to austenite takes place during drilling. Considering various other processes by which nano grained ferrite was produced, it is proposed that heavy strains with large strain gradients together with dynamic transformation are necessary to reach nano grained ferrite structure.

scholarly journals Influence of special features of the gradient structure formation during severe plastic deformation of alloys with different types of a crystalline lattice

2019 ◽  
Vol 17 (1) ◽  
pp. 64-75 ◽  
Author(s):  
Georgy I. Raab ◽  
Ilyas S. Kodirov ◽  
Gennady N. Aleshin ◽  
Arseniy G. Raab ◽  
Nikolai K. Tsenev
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Structure Formation ◽  
High Pressure Torsion ◽  
Crystalline Lattice ◽  
Gradient Structure ◽  
Temperature Range ◽  
Deformation Treatment

Problem Statement (Relevance): The paper describes some features and prospective benefits of deformation by methods of drawing with shear (SD) and high pressure torsion (HPT) in a temperature range of dynamic strain aging (DSA) effect, which allow receiving a high complex of physical and mechanical properties. Objectives: The study aims to investigate and analyze features of the structure formation with the combined application of severe plastic deformation (SPD) and the DSA effect during deformation by drawing with shear and high pressure torsion, to establish patterns of the gradient structure formation. Methods Applied: 1. Computer simulation in Deform 3D software to investigate the stress-strain state on materials with various types of a crystalline lattice: copper grade M1 (FCC), Steel 10 (BCC) and titanium VT1-0 (HCP) and a further comparison with experimental results. 2. Microhardness measurement 3. Scanning and transmission electron microscopy. Originality: This research resulted in investigation of the combined effect of the DSA effect and SPD on the gradient structure formation and mechanical properties of metals with various crystalline lattices. Findings: the paper presents the results of the study of the structure formation during non-monotonous plastic deformation of the alloys (steel 10, copper and titanium) with various crystalline lattice types by SD, as well as ECAP and HPT of low-carbon steel in the temperature range of the DSA effect. Deformation mechanisms and features of the deformation behavior on a mesoscopic scale under various deformation treatment modes are analyzed. The temperature range of the DSA effect in steel 10 under ECAP and the fact of the gradient structure formation under HPT are established. Practical Relevance: The study helped to obtain data that can be used to choose the optimal deformation treatment mode with the DSA effect.

Recrystallization and Grain Growth in Ultra Fine Grained Materials Produced by High Pressure Torsion

2012 ◽  
Vol 715-716 ◽  
pp. 373-373
Author(s):  
Anahita Khorashadizadeh ◽  
Myrjam Winning ◽  
Stefan Zaefferer ◽  
Dierk Raabe
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Grain Growth ◽  
High Pressure Torsion ◽  
Fine Grained ◽  
Fine Grained Material

Investigations of the microstructure of materials processed via severe plastic deformation methods such as high pressure torsion (HPT) and their recrystallization behaviour is of great interest as they are capable of producing ultra fine grained material (UFD) with good mechanical properties.

Developing the Technique of Severe Plastic Deformation Processing through High-Pressure Torsion

2010 ◽  
Vol 667-669 ◽  
pp. 397-402 ◽  
Author(s):  
Megumi Kawasaki ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Severe Plastic Deformation Processing ◽  
Average Grain Size ◽  
High Purity Aluminum ◽  
Sample Characteristics ◽  
Nanoscale Range

The processing of metals through the application of severe plastic deformation provides the potential for achieving exceptional grain refinement in bulk solids. Several SPD methods are now available but processing by high-pressure torsion (HPT) has attracted much attention over the last five years. Numerous reports are now available describing the application of HPT to a range of pure metals and simple alloys and excellent grain refinement were achieved using this process with the average grain size often reduced to the nanoscale range. However, in order to make this technique more practical, the nature of the sample characteristics immediately after conventional HPT must be considered in order to understand the fundamental principles of HPT processing. This report examines the procedure with special emphasis on the evolution in hardness homogeneity in both high-purity aluminum and a Zn-22% Al eutectoid alloy processed by HPT.

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