Cyclic Softening of Cu-Ni-Si Alloy Single Crystals under Low-Cycle Fatigue

2010 ◽  
Vol 654-656 ◽  
pp. 1287-1290 ◽  
Author(s):  
Toshiyuki Fujii ◽  
Hiroshi Kamio ◽  
Yoshifumi Sugisawa ◽  
Susumu Onaka ◽  
Masaharu Kato

Cu-2.2wt%Ni-0.5wt%Si alloy single crystals were grown by the Bridgman method and aged at 723 K for 10 h to form Ni2Si precipitates. Fully reversed tension-compression fatigue tests were conducted on the aged single crystals with a single slip orientation under constant plastic-strain amplitudes at room temperature. Cyclic softening occurred at plastic-strain amplitudes between 2.5x10-4 and 2.5x10-2. Using the maximum stress amplitude in each cyclic hardening/softening curve, a pseudo cyclic stress-strain curve (CSSC) was obtained. The CSSC was found to exhibit a plateau region with a stress level of about 167 MPa. Transmission electron microscopic observation revealed the formation of persistent slip bands (PSBs) in the plateau regime. It was found that the Ni2Si precipitate particles were intensively sheared by glide dislocations within the PSBs and were eventually re-dissolved into the Cu matrix. The macroscopic cyclic softening can be attributed to the local softening induced by the re-dissolution of the Ni2Si particles in the PSBs.

2014 ◽  
Vol 891-892 ◽  
pp. 1131-1136 ◽  
Author(s):  
Tomáš Kruml ◽  
Alice Chlupová ◽  
Karel Obrtlík

Ternary TiAl alloy with 8 at.% Nb and lamellar microstructure is subjected to low cycle fatigue tests at temperatures ranging from room temperature to 800 °C. The aim of the study is to find limit conditions when the microstructure is still stable and to study mechanisms of microstructural degradation when this limit is exceeded. Up to 750 °C, no cyclic softening or hardening is observed and cyclic stress-strain curve follows the tensile curve. Cyclic softening is characteristic for 800 °C. The TEM observation did not reveal any substantial changes in the microstructure due to the cycling up to 700°C. The lamellar structure is altered by cyclic straining at 750 °C and, to a higher extent, at 800°C. In specimens cycled to fracture at 800 °C, the domains without lamellar structure cover about 10% of volume and are almost dislocation free. The destruction of lamellar microstructure is the reason for the marked cyclic softening at 800 °C.


2007 ◽  
Vol 561-565 ◽  
pp. 2213-2216
Author(s):  
Toshiyuki Fujii ◽  
Shizuma Uju ◽  
Chihiro Watanabe ◽  
Susumu Onaka ◽  
Masaharu Kato

Fully reversed tension-compression fatigue tests were performed on solid-solutioned Al-0.7mass%Mg single crystals with a single slip orientation under constant plastic-strain amplitudes. Dislocation microstructures were quantitatively examined by transmission electron microscopy. The cyclic stress–strain curve (CSSC) exhibited three distinct regions with a short plateau region in the intermediate plastic-strain amplitude range, and the plateau stress was 26MPa. Characteristic microstructures were developed corresponding to the three regions in the CSSC. Vein structure was observed at the low strain-amplitude region. In the plateau regime, the persistent slip bands (PSBs) were observed. Labyrinth structure was also observed at the higher strain-amplitude region. The plateau stress, the cyclic flow stress of PSBs, can be explained by considering not only the Orowan bowing stress and the dipole passing stress of screw dislocations but also solid-solution hardening by Mg atoms.


1970 ◽  
Vol 5 (3) ◽  
pp. 185-192 ◽  
Author(s):  
K J Miller

The effect of strain rate on the cyclic behaviour of two materials is presented. For the material that cyclically hardens (En 32B) a decrease in strain rate decreases the maximum cyclic hardening of the material, whilst for a material that cyclically softens (En 25) a decrease in the rate of deformation increases the maximum cyclic softening. It is concluded that the effect of strain rate on the cyclic stress-strain curve should be more closely studied than the effect of frequency since the frequency may be constant whilst the straining rate may vary considerably in plastically deformed zones. For those zones that suffer low strain rates the inclusion of time-dependent deformation processes can maximize the degree of softening or minimize the degree of hardening, thereby creating a greater localization of the plastic strain which should increase strain-concentration factors. Finally it is argued that it is better to predict fatigue behaviour from an incremental-step high-strain fatigue test on a single specimen than from static-test data. For the same reasons correlations between static tests and fatigue tests should be discouraged, especially for those materials that exhibit marked cyclic softening.


2016 ◽  
Vol 853 ◽  
pp. 77-82
Author(s):  
Xu Chen ◽  
Rui Si Xing ◽  
Xiao Peng Liu

Aluminium alloys are widely used in the fields of automobile, machinery and naval construction. To investigate the effect of non-proportional loadings and corrosive environment on the fatigue resistance of 6061-T6 aluminum alloy, a set of uniaxial and multiaxial low cycle fatigue tests were carried out. Firstly, the results of uniaxial tests showed that the alloy exhibited cyclic hardening then cyclic softening. With the increase of stress amplitude the cyclic softening became pronounced. The increasing of plastic deformation was basically cyclically stable with small plastic strain amplitude accumulation when the stress amplitude was lower than 200MPa ,while it was increasing rapidly when the stress amplitude was higher than 220MPa. Secondly, it was observed that non-proportional cycle additional hardening of 6061-T6 aluminum alloy was little. While the fatigue life was badly affected by the loading paths. Thirdly ,the fatigue corrosion interactions were also talked about in details by performing the tests under the same loading conditions with corrosive environment. The experiment proved that the seawater corrosion has huge impact on fatigue life under pH 3. Finally, a multi-axial fatigue life prediction model was used to predict the fatigue life with or without the corrosive environment which showed a good agreement with experimental data.


2016 ◽  
Vol 713 ◽  
pp. 86-89 ◽  
Author(s):  
Ivo Šulák ◽  
Karel Obrtlík ◽  
Ladislav Čelko

The present work is focused on the study of microstructure and low cycle fatigue behavior of the first generation nickel-base superalloy IN 713LC (low carbon) and its promising second generation successor MAR-M247 HIP (hot isostatic pressing) at 900 °C. Microstructure of both alloys was studied by means of scanning electron microscopy (SEM). The microstructure of both materials is characterized by dendritic grains, carbides and casting defects. Size and morphology of precipitates and casting defects were evaluated. Fractographic observations have been made with the aim to reveal the fatigue crack initiation place and relation to the casting defects and material microstructure. Low cycle fatigue tests were conducted on cylindrical specimens in symmetrical push-pull cycle under strain control with constant total strain amplitude and strain rate at 900 °C in air. Hardening/softening curves, cyclic stress-strain curve and fatigue life data of both materials were obtained. Cyclic stress-strain curve of MAR M247 is shifted approximately to 120 MPa higher stress amplitudes in comparison with IN 713LC. Significantly higher fatigue life of MAR-M247 has been observed in Basquin representation. On the other hand IN 713LC shows prolonged lifetime compared with MAR-M247 in the Coffin-Manson representation. Results obtained from high temperature low cycle fatigue tests are discussed.


2006 ◽  
Vol 324-325 ◽  
pp. 1241-1244 ◽  
Author(s):  
Li Xun Cai ◽  
Yu Ming Ye

A series of strain fatigue tests were carried out on small bugle-like slice-specimens of Zr-4 alloy at 20 and 400. According to Elastic and Plastic Finite Element Analysis and assumption of local damage equivalence, a strain formula was given to transform transverse strain of the specimen to uniaxial strain. Based on the test results of the alloy and the strain transform formula, M-C (Manson-Coffin) models to be used for estimating uniaxial fatigue life of Zr-4 alloy were obtained. The results show that, the alloy mainly behaves as cyclic softening at 20 and as cyclic hardening at 400, and the elevated temperature can lead serious additional fatigue damage of the alloy and the effect of the elevated temperature impairs gradually with increasing of amplitude strain. A conclusion is helpful that prediction life by using M-C model based on traditional strain transform equation is quite conservative when uniaxial strain amplitude is less than 0.5%.


2008 ◽  
Vol 378-379 ◽  
pp. 17-28 ◽  
Author(s):  
I. Alvarez-Armas ◽  
Suzanne Degallaix

The cyclic hardening–softening response, the cyclic stress–strain curve and the substructure evolution of a high nitrogen duplex stainless steel S32750 have been evaluated and the results compared with reference to low and medium nitrogen duplex stainless steels, S32205 and S32900 grades, respectively. The beneficial effects of nitrogen on the cyclic properties of most modern alloys have been analyzed in terms of the flow stress components, i.e. the internal and the effective stress.


1992 ◽  
Vol 114 (4) ◽  
pp. 390-398 ◽  
Author(s):  
T. Bui-Quoc ◽  
R. Gomuc ◽  
A. Biron

Low-cycle fatigue tests on Ti 6-4 (Ti-6Al-4V) have been carried out at 260°C under strain-controlled conditions with constant strain amplitude and increasing multistep strain levels. The results of constant strain amplitude tests were used to establish the fatigue diagram whereas the multistep tests were examined to assess the cyclic stress-strain behavior in comparison with the conventional stress-strain curve. Most of the tests were carried out under zero-to-tension conditions in the intermediatecycle range (Nf ≃ 3 x 103 to 105 cycles). The effect of prior strain cycling on the tensile properties was also investigated. The experimental data is discussed together with theoretical evaluations. In addition, microstructural examinations of the rupture surfaces have been made to show evidence on the type of crack initiation sites and on the crack propagation modes at different strain levels.


Author(s):  
Zhong Zhang ◽  
Xijia Wu

Abstract A general fatigue life equation is derived by modifying the Tanaka-Mura-Wu dislocation pile-up model for variable strain-amplitude fatigue processes, where the fatigue crack nucleation life is expressed in terms of the root mean square of plastic strain range. Low-cycle fatigue tests were conducted on an austenitic stainless steel. at 400°C and 600°C, the material exhibits continuously cyclic-hardening behaviour. The root mean square of plastic strain ranges is evaluated from the experimental data for each test condition at strain rates ranging from 0.0002/s to 0.02/s. The variable-amplitude Tanaka-Mura-Wu model is found to be in good agreement with the LCF data, which effectively proves Miner’s rule on the stored plastic strain energy basis.


2010 ◽  
Vol 638-642 ◽  
pp. 455-460 ◽  
Author(s):  
A. Rutecka ◽  
L. Dietrich ◽  
Zbigniew L. Kowalewski

The AlSi8Cu3 and AlSi7MgCu0.5 cast aluminium alloys of different composition and heat treatment were investigated to verify their applicability as cylinder heads in the car engines [1]. Creep tests under the step-increased stresses at different temperatures, and low cycle fatigue (LCF) tests for a range of strain amplitudes and temperatures were carried out. The results exhibit a significant influence of the heat treatment on the mechanical properties of the AlSi8Cu3 and AlSi7MgCu0.5. An interesting fact is that the properties strongly depend on the type of quenching. Lower creep resistance (higher strain rates) and lower stress response during fatigue tests were observed for the air quenched materials in comparison to those in the water quenched. Cyclic hardening/softening were also observed during the LCF tests due to the heat treatment applied. The mechanical properties determined during the tests can be used to identify new constitutive equations and to verify existing numerical models.


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