Precipitation Behavior of High-Nitrogen Low-Nickel Austenitic Stainless Steel at Intermediate Temperature

2012 ◽  
Vol 724 ◽  
pp. 359-362
Author(s):  
De Ning Zou ◽  
Rong Liu ◽  
Jiao Li ◽  
Kun Wu ◽  
Xiao Hua Liu
Keyword(s):  
Stainless Steel ◽  
Austenitic Stainless Steel ◽  
Grain Boundaries ◽  
Volume Fraction ◽  
Intermediate Temperature ◽  
Air Cooling ◽  
Precipitation Behavior ◽  
Lower Aging Temperature ◽  
Electron Microscopy Analysis ◽  
Microscopy Analysis

The precipitation behavior of nitrides and carbides occurred in aging process for 10Cr21Mn16NiN austenitic stainless steel at intermediate temperature was investigated by use of thermodynamic calculation, metallography and electron microscopy analysis. The precipitates evolved from chain-like initiatively along grain boundaries at lower aging temperature, to that along grain boundaries and inside the grain of austenite with more content as the temperature rising gradually. When aging at 800 °C, precipitates became layered tablet shaped and the composition was ascertained the mixture of Cr2N and M23C6. At a certain temperature, the volume fraction of precipitates for the aged testing steel by air cooling was slightly higher than that by water quenching.

Precipitation Behavior in AL6XN Austenitic Stainless Steel

2010 ◽  
Vol 654-656 ◽  
pp. 2330-2333 ◽  
Author(s):  
Li Jun Meng ◽  
Hui Xing ◽  
Jian Sun
Keyword(s):  
Stainless Steel ◽  
Electron Microscope ◽  
Austenitic Stainless Steel ◽  
Electron Diffraction ◽  
Grain Boundaries ◽  
Electron Diffraction Pattern ◽  
Precipitation Behavior ◽  
Laves Phases ◽  
X Ray ◽  
Creep Temperature

The precipitation behavior in the AL6XN austenitic stainless steel after creep deformation at temperatures 500~750 °C up to 3600 hours has been studied by electron microscope. The results showed that precipitates were hardly observed for the steel crept at 500~550 °C, and that the precipitates of carbides were mainly found at grain boundaries in samples crept at 600 °C. When the creep temperature was increased to 650~750 °C, a high density precipitates was found both at grain boundaries and within grains. The electron diffraction pattern and energy-dispersive X-ray spectroscopy analyses confirmed that these precipitates are  and Laves phases.

Magnetic Characterization of SUS316L Deformed by High Pressure Torsion

2011 ◽  
Vol 239-242 ◽  
pp. 1300-1303
Author(s):  
Hong Cai Wang ◽  
Minoru Umemoto ◽  
Innocent Shuro ◽  
Yoshikazu Todaka ◽  
Ho Hung Kuo
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Stainless Steel ◽  
Phase Transformation ◽  
Austenitic Stainless Steel ◽  
Volume Fraction ◽  
High Pressure Torsion ◽  
Austenitic Matrix ◽  
Magnetic Characterization

SUS316L austenitic stainless steel was subjected to severe plastic deformation (SPD) by the method of high pressure torsion (HPT). From a fully austenitic matrix (γ), HPT resulted in phase transformation from g®a¢. The largest volume fraction of 70% a¢ was obtained at 0.2 revolutions per minute (rpm) while was limited to 3% at 5rpm. Pre-straining of g by HPT at 5rpm decreases the volume fraction of a¢ obtained by HPT at 0.2rpm. By HPT at 5rpm, a¢®g reverse transformation was observed for a¢ produced by HPT at 0.2rpm.

Effects of Deformation Mode on Resistivity Curve Used for Estimating Martensite Induced in Stainless Steel

2010 ◽  
Vol 638-642 ◽  
pp. 2992-2997 ◽  
Author(s):  
Hidefumi Date
Keyword(s):  
Stainless Steel ◽  
Austenitic Stainless Steel ◽  
Linear Relation ◽  
Volume Fraction ◽  
Tensile Deformation ◽  
Deformation Mode ◽  
Transformation Process ◽  
Martensite Formation ◽  
Austenitic Phase ◽  
Ε Phase

The martensite induced in three types of austenitic stainless steel, which indicate the different stability of the austenitic phase (γ), were estimated by the resistivity measured during the tensile deformation or compressive deformation at the temperatures 77, 187 and 293 K. The resistivity curves were strongly dependent on the deformation mode. The volume fraction of the martensite (α’) was also affected by the deformation mode. The ε phase, which is the precursor of the martensite and is induced from the commencement of the deformation, decreased the resistivity. However, lots of defects generated by the deformation-induced martensite increased the resistivity. The experimental facts and the results shown by the modified parallelepiped model suggested a complicated transformation process depending on each deformation mode. The results shown by the model also suggested a linear relation between the resistivity and the martensite volume at the region of the martensite formation. The fact denoted that the resistivity is mostly not controlled by the austenite, ε phase and martensite, but by the defects induced due to the deformation-induced martensite.

scholarly journals Surface Modification of a Nickel-Free Austenitic Stainless Steel by Low-Temperature Nitriding

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1845
Author(s):  
Francesca Borgioli ◽  
Emanuele Galvanetto ◽  
Tiberio Bacci
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Austenitic Stainless Steel ◽  
Low Temperature ◽  
Stainless Steels ◽  
Volume Fraction ◽  
Surface Hardness ◽  
Austenitic Stainless Steels ◽  
Surface Layers ◽  
Modified Surface

Low-temperature nitriding allows to improve surface hardening of austenitic stainless steels, maintaining or even increasing their corrosion resistance. The treatment conditions to be used in order to avoid the precipitation of large amounts of nitrides are strictly related to alloy composition. When nickel is substituted by manganese as an austenite forming element, the production of nitride-free modified surface layers becomes a challenge, since manganese is a nitride forming element while nickel is not. In this study, the effects of nitriding conditions on the characteristics of the modified surface layers obtained on an austenitic stainless steel having a high manganese content and a negligible nickel one, a so-called nickel-free austenitic stainless steel, were investigated. Microstructure, phase composition, surface microhardness, and corrosion behavior in 5% NaCl were evaluated. The obtained results suggest that the precipitation of a large volume fraction of nitrides can be avoided using treatment temperatures lower than those usually employed for nickel-containing austenitic stainless steels. Nitriding at 360 and 380 °C for duration up to 5 h allows to produce modified surface layers, consisting mainly of the so-called expanded austenite or gN, which increase surface hardness in comparison with the untreated steel. Using selected conditions, corrosion resistance can also be significantly improved.

The Microstructure and Creep Behavior of Cold Rolled Udimet 188 Sheet

2010 ◽  
Vol 17 (3) ◽  
pp. 350-361
Author(s):  
C.J. Boehlert ◽  
S.C. Longanbach
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Creep Behavior ◽  
Volume Fraction ◽  
Solution Treatment ◽  
Tensile Creep ◽  
Dislocation Creep ◽  
Grain Boundary Character Distribution ◽  
Air Cooling ◽  
Cold Rolled

AbstractUdimet 188 was subjected to thermomechanical processing (TMP) in an attempt to understand the effects of cold-rolling deformation on the microstructure and tensile-creep behavior. Commercially available sheet was cold rolled to varying amounts of deformation (between 5–35% reduction in sheet thickness) followed by a solution treatment at 1,464 K (1,191°C) for 1 h and subsequent air cooling. This sequence was repeated four times to induce a high-volume fraction of low-energy grain boundaries. The resultant microstructure was characterized using electron backscattered diffraction. The effect of the TMP treatment on the high-temperature [1,033–1,088 K (760–815°C)] creep behavior was evaluated. The measured creep stress exponents (6.0–6.8) suggested that dislocation creep was dominant at 1,033 K (760°C) for stresses ranging between 100–220 MPa. For stresses ranging between 25–100 MPa at 1,033 K (760°C), the stress exponents (2.3–2.8) suggested grain boundary sliding was dominant. A significant amount of grain boundary cracking was observed both on the surface and subsurface of deformed samples. To assess the mechanisms of crack nucleation, in situ scanning electron microscopy was performed during the elevated-temperature tensile-creep deformation. Cracking occurred preferentially along general high-angle grain boundaries (GHAB) and less than 25% of the cracks were found on low-angle grain boundaries (LAB) and coincident site lattice boundaries (CSLB). Creep rupture experiments were performed at T = 1,088 K (815°C) and σ = 165 MPa and the greatest average time-to-rupture was exhibited by the TMP sheet with the greatest fraction of LAB+CSLB. However, a clear correlation was not exhibited between the grain boundary character distribution and the minimum creep rates. The findings of this work suggest that although grain boundary engineering may be possible for this alloy, simply relating the fraction of grain boundary types to the creep resistance is not sufficient.

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