Hot Deformation Behavior and Microstructural Evolution of Mg-Nd-Zn-Zr Magnesium Alloy

2013 ◽  
Vol 747-748 ◽  
pp. 320-326 ◽  
Author(s):  
Wen Xiang Wu ◽  
Li Jin ◽  
Jie Dong ◽  
Zhen Yan Zhang ◽  
Wen Jiang Ding

The hot deformation behaviors and microstructural evolution of Mg-3.0Nd-0.2Zn-0.4Zr (wt. %, NZ30K) alloy were investigated by means of the isothermal hot compression tests at temperatures of 350-500 °C with strain rates of 0.001, 0.01, 0.1 and 1s-1. The results showed that the flow stress increased to a peak and then decreased which showed a dynamic flow softening. The flow stress behavior was described by the hyperbolic sine constitutive equation with an average activation energy of 193.8 kJ/mol. The average size of dynamically recrystallized grains of hot deformed NZ30K alloy was reduced by increasing the strain rate and/or decreasing the deformation temperature. A large amount of fine particles precipitated in the grains interior and at the grain boundaries when heated to the compression temperatures and soaked for 5min below 450 °C. However, the volume fraction of particles decreased significantly when soaked for 5 min at 500 °C, and the coarse particles precipitated mainly at the grain boundaries. Hot deformation at the temperature of 500 °C around and at the strain rate range of 0.1s-1 was desirable for NZ30K alloy.

2015 ◽  
Vol 816 ◽  
pp. 810-817
Author(s):  
Yong Biao Yang ◽  
Zhi Min Zhang ◽  
Xing Zhang

The hot deformation behaviors of Aluminum alloy C919 were studied in the present investigation. The hot compression tests for C919 were carried out in the temperature range of 350°C~470°C and strain rates range of 0.001s-1~1s-1 using GLEEBLE-1500 thermal simulate testing machine. Optical microscopy (OM) was used for the microstructure characterization. The experimental results showed that the flow stress of C919 aluminum alloy decreased with increasing temperature and decreasing strain rates and the flow stress curves tended to increase at a strain rate of 1s-1 with increasing strain, while the flow stresses kept with increasing strain at lower strain rate. The alloys were more prone to dynamic recrystallization with decreasing strain rates during hot deformation. The hot compression behavior of C919 aluminum alloy can be described as hyperbolic sine function corrected Arrhenius relation. The processing maps for the alloy were built at a strain of 0.6. The instability deformation domain occurred at temperatures range from 350°C and 380°C and at a strain rate of 0.1-1s-1. Based on the processing maps and microstructure observations, the optimum hot-working parameters were determined to be at a temperature of 470°C in the strain rate range from 0.1-0.01s−1 for the C919 aluminum alloy.


2016 ◽  
Vol 35 (3) ◽  
pp. 327-336 ◽  
Author(s):  
Sendong Gu ◽  
Liwen Zhang ◽  
Chi Zhang ◽  
Wenfei Shen

AbstractThe hot deformation characteristics of nickel-based alloy Nimonic 80A were investigated by isothermal compression tests conducted in the temperature range of 1,000–1,200°C and the strain rate range of 0.01—5 s–1on a Gleeble-1500 thermomechanical simulator. In order to establish the constitutive models for dynamic recrystallization (DRX) behavior and flow stress of Nimonic 80A, the material constantsα,nand DRX activation energyQin the constitutive models were calculated by the regression analysis of the experimental data. The dependences of initial stress, saturation stress, steady-state stress, dynamic recovery (DRV) parameter, peak strain, critical strain and DRX grain size on deformation parameters were obtained. Then, the Avrami equation including the critical strain for DRX and the peak strain as a function of strain was established to describe the DRX volume fraction. Finally, the constitutive model for flow stress of Nimonic 80A was developed in DRV region and DRX region, respectively. The flow stress values predicted by the constitutive model are in good agreement with the experimental ones, which indicates that the constitutive model can give an accurate estimate for the flow stress of Nimonic 80A under the deformation conditions.


Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1277 ◽  
Author(s):  
Guoqing Dai ◽  
Yuwen Cui ◽  
Danying Zhou ◽  
Yanhua Guo ◽  
Hui Chang ◽  
...  

The isothermal hot compression behavior of new Ti–Fe–B (named as TF400) alloy was investigated in the temperature range of 750–950 °C and strain rate range from 0.01 to 10 s−1 with the maximum height reduction of 60% by using a Gleeble 3800 thermal simulator. By considering the effect of strain via variable material parameters, a modified constitutive model was proposed to accurately predict the flow stress. The predicted results demonstrate that the flow stress decreases with the increase of temperature while it increases as the strain rate increases, in good agreement with the present experimental results. A mechanistic understanding of plastic deformation behavior in the TF400 alloys was developed by inspecting the microstructural characteristics prior to and after deformations. Dynamic recrystallization and dynamic transformation were found to be the dominant restoration mechanism during the hot deformation process.


2014 ◽  
Vol 1058 ◽  
pp. 165-169 ◽  
Author(s):  
Shi Ming Hao ◽  
Jing Pei Xie

The hot deformation behaviors of 30%SiCp/2024 aluminum alloy composites was studied by hot compression tests using Gleeble-1500 thermomechanical simulator at temperatures ranging from 350-500°C under strain rates of 0.01-10 s-1. The true stress-true strain curves were obtained in the tests. Constitutive equation and processing map were established. The results show that the flow stress decreases with the increase of deformation temperature at a constant strain rate, and increases with the increase of strain rate at constant temperature, indicating that composite is a positive strain rate sensitive material. The flow stress behavior of composite during hot compression deformation can be represented by a Zener-Hollomon parameter in the hyperbolic sine form. Its activation energy for hot deformation Q is 183.251 kJ/mol. The optimum hot working conditions for this material are suggested.


2013 ◽  
Vol 709 ◽  
pp. 143-147 ◽  
Author(s):  
Tao Wang ◽  
Zhao Li ◽  
Shu Hong Fu ◽  
Yong Zhang ◽  
Yu Xin Zhao ◽  
...  

The hot deformation behavior of U720Li was investigated by isothermal compression tests at temperature ranging from 1060-1180°C and strain rate from 0.001s-1 to 20s-1. The flow stress-strain curves and microstructures were investigated and a constitutive equation was established. It is found that flow stress is sensitive to stain rate and deformation temperature greatly. The higher stain rate resultes in a larger fluctuation in flow stress. The hot deformation activation energy is determined to be 552.8kJ/mol. Grain size increases with increasing temperature and decreases firstly and then increases with increasing strain rate. U720Li alloy should be deformed below the solve temperature of γ primary phase with lower strain rate in order to obtain the even and fine grain size.


2019 ◽  
Vol 51 (1) ◽  
pp. 467-481
Author(s):  
Suwaree Chankitmunkong ◽  
Dmitry G. Eskin ◽  
Chaowalit Limmaneevichitr

Abstract Aluminum piston alloys of the AA4032 type are produced by direct-chill (DC) casting and subsequent forging; therefore, it is important to understand their thermomechanical behavior. In recent years, it was shown that additions of Cu and Er could improve mechanical properties of these alloys at room and high temperatures. In this work, we studied the constitutive behavior of AA4032-type alloys with and without Cu and Er additions. The experimental true stress–true strain curves were obtained by compression tests under various temperatures [683 K to 723 K (410 °C to 450 °C)] and strain rates (0.01 to 10 s−1) to determine constitutive parameters [strain-rate sensitivity, activation energy, and Zener–Hollomon (Z) parameter] for the hot deformation behavior of AA4032-type piston alloys with and without additions of Cu and Er. The flow stress decreased with increasing deformation temperature and decreasing strain rate. The results also showed that increasing the Cu content increased the flow stress over the applied range of deformation conditions due to solid-solution strengthening and the formation of primary Si particles, which led to an increase in the activation energy during hot deformation. Moreover, the main microstructural damage in the AA4032 alloy with 3.5 pct Cu was predominantly due to the cracking of primary Si particles. Additions of 0.4 pct Er and 3.5 pct Cu lower the activation energy of deformation, Q, as compared to the base alloy and the alloy with 3.5 pct Cu. The microstructures in the deformed specimens consisted of subgrains, recrystallized grains, and fine eutectic phases. The alloys containing Er demonstrated more polygonized grains at a low strain rate than the alloys without Er, indicating that Er hindered recrystallization development. The peak stress of the AA4032 alloy with 3.5 pct Cu alloy was higher than for the base AA4032 alloy and for the AA4032 alloy with 3.5 pct Cu and 0.4 pct Er additions, which was attributed to the prevalence of the work-hardening mechanism over the softening mechanism.


2013 ◽  
Vol 17 (5) ◽  
pp. 1523-1528
Author(s):  
Bao-Hua Jia ◽  
Wei-Dong Song ◽  
Hui-Ping Tang ◽  
Jian-Guo Ning

Isothermal compression tests of TC18 titanium alloy at the deformation temperatures ranging from 25?C to 800?C and strain rate ranging from 10-4 to 10-2 s-1 were conducted by using a WDW-300 electronic universal testing machine. The hot deformation behavior of TC18 was characterized based on an analysis of the true stress-true strain curves of TC18 titanium alloy. The curves show that the flow stress increases with increasing the strain rate and decreases with increasing the temperature, and the strain rate play an important role in the flow stress when increasing the temperatures. By taking the effect of strain into account, an improved constitutive relationship was proposed based on the Arrhenius equation. By comparison with the experimental results, the model prediction agreed well with the experimental data, which demonstrated the established constitutive relationship was reliable and can be used to predict the hot deformation behavior of TC18 titanium alloy.


2017 ◽  
Vol 898 ◽  
pp. 137-143
Author(s):  
Lin Xiang ◽  
Bin Tang ◽  
Hong Chao Kou ◽  
Jie Shao ◽  
Jin Shan Li

Isothermal compression tests were conducted to investigate the effect of hot deformation parameters on flow behavior and microstructure of Ti-6Al-4V-0.2O alloy. The experimental results show that the strain rate and height reduction have little effect on the volume fraction of primary α at a deformation temperature of 860 ̊C. At a deformation temperature of 940 ̊C, the volume fraction of primary α at a high strain rate (10s-1) is about 10% less than that at low strain rates (0.01s-1~1s-1). It may be one of the reasons for the significantly discontinuous yielding phenomenon. Another reason is that the dislocation density decreased suddenly due to the dynamic recovery. With the increasing strain rate and the decreasing deformation temperature, the volume fraction of irregular secondary α increases and lamellar secondary α decreases. And with height reduction increasing, the irregular secondary α increases firstly and then tends to be steady because of dynamic recovery and recrystallization.


2013 ◽  
Vol 652-654 ◽  
pp. 1080-1083
Author(s):  
Chun Xia Wang ◽  
Fu Xiao Yu ◽  
Da Zhi Zhao ◽  
Xiang Zhao ◽  
Liang Zuo

The deformation behavior of DC cast Al-2Si and Al-15Si alloys have been studied by means of compression test at temperature range of 300-500°C and strain rate range of 0.01-5 s-1. The results show that the flow stress of the Al-Si alloys increases with decreasing compression temperature and increasing strain rate. The flow curves determined from the compression tests exhibit that the deformation of the materials is controlled by two competing mechanisms: strain hardening and flow softening. Higher silicon content in the alloys also leads to higher flow stress during deformation and tend to show more significant flow softening. Particle damage during the deformation may have an influence on the flow curves of the alloys.


2018 ◽  
Vol 37 (1) ◽  
pp. 75-87
Author(s):  
Jun Cai ◽  
Kuaishe Wang ◽  
Jiamin Shi ◽  
Wen Wang ◽  
Yingying Liu

AbstractConstitutive analysis for hot working of BFe10-1-2 alloy was carried out by using experimental stress–strain data from isothermal hot compression tests, in a wide range of temperature of 1,023~1,273 K, and strain rate range of 0.001~10 s–1. A constitutive equation based on modified double multiple nonlinear regression was proposed considering the independent effects of strain, strain rate, temperature and their interrelation. The predicted flow stress data calculated from the developed equation was compared with the experimental data. Correlation coefficient (R), average absolute relative error (AARE) and relative errors were introduced to verify the validity of the developed constitutive equation. Subsequently, a comparative study was made on the capability of strain-compensated Arrhenius-type constitutive model. The results showed that the developed constitutive equation based on modified double multiple nonlinear regression could predict flow stress of BFe10-1-2 alloy with good correlation and generalization.


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