Thermal Shock Resistance of Liquid Phase Sintered SiC

2016 ◽  
Vol 881 ◽  
pp. 103-108
Author(s):  
Roberta Monteiro de Mello ◽  
Ana Helena de Almeida Bressiani
Keyword(s):  
Silicon Carbide ◽  
Liquid Phase ◽  
Thermal Shock ◽  
Water Samples ◽  
Thermal Cycle ◽  
Thermal Shock Resistance ◽  
Sintering Temperature ◽  
Shock Resistance

The aim of this study was to evaluate the effect of Y2O3:Al2O3 additives and sintering temperature on thermal shock resistance of silicon carbide sintered via liquid phase. Silicon carbide samples containing 10 mol% Y2O3:Al2O3 (1:3 and 1:4) were prepared, compacted and sintered at 1750, 1850 and 1950 °C in a graphite resistive furnace. Thermal shock resistance was evaluated after each thermal cycle performed at 600, 750 and 900 °C followed by abrupt cooling in water. Samples with two Y2O3:Al2O3 proportions did not show major differences when sintered at the same temperature, though, rising the sintering temperature improves Y2O3:Al2O3 modified-SiC thermal shock resistance.

Preparation of ZrO2 Composite Ceramics with High Thermal Shock Resistance

2012 ◽  
Vol 455-456 ◽  
pp. 650-654 ◽  
Author(s):  
He Yi Ge ◽  
Jian Ye Liu ◽  
Xian Qin Hou ◽  
Dong Zhi Wang
Keyword(s):  
Mechanical Properties ◽  
Water Absorption ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Sintering Temperature ◽  
Fiber Composite ◽  
Physical And Mechanical Properties ◽  
Composite Ceramics ◽  
Shock Resistance ◽  
Absorption Measurements

The physical and mechanical properties of nanometer ZrO2-ZrO2fiber composite ceramics were studied by introduction of ZrO2fiber. ZrO2composite ceramics at different sintering temperature was investigated by porosity and water absorption measurements, flexual strength and thermal shock resistance analysis. Results showed that ZrO2composite ceramics containing 15 wt% ZrO2fiber with sintering temperature of 1650°C exhibited good mechanical properties and thermal shock resistance. The porosity and the water absorption were 8.84% and 1.62%, respectively. The flexual strength was 975 MPa and the thermal shock times reached 31 times. Scanning electron microscope (SEM) was used to analyze the microstructure of ZrO2composite ceramics.

Thermal Shock Resistance of ZrO2 Fiber/Al2O3 Ceramics

2011 ◽  
Vol 306-307 ◽  
pp. 754-757 ◽  
Author(s):  
Xian Qin Hou ◽  
Jian Ye Liu ◽  
He Yi Ge
Keyword(s):  
Mechanical Properties ◽  
Electron Microscope ◽  
Water Absorption ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Sintering Temperature ◽  
Physical And Mechanical Properties ◽  
Shock Resistance ◽  
Scanning Electron ◽  
Absorption Measurements

The physical and mechanical properties of alumina (Al2O3) ceramics by introduction of zirconia (ZrO2) fiber were studied. ZrO2/Al2O3ceramics at different sintering temperature was investigated by porosity and water absorption measurements, flexual strength and thermal shock resistance analysis. Results showed that Al2O3 ceramics containing 15 wt% ZrO2fiber with sintering temperature of 1650°C exhibited good mechanical properties and thermal shock resistance. The porosity and water absorption were 7.4% and 0.69%, respectively. The flexual strength was 613 MPa and the thermal shock times reached 29 times. Scanning electron microscope (SEM) was used to analyze the microstructure of Al2O3 ceramics.

Influence of Zircon Addition on Thermal Shock Resistance of ZTA for Plasma Reactors

2007 ◽  
Vol 544-545 ◽  
pp. 379-382
Author(s):  
Kyung Hun Jang ◽  
Bum Rae Cho
Keyword(s):  
Thermal Expansion ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Sintering Temperature ◽  
Plasma Reactors ◽  
Alumina Ceramics ◽  
Low Thermal Expansion ◽  
Resultant Data ◽  
Shock Resistance ◽  
Zirconia Toughened Alumina

The effect of CaO, MgO and SiO2 as a flux on the sinterability of zirconia toughened alumina(ZTA) used for plasma reactors was investigated and the effect of zircon addition on thermal shock resistance of ZTA with 15wt.% of ZrO2 was also investigated. The resultant data revealed that ZTA shows the best sinterability at the composition of 2wt.% of CaO, 4wt.% of MgO and 2wt.% of SiO2 and at the sintering temperature of 1350°C. Thermal shock resistance of ZTA containing zircon was improved significantly. It is shown that ZTA containing 10wt.% of zircon shows better thermal shock resistance than others. This fact can be explained due to the low thermal expansion coefficient of zircon. It was concluded that zircon is an effective material to improve thermal shock resistance of alumina ceramics.

Influence of Additives on Performance of Silicon Carbide Refractory

2012 ◽  
Vol 538-541 ◽  
pp. 2277-2280
Author(s):  
You Fu Guo ◽  
Ming Yue Zheng ◽  
Jing Long Bu ◽  
Yue Jun Chen ◽  
Li Xue Yu ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Thermal Expansion ◽  
Bulk Density ◽  
Thermal Shock ◽  
Silica Fume ◽  
Thermal Shock Resistance ◽  
Bending Strength ◽  
Carbide Refractory ◽  
Shock Resistance ◽  
Silicon Carbide Refractory

Silicon carbide with diffierent granularity was used as raw material, quartz, silica fume, aluminum powder or alumina was used as additive with dosages of 1% (in mass, similarly hereinafter), 3% and 5%. Silicon carbide refractory material was prepared in oxidizing atmosphere at 1400 °C for 3 h. Performence of samples were researched by measurements of apparent porosity, bulk density, bending strength at room temperature, thermal shock resistance and thermal expansion rate, and analyzed by SEM. The results showed that samples added silica fume have low thermal expansion rate and apparent porosity, high bending strength and bulk density, good thermal shock resistance, compact texture as well. It can be deduced that 5% silica fume plays the excellent role to improve integrated performance of silicon carbide refractory material.

Thermal shock resistance and hoop strength of triplex silicon carbide composite tubes

2017 ◽  
Vol 14 (6) ◽  
pp. 1069-1076 ◽  
Author(s):  
Daejong Kim ◽  
Donghee Lee ◽  
Sanghwan Lee ◽  
Kwangheon Park ◽  
Hyeon-Geun Lee ◽  
...  
Keyword(s):  
Silicon Carbide ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Composite Tubes ◽  
Carbide Composite ◽  
Shock Resistance

Research of Thermal Shock Resistance of Si3N4 and SiC

2012 ◽  
Vol 549 ◽  
pp. 691-694
Author(s):  
Fang Zhang ◽  
Zhi Liang Huang
Keyword(s):  
Bulk Density ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Silicon Powder ◽  
Nitrogen Atmosphere ◽  
Production Practice ◽  
Shock Resistance ◽  
Powder Content

The study is carried out combing with the production practice in Danjiangkou Hongyuan SiC limited. Si3N4 and SiC were prepared successfully from SiC and Silicon power in nitrogen atmosphere at 1425°C and 1375°C sintering temperature by the serial of techniques, such as ingredients, mixing, molding and drying, respectively. In the actual production, silicon powder content and sintering temperature will directly influence the products of the bending strength and thermal shock resistance. By measuring bending strength, porosities, bulk density, XRD and FESEM, the bending strength and thermal shock resistance of samples were studied mainly by changing sintering temperature and silicon powder content. The results show that bending strength and thermal shock resistance of sample which was added 16% Si powder is best. And bending strength and thermal shock resistance of sample of 1425°C sintering temperature is higher than that of 1375°C sintering temperature.

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