Grain Refinement of AZ61 Alloy after ECAP Processing

2017 ◽  
Vol 891 ◽  
pp. 372-376 ◽  
Author(s):  
Ondřej Hilšer ◽  
Stanislav Rusz ◽  
Wojciech Maziarz ◽  
Robert Chulist ◽  
Jan Dutkiewicz ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
Grain Boundaries ◽  
Two Phase ◽  
Ecap Processing ◽  
The Third ◽  
Az61 Alloy ◽  
Solid Solution Matrix ◽  
Microscopy Techniques ◽  
Electron Back Scattered Diffraction ◽  
Solution Matrix

Electron microscopy techniques were used to characterize the microstructure and deformation behavior of AZ61 alloy proceeded by ECAP. The commercial AZ61 alloy subjected to severe plastic deformation possesses a two-phase microstructure consisting of solid solution matrix and massive γ-phase Mg17Al12, or Mg17(Al,Zn)12 distributed mostly at grain boundaries. Based on selected area diffraction and electron back scattered diffraction applied to a sample after the third pass, it can be concluded that plastic deformation induced by ECAP occurs mainly by slip mode forming a high density network of dislocation inside the grains. The grains size was significantly refined to 1.4 μm after the third pass of ECAP. The refinement of grain size is probably due to polygonization process associated with formation of high angle grain boundaries due to dislocations rearrangement. (Al, Zn)12Mg17 precipitates of size scattered from 100 to 200 nm and also the primary precipitates of Al6Mn phase were observed in this alloy.

Precipitation in Partially-Stabilized Zirconia

1976 ◽  
Vol 34 ◽  
pp. 628-629
Author(s):  
D. L. Porter ◽  
A. H. Heuer
Keyword(s):  
Phase Region ◽  
Precipitate Size ◽  
Tetragonal Symmetry ◽  
Stabilized Zirconia ◽  
Two Phase ◽  
Slow Cooling ◽  
Partially Stabilized Zirconia ◽  
Large Particles ◽  
Solid Solution Matrix ◽  
Solution Matrix

Precipitation in commercial partially-stabilized zirconia (PSZ) has been studied in order to facilitate "alloy design" in these materials. The commercial material used in this study is a 2.8 wt. % MgO alloy and has the cubic flourite structure at its sintering temperature. Upon cooling, a nearly MgO-free ZrO2 phase with tetragonal symmetry precipitates, which on further cooling inverts martensitically to a phase with monoclinic symmetry. At room temperature, commercial PSZ's therefore consist of a cubic solid solution matrix containing monoclinic precipitate; size, morphology, and distribution of the precipitate phase strongly influence mechanical properties.Figures I and II show typical microstructures of the material as it is commercially produced. Both large and small precipitates are present (Figure I), indicative of precipitation over a range of temperatures during slow cooling through the two-phase region. Figure II shows heavily-twinned monoclinic particle; such large particles produced during commercial fabrication are believed to be deleterious to the mechanical behavior.

Phase equilibrium between bcc solid solution matrix and B2 aluminides in Nb-based alloy

2015 ◽  
Vol 1760 ◽  
Author(s):  
Takuya Yamanouchi ◽  
Seiji Miura
Keyword(s):  
Solid Solution ◽  
Phase Equilibrium ◽  
Phase Field ◽  
Composition Range ◽  
Basic Information ◽  
Two Phase ◽  
Nial Phase ◽  
Solid Solution Matrix ◽  
Solution Matrix

ABSTRACTB2 aluminides have a role of Al reservoir for Al2O3 surface and it is expected to increase oxidation resistance of (Nb,Mo)-bccss substrate. For the accumulation of the basic information to design the alloy composed of B2 coating on bccss matrix, bccss - B2 two-phase field was investigated in the Nb-Mo-Ni-Pd-Al system at 1273 K. It is found that Pd-rich B2-(Ni,Pd)Al phase is in equilibrium with Nb-rich bccss phase, while without Pd, the composition range of bccss coexisting with B2-NiAl phase is limited to be low Nb.

Crack Growth Behavior in a Two-Phase Mo-Si-B Alloy

2006 ◽  
Vol 980 ◽  
Author(s):  
Sharvan Kumar ◽  
Amruthavalli Pallavi Alur
Keyword(s):  
Cyclic Loading ◽  
Crack Growth ◽  
Maximum Stress ◽  
Crack Tip ◽  
Growth Behavior ◽  
Crack Growth Behavior ◽  
Two Phase ◽  
Creep Cavitation ◽  
Solid Solution Matrix ◽  
Solution Matrix

AbstractMo-rich Mo-Si-B multiphase alloys are currently being explored for their potential as high-temperature structural materials for components in hot sections in aircraft engines. In this paper, we present crack growth behavior in one such two-phase alloy consisting of a Mo solid solution matrix in which is dispersed approximately 40 volume percent of the Mo5SiB2 (T2) phase. Crack growth under monotonic and cyclic loading is considered over a temperature range spanning 20°C to 1400°C. The effects of loading rate (in monotonic loading) and dwell times at maximum stress (in cyclic loading) at high temperatures on crack growth were examined to understand the contribution from creep. Results confirm a gradual increase in fracture toughness upto 1000°C, beyond which the increase is more substantial with temperature; fatigue susceptibility was also observed in excess of 900°C and crack-tip-stresses-driven microstructural instability is evident at 1400°C. At this temperature, slow loading rates or dwell times at maximum stress lead to crack-tip recrystallization and creep cavitation that together degrade the material's properties.

Dependence of Intergranular Fracture on Boundary Topography and Cohesion

1973 ◽  
Vol 31 ◽  
pp. 150-151
Author(s):  
J. E. Doherty ◽  
A. F. Giamei ◽  
B. H. Kear ◽  
C. W. Steinke
Keyword(s):  
Grain Boundary ◽  
Room Temperature ◽  
Nickel Base Superalloy ◽  
Boundary Shear ◽  
Room Temperature Ductility ◽  
Solid Solution Matrix ◽  
Nickel Base ◽  
Solution Matrix ◽  
Different Levels ◽  
Base Superalloy

Recently we have been investigating a class of nickel-base superalloys which possess substantial room temperature ductility. This improvement in ductility is directly related to improvements in grain boundary strength due to increased boundary cohesion through control of detrimental impurities and improved boundary shear strength by controlled grain boundary micros true tures.For these investigations an experimental nickel-base superalloy was doped with different levels of sulphur impurity. The micros tructure after a heat treatment of 1360°C for 2 hr, 1200°C for 16 hr consists of coherent precipitates of γ’ Ni3(Al,X) in a nickel solid solution matrix.

Simulation of Two Phase Flow Dynamics in Flexible Riser Exit Geometries for Oil and Gas Applications

2018 ◽  
Vol 39 ◽  
pp. 1-13
Author(s):  
Ikpe E. Aniekan ◽  
Owunna Ikechukwu ◽  
Satope Paul
Keyword(s):  
Oil And Gas ◽  
Two Phase Flow ◽  
Flow Analysis ◽  
Computational Cost ◽  
Maximum Velocity ◽  
Oil Well ◽  
Phase Flow ◽  
Two Phase ◽  
The Third ◽  
Riser Pipe

Four different riser pipe exit configurations were modelled and the flow across them analysed using STAR CCM+ CFD codes. The analysis was limited to exit configurations because of the length to diameter ratio of riser pipes and the limitations of CFD codes available. Two phase flow analysis of the flow through each of the exit configurations was attempted. The various parameters required for detailed study of the flow were computed. The maximum velocity within the pipe in a two phase flow were determined to 3.42 m/s for an 8 (eight) inch riser pipe. After thorough analysis of the two phase flow regime in each of the individual exit configurations, the third and the fourth exit configurations were seen to have flow properties that ensures easy flow within the production system as well as ensure lower computational cost. Convergence (Iterations), total pressure, static pressure, velocity and pressure drop were used as criteria matrix for selecting ideal riser exit geometry, and the third exit geometry was adjudged the ideal exit geometry of all the geometries. The flow in the third riser exit configuration was modelled as a two phase flow. From the results of the two phase flow analysis, it was concluded that the third riser configuration be used in industrial applications to ensure free flow of crude oil and gas from the oil well during oil production.

Microstructural Design of an AlMgSi Alloy via ECAP Processing: An Advanced SPD Manufacturing Technique for NC/UFG Materials

2015 ◽  
Vol 1114 ◽  
pp. 143-148
Author(s):  
Nicolae Serban ◽  
Doina Răducanu ◽  
Vasile Danut Cojocaru ◽  
Nicolae Ghiban
Keyword(s):  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Grain Refinement ◽  
Shape Change ◽  
Large Strain ◽  
Metallographic Analysis ◽  
Cross Sectional ◽  
Ecap Processing ◽  
Microstructural Design ◽  
Almgsi Alloy

Severe plastic deformation (SPD) has received enormous interest over the last two decades as a method capable of producing fully dense and bulk ultra-fine grained (UFG) and nanocrystalline (NC) materials. Significant grain refinement obtained by SPD leads to improvement of mechanical, microstructural and physical properties. Compared to classical deformation processes, the big advantage of SPD manufacturing techniques, represented in particular by equal channel angular pressing (ECAP) is the lack of shape-change deformation and the consequent possibility to impart extremely large strain. In ECAP processing, the workpiece is pressed through a die in which two channels of equal cross-section intersect at an angle of ϕ and an additional angle of ψ define the arc of curvature at the outer point of intersection of the two channels. As a result of pressing, the sample theoretically deforms by simple shear and retains the same cross-sectional area to allow repeated pressings for several cycles. A commercial AlMgSi alloy was investigated in our study. The specimens were processed at room temperature for multiple passes, using three different ECAP dies. All samples (ECAP processed and as-received) were subjected to metallographic analysis and mechanical testing. Several correlations between the main processing parameters and the resulting microstructural aspect and mechanical features for the processed material were established. It was shown that severe plastic deformation by means of ECAP processing can be used in aluminum alloys microstructural design as an advanced tool for grain refinement in order to attain the desired microstructure and mechanical properties.

Microstructure and Texture Evolution in Nickel during Accumulative Roll Bonding

2016 ◽  
Vol 879 ◽  
pp. 454-458 ◽  
Author(s):  
Jia Qi Duan ◽  
Md Zakaria Quadir ◽  
Michael Ferry
Keyword(s):  
Grain Boundaries ◽  
Accumulative Roll Bonding ◽  
Texture Evolution ◽  
Shear Bands ◽  
Rolling Direction ◽  
Sample Surface ◽  
Deformation Texture ◽  
Roll Bonding ◽  
Equiaxed Grains ◽  
Electron Back Scattered Diffraction

Microstructure and texture evolution of commercially pure Ni processed by accumulative roll-bonding (ARB) up to eight cycles were studied using electron back scattered diffraction (EBSD). During ARB processing, the original coarse equiaxed grains were gradually transformed into refined lamellar grains along the rolling direction (RD). Shear bands started forming after three cycles. The fraction of low angle grain boundaries (LAGBs) increased after the first and second cycle because of orientation spreading within the original grains. However, their fraction decreased with the evolution of high angle grain boundaries (HAGBs) during subsequent deformations, until saturation was reached after six cycles. Overall, the typical deformation texture components (S, Copper and Brass) were enhanced up to six ARB cycles and then only Copper was further strengthened. At higher cycles a higher Copper concentration was found near sample surface than the interiors due to a high frictional shear of ARB processing.

Local plastic deformation in the vicinity of grain boundaries in Fe–3 mass% Si alloy bicrystals and tricrystal

2014 ◽  
Vol 49 (14) ◽  
pp. 4698-4704 ◽  
Author(s):  
Sadahiro Tsurekawa ◽  
Yuta Chihara ◽  
Kyohei Tashima ◽  
Seiichiro Ii ◽  
Pavel Lejček
Keyword(s):  
Plastic Deformation ◽  
Grain Boundaries ◽  
Local Plastic ◽  
Local Plastic Deformation

Microstructure of Polycrystalline MgO Penetrated by a Silicate Liquid

1996 ◽  
Vol 2 (3) ◽  
pp. 113-128 ◽  
Author(s):  
Sundar Ramamurthy ◽  
Michael P. Mallamaci ◽  
Catherine M. Zimmerman ◽  
C. Barry Carter ◽  
Peter R. Duncombe ◽  
...  
Keyword(s):  
Grain Boundaries ◽  
Grain Growth ◽  
Glassy Phase ◽  
Silicate Liquid ◽  
Two Phase ◽  
The Matrix ◽  
Devitrification Process ◽  
Phase Mixture

Dense, polycrystalline MgO was infiltrated with monticellite (CaMgSiO4) liquid to study the penetration of liquid along the grain boundaries of MgO. Grain growth was found to be restricted with increasing amounts of liquid. The inter-granular regions were generally found to be comprised of a two-phase mixture: crystalline monticellite and a glassy phase rich in the impurities present in the starting MgO material. MgO grains act as seeding agents for the crystallization of monticellite. The location and composition of the glassy phase with respect to the MgO grains emphasizes the role of intergranular liquid during the devitrification process in “snowplowing” impurities present in the matrix.

On the performance of a cascade of turbine rotor tip section blading in wet steam Part 3: Wake traverses

1997 ◽  
Vol 211 (8) ◽  
pp. 639-648 ◽  
Author(s):  
F Bakhtar ◽  
H Mashmoushy ◽  
O C Jadayel
Keyword(s):  
Liquid Phase ◽  
Two Phase Flow ◽  
Turbine Rotor ◽  
Phase Flow ◽  
Wet Steam ◽  
Flow Conditions ◽  
Two Phase ◽  
Blow Down ◽  
The Third ◽  
Phase Mixture

During the course of expansion of steam in turbines the fluid first supercools and then nucleates to become a two-phase mixture. The liquid phase consists of a large number of extremely small droplets which are difficult to generate except by nucleation. To reproduce turbine two-phase flow conditions requires a supply of supercooled vapour which can be achieved under blow-down conditions by the equipment employed. This paper is the third of a set describing an investigation into the performance of a cascade of rotor tip section profiles in wet steam and presents the results of the wake traverses.

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