Impregnation Behavior of Polyamide 6 in Carbon Fibers and the Properties of their Composites

2017 ◽  
Vol 898 ◽  
pp. 2134-2142
Author(s):  
Yu Fei Hu ◽  
Jian Zhang ◽  
Biao Wang ◽  
Xue Na Zhang
Keyword(s):  
Mechanical Properties ◽  
Carbon Fibers ◽  
Simulated Data ◽  
Polyamide 6 ◽  
Processing Parameters ◽  
Void Content ◽  
Processing Temperature ◽  
Resin Flow ◽  
Minimum Level ◽  
Properties Of Composites

Unidirectional carbon fiber (CF) / Polyamide 6 (PA6) composites were prepared by stacking fabrics method. Due to the effect of the textile structure and rough surface of PA6 fabrics, slipping of carbon fibers (CFs) during the stacking process was prevented and uniformity of impregnation was improved. Meanwhile, the usage of PA6 fabrics resulted in the minimum level of void content of composites, which improved the mechanical properties of composites. Additionally, the void content of materials was associated with the mechanical properties of composites. The flexural strength of composite reached 819.58 MPa when its void content was 3.49%. Moreover, a model based on Darcy’s law was developed to simulate the impregnation behavior of PA6 in CFs which was made by stacking fabrics method. The resin flow was observed by using optical microscopy. The evolution of void content in composites was related to the processing parameters (holding time, processing temperature and processing pressure).The comparison between the experimental and simulated data showed that the model was reliable to describe the impregnation process.

scholarly journals Mechanical and structural properties of composites made from recycled and virgin polyethylene terephthalate (PET) and metal chip or mesh wire

2019 ◽  
Vol 299 ◽  
pp. 06007
Author(s):  
Mircea Aurelian Antoniu Rusu ◽  
Sever-Adrian Radu ◽  
Catalin Moldovan ◽  
Codruta Sarosi ◽  
Ionela Amalia Mazilu (Moldovan) ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Polyethylene Terephthalate ◽  
Processing Parameters ◽  
Sem Images ◽  
Major Drawback ◽  
Recycled Pet ◽  
Plastic Processing ◽  
Metal Chip ◽  
Intense Research ◽  
Properties Of Composites

Although polyethylene terephthalate (PET) is a champion of recycling, intense research is being done to find new solutions for using recycled plastic. This study aims to characterize the mechanical andstructural properties (SEM- scanning electron microscopy) of products made from recycled metal swarf or mesh wire with recycled plastic (PET) in comparison with virgin plastic. Samples manufactured from virgin and recycled PET are made by pressing and high temperature. The loss of mechanical properties ofproducts made from recycled plastic is a major drawback that influences their use. SEM images confirm that the dispersion and distribution of the PET phase is not very uniform. By addition of virgin plastic in various compositions with recycled plastic, processing parameters and mechanical properties can be optimized.

Postprocessing method-induced mechanical properties of carbon fiber-reinforced thermoplastic composites

2020 ◽  
pp. 089270572094537
Author(s):  
Van-Tho Hoang ◽  
Bo-Seong Kwon ◽  
Jung-Won Sung ◽  
Hyeon-Seok Choe ◽  
Se-Woon Oh ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Carbon Fiber ◽  
Processing Parameters ◽  
Thermoplastic Composites ◽  
Void Content ◽  
Fiber Reinforced ◽  
Crystallinity Degree ◽  
Automated Fiber Placement ◽  
Carbon Fiber Reinforced

Promising carbon fiber-reinforced thermoplastic (CF/polyetherketoneketone (PEKK)) composites were fabricated by the state-of-the-art technology known as “Automated Fiber Placement.” The mechanical properties of CF/PEKK were evaluated for four different postprocessing methods: in situ consolidation, annealing, vacuum bag only (VBO), and hot press (HP). The evaluation was performed by narrowing down the relevant processing parameters (temperature and layup speed). Furthermore, the void content and crystallinity of CF/PEKK were measured to determine the effect of these postprocessing processes. The HP process resulted in the best quality with the highest interlaminar shear strength, highest crystallinity degree, and lowest void content. The second most effective method was VBO, and annealing also realized an improvement compared with in situ consolidation. The correlation between the postprocessing method and the void content and crystallinity degree was also discussed.

Pultrusion Technology Optimization for Hybrid Fiber Composites Based on DSC and Mechanical Property Testing

2011 ◽  
Vol 295-297 ◽  
pp. 383-387 ◽  
Author(s):  
Li Chen ◽  
Qi Lin Zhao ◽  
Ke Bin Jiang ◽  
Yong Ding
Keyword(s):  
Mechanical Properties ◽  
Fiber Composite ◽  
Processing Parameters ◽  
Fiber Composites ◽  
Processing Temperature ◽  
Processing Parameter ◽  
Heating Rates ◽  
Hybrid Fiber ◽  
Scanning Calorimetry ◽  
Parameter Ranges

In the interest of improving the curing effect and mechanical properties of pultruded carbon/glass bybrid fiber composites, the DSC (Differential Scanning Calorimetry) technology was introduced and the curing DSC curves for the hybrid fiber composites at 4 different heating rates was attained. Then the range of the processing temperature for the three-stage heating pultrusion was primarily determined with T-β method. Subsequently a kind of carbon/glass hybrid composite pole with a diameter of 11mm was selected as the research object, and was manufactured with varies of processing temperatures and speeds. The produced poles were mechanically tested to investigate the effect of processing parameters on the mechanical properties of the composite, so as to further more ascertain the processing parameter ranges fitting to this material formula. As the result shows: the pultrusion processing parameters for the hybrid fiber composite acquired in this study can satisfy the require of manufacturing; compared with the traditional method that attain processing parameters by experience, the method for attaining processing parameters suggested in this paper is more efficiency, more economical and more accurate.

Filament winding of aramid/PA6 commingled yarns with in situ consolidation

2017 ◽  
Vol 31 (4) ◽  
pp. 465-482 ◽  
Author(s):  
Joanna CH Wong ◽  
Javier Molina Blanco ◽  
Paolo Ermanni
Keyword(s):  
Experimental Investigation ◽  
Polyamide 6 ◽  
Processing Parameters ◽  
Filament Winding ◽  
Void Content ◽  
Compression Moulding ◽  
Compaction Force ◽  
Commingled Yarns ◽  
Filament Winding Process

The in situ consolidation of commingled yarns during filament winding is demonstrated on an aramid fibre-reinforced polyamide 6 material. This article is a systematic experimental investigation of the filament winding processing parameters, namely, the heat gun temperature, line speed, fibre tension, compaction force and preheater temperature. Optimizing the processing parameters in this filament winding process produced a fully consolidated material with a void content of ∼0.25% which is comparable to the material quality achieved by means of compression moulding using the same intermediate materials.

Thermal, morphological and mechanical properties of composites based on polyamide 6 with cellulose, silica and their hybrids from rice husk

2020 ◽  
pp. 002199832097829
Author(s):  
Renato P Melo ◽  
Marcelo P da Rosa ◽  
Paulo H Beck ◽  
Lucas GP Tienne ◽  
Maria de Fátima V Marques
Keyword(s):  
Mechanical Properties ◽  
Rice Husk ◽  
Natural Fibers ◽  
Polyamide 6 ◽  
Mechanical Analysis ◽  
Degree Of Crystallinity ◽  
Scanning Calorimetry ◽  
Cellulosic Fibers ◽  
The One ◽  
Properties Of Composites

The use of cellulosic fibers from different natural sources as fillers in polymer matrices to improve their properties has been extensively studied in the last years. It is mainly due to the vast availability of natural fibers as well as their biodegradability. The purpose of this present work was to extract cellulose, silica, and cellulose-silica fillers – these last called “hybrids” – from rice husk through delignification and subsequent oxidation and, then, prepare composites with polyamide 6 and improve mainly its thermal-mechanical properties. The content of 10 wt.% of fillers was inserted in PA 6 matrix. Infrared spectroscopy pointed the main characteristic peaks of cellulose and silica of hybrids, as thermogravimetric analysis showed high thermal stability of fillers, allowing their incorporation in PA-6 matrix by extrusion method. Thermo dynamic-mechanical analysis showed, in a general overview, a significant improvement of mechanical properties of composites, as elastic modulus, compared with neat polyamide-6, mainly the one with 2.5 wt% of silica and 7.5% of cellulose. This last also showed increasing of degree of crystallinity, measured by differential scanning calorimetry, showing the extraction efficiency of fillers from rice husk as well as the potential application of composites as structural components in automotive parts.

scholarly journals Annealing Effects on the Crystallinity of Carbon Fiber-Reinforced Polyetheretherketone and Polyohenylene Laminate Composites Manufactured by Laser Automatic Tape Placement

2020 ◽  
Vol 26 (3) ◽  
pp. 308-316
Author(s):  
Svetlana RISTESKA ◽  
Anka T. PETKOSKA ◽  
Samoil SAMAK ◽  
Marian DRIENOVSKY
Keyword(s):  
Mechanical Properties ◽  
Composite Materials ◽  
Carbon Fiber ◽  
Processing Parameters ◽  
Polyphenylene Sulfide ◽  
Thermoplastic Composites ◽  
Void Content ◽  
Angle Of Incidence ◽  
Annealing Step

In situ consolidation of thermoplastic composites by Automated Tape Placement (ATP) is challenging. High quality ATP grade pre-preg material and tape head equipped with an efficient heat sources like lasers offer an opportunity towards high deposition rates and improved mechanical properties of composite materials. In this study uni-directional carbon fiber/ polyphenylene sulfide (UD tape prepreg CF/PPS), carbon fiber/polyetheretherketone (UD tape prepreg CF/PEEK) as well as blend of carbon fiber/polyetheretherketone/polyphenylene sulfide (UD tapes prepregs CF/PEEK/PPS) laminates are compared in terms of their properties after beeing processed by ATP technology. CF/PPS, CF/PEEK and blend CF/PPS/PEEK laminate specimens were processed using in-situ laser-assisted ATP (LATP) process. LATP processing parameters used in this study were chosen based on a preliminary trials; the results provide a basis for refinement of these parameters and prepreg material with an optimal and balanced set of final mechanical properties. This study showed an attempt how to manage the processing parameters for LATP process and to obtain composite materials with tailored properties. The process for production of thermoplastic plates with LATP head in general is a process that is governed by many parameters such as: laser power, angle of incidence, roller pressure and temperature, placement speed, tool temperature, then types of the roller material and the tool material. These parameters are not subject of discussing in this paper; they are kept constant, and the goal of the paper is to manage the crystallinity level within the composite thermoplastic material during annealing step at different temperatures after LATP process. Also, the void content during the production process could be controlled. More particularly, the authors showed that composites based on PPS matrix manufactured with LATP process possess higher flexural strength, with less void content compared to samples based on PEEK matrix. These samples showed also higher crystallinity after annealing step.

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