Investigation of Flotation Separation of Elemental Sulfur and Sulfides from Lead Sulfate from Low-Temperature Leaching of Lead Concentrates

2020 ◽  
Vol 989 ◽  
pp. 537-542
Author(s):  
Kirill A. Karimov ◽  
Aleksei V. Kritskii ◽  
Sergey E. Polygalov
Keyword(s):  
Low Temperature ◽  
Filter Cake ◽  
Elemental Sulfur ◽  
Lead Sulfate ◽  
Raw Material ◽  
Granulation Process ◽  
Flotation Concentrate ◽  
Autoclave Leaching ◽  
Sulfate Lead ◽  
Concentrate Yield

Monometallic ore that is mostly lead found in nature is extremely rare. The main natural raw material for the lead production is sulfide polymetallic ores. In this study the filter cake processing after the low-temperature autoclave leaching of the lead concentrate to produce a sulphide concentrate and lead tailings was investigated The study of component separation was carried out using the methods of mathematical planning of the second order experiment. The following optimal costs of reagents, g/t: 140-200 potassium xanthate, 70-100 foaming agent, 100 copper sulfate; the concentrate yield is 41-43 %; it is extracted to, %: 95 Fe, 49 Cu, 96 Zn, 98 S0, 18-19 Pb. At flotation 18,7% of lead goes into flotation concentrate and 80.5% is lead sulfate. The rectification of the obtained concentrate by flotation did not give acceptable results, since the yield of the foam product in all experiments was 93-96%. For the separation of lead sulphate from sulphur-sulfide concentrate was used in the granulation of sulfur in the following conditions: t = 145 °C, Po2 = 0,0-0,5 MPa, τ = 60 to 120 min. In the granulation process of the flotation concentrate is a division of lead sulfate and elemental sulfur, the sulfate lead content in sulphur-sulfide phase is decreased from 28.44 % to 3.5 %, its recovery in a sulfate filter cake has reached 90.6 %

Preparation of high-purity lead oxide from spent lead paste by low temperature burning and hydrometallurgical processing with ammonium acetate solution

RSC Advances ◽  
2016 ◽  
Vol 6 (25) ◽  
pp. 21148-21155 ◽  
Author(s):  
Cheng Ma ◽  
Yuehong Shu ◽  
Hongyu Chen
Keyword(s):  
Low Temperature ◽  
Lead Oxide ◽  
Ammonium Acetate ◽  
Lead Dioxide ◽  
Lead Sulfate ◽  
Acetate Solution ◽  
Lead Acid Battery ◽  
Hydrometallurgical Processing ◽  
Sulfate Lead ◽  
Main Components

Lead sulfate, lead dioxide and lead oxide are the main components of lead paste in a spent lead-acid battery.

scholarly journals Preparation and application of carbon and hollow TiO2 microspheres by microwave heating at a low temperature

e-Polymers ◽  
2021 ◽  
Vol 21 (1) ◽  
pp. 200-209
Author(s):  
Caiyun Zhang ◽  
Chunhong Li ◽  
Bolin Ji ◽  
Zhaohui Jiang
Keyword(s):  
Low Temperature ◽  
Microwave Heating ◽  
Raw Material ◽  
Carbon Microspheres ◽  
Microwave Assisted ◽  
The Core ◽  
Good Crystallinity ◽  
Carbon Core ◽  
Microwave Assisted Method ◽  
Uniform Particle Size

Abstract A fast, simple, and energy-saving microwave-assisted approach was successfully developed to prepare carbon microspheres. The carbon microspheres with a uniform particle size and good dispersity were prepared using glucose as the raw material and HCl as the dehydrating agent at low temperature (90°C) in an open system with the assistance of microwave heating. The carbon microspheres were characterized by elemental analysis, XRD, SEM, FTIR, TG, and Raman. The results showed that the carbon microspheres prepared under the condition of 18.5% (v/v) HCl and heating for 30 min by microwave had a narrow size distribution. The core–shell structure of the carbon core and TiO2 shell was prepared with (NH4)2TiF6, H3BO3 using the microwave-assisted method. The hollow TiO2 microspheres with good crystallinity and high photocatalytic properties were successfully prepared by sacrificing the carbon microspheres.

The Experimental of Low Temperature Color Slip for Decorative on Earthenware Body

2016 ◽  
Vol 690 ◽  
pp. 282-285
Author(s):  
Soravich Mulinta
Keyword(s):  
Low Temperature ◽  
Physical Properties ◽  
Manganese Oxide ◽  
Ferric Oxide ◽  
Potassium Feldspar ◽  
Raw Material ◽  
Blue Color ◽  
X Ray ◽  
Yellow Color

The purpose of the study was to investigate the effects of dolomite body, frit and potassium feldspar on the properties of color slip for decorative method of color slip on earthen ware production. The characterization of raw material was analyzed by X-ray fluorescence (XRF). The experiment started with triaxial blend of dolomite body, frit and potassium feldspar in the defined ratio and then to painting of color slips on earthenware production. After that, firing specimens at 950 °C in oxidation atmosphere. Finally, the specimens were tested microstructure and physical properties. The results showed that the ratio of 50% dolomite body, 40% frit and 10% potassium feldspar were optimum properties for decorative on earthenware body. In color slip consisting of blue color added Cobalt oxide 1% ,Green colors added chromic oxide 10% , Gray color added manganese oxide 10% ,yellow color added stain 2225 10% and hazel color added ferric oxide 2 wt %.

Gravity-flotation gold-bearing ore concentration

2021 ◽  
Vol 1 (1) ◽  
pp. 4-15
Author(s):  
P. K. Fedotov ◽  
A. E. Senchenko ◽  
K. V. Fedotov ◽  
A. E. Burdonov
Keyword(s):  
High Performance ◽  
Gold Recovery ◽  
Gold Content ◽  
Flotation Concentrate ◽  
Stage Scheme ◽  
Study Results ◽  
Ore Minerals ◽  
Concentrate Yield ◽  
Flotation Concentration ◽  
Gold Bearing

The paper focuses on the study of the gold-bearing ore dressability. According to technological research, the average gold content is 11.88 g/t. The silver content is insignificant – 2.43 g/t. Main ore minerals in the sample are pyrite and pyrrhotite. According to mineralogical and X-ray structural analysis, the average content of these minerals in the ore is about 6 % (in total). Main rock-forming minerals of the original ore are: quartz (60.1 %), quartz-chlorite-mica aggregates (3.8 %), carbonates (7.1 %). According to the study results, it was found that the gold recovery in the GRG test was 72.75 % with a total concentrate yield of 1.34 % and a content of 664.78 g/t. At the same time, the gold content in tailings was 3.29 g/t. A stage test showed that it is advisable to use a two-stage scheme for ore processing by gravity technology only. The first stage is in the grinding cycle with the 60–70 % ore size, and the second stage is with the final classifier overflow size of 90 % –0.071 mm. Centrifugal separation has high performance as a free gold recovery operation in the grinding cycle. A concentrate with a gold content of 2426 g/t was obtained with a yield of 0.31 % and a recovery of 63.74 %. The beneficiation of first stage tailings ground to 90 % –0.071 mm at the KC-CVD concentrator (modeling) made it possible to extract gold into a total gravity concentrate (KC-MD + KC-CVD) of 87.25 % with a concentrate yield of 22.63 %. The gold content in tailings was 1.97 g/t. The results of gravity and flotation concentration of the original ore indicate the feasibility of using a combined gravity-flotation technological scheme. In a closed experiment of the initial ore beneficiation according to the gravity-flotation scheme at a natural pH of the pulp (without adding acid), the following products were obtained: gravity concentrate with a gold content of 2426 g/t at a yield of 0.31 % and recovery of 64.06 %; flotation concentrate (after the II cleaning) with a gold content of 122 g/t at a yield of 2.90 % and recovery of 33.01 %; the total gold recovery in the gravity-flotation concentrate was 94.07 % with a yield of 3.21 % and an Au content of 345.87 g/t, the gold content in the flotation tailings was 0.72 g/t.

The Study of the Melting of Waelz Oxide with an Increase in the Temperature of the Calcination Process

2021 ◽  
Vol 316 ◽  
pp. 705-710
Author(s):  
A.G. Ryazanov ◽  
A.V. Senin ◽  
V.D. Nasonov
Keyword(s):  
Partial Melting ◽  
Gas Phase ◽  
Lead Oxide ◽  
Elevated Temperatures ◽  
Lead Sulfate ◽  
Raw Material ◽  
Chemical Transformations ◽  
Calcination Process ◽  
Waelz Oxide ◽  
Negative Effect

Waelz-oxide is a raw material for the production of metallic zinc. Waelz-oxide contains impurities of zinc and lead chlorides and fluorides. Halides have a negative effect on the process of zinc electrolysis. Halides have a relatively low boiling point; therefore, they are removed into the gas phase by calcining Waelz-oxide at 800–850 °С. To intensify the process, calcination is sometimes carried out at elevated temperatures of 1100–1250 °С. However, an increase in temperature leads to partial melting and granulation of the calcined product. In the present work, the chemical and phase composition of the initial and calcined Waelz-oxide was studied. Thermodynamic modeling of phase and chemical transformations of Waelz-oxide components during heating has been performed. Experiments on calcination of Waelz-oxide in laboratory conditions at temperatures of 600–1250 °C were carried out. It was found that partial melting and granulation of Waelz-oxide is the result of the formation of fusible eutectics containing lead oxide. Lead oxide is formed as a result of decomposition of lead sulfate when heated above 1100 °C. A similar effect is not observed at a standard calcination temperature of 850 °C.

scholarly journals Composition and properties of ceramic heat insulating building materials made ofthe masses of low temperature foaming on the basis of clay raw material

2012 ◽  
Vol 29 (3) ◽  
pp. 35-40
Author(s):  
Y.V. Selivanov ◽  
A.D. Shiltsina ◽  
Y.V. Loginova ◽  
N.N. Korolkova ◽  
V.M. Selivanov
Keyword(s):  
Low Temperature ◽  
Building Materials ◽  
Raw Material

Synthesis and Characterization of Calcium Zeolite-Cowlesite.

2021 ◽  
Vol 23 (05) ◽  
pp. 787-790
Author(s):  
Abhijit M ◽  
◽  
Suresh Kumar. B. V ◽  
Keyword(s):  
Low Temperature ◽  
Elemental Concentration ◽  
Stoichiometric Composition ◽  
Lattice Parameter ◽  
Raw Material ◽  
Synthesis And Characterization ◽  
Aluminum Silicate ◽  
Hydrothermal Conditions ◽  
Orthorhombic System

Cowlesite is a Calcium Aluminum silicate CaAl2Si3O106H2O which formed under the hydrothermal conditions of low temperature (1800C) and pressure (1.013250bar). Cowlesite minerals are known for their peculiar occurrence. Synthesis of Cowlesite mineral was carried by suitable stoichiometric composition. Hydrothermal synthesized Cowlesite mineral was characterized by XRD, SEM, and EDAX. It crystallized in the orthorhombic system and a lattice parameter a=23.22Å, b=30.58Å, c=25.01Å, Volume of Unit cell=17758.79Å3, α=β=γ=900. EDAX results show the elemental concentration of raw material which was used.

scholarly journals The investigation of producing bacterial cellulose fibres through hand-spun

2019 ◽  
Vol 131 ◽  
pp. 01052
Author(s):  
Yu Wang
Keyword(s):  
Tensile Strength ◽  
Bacterial Cellulose ◽  
Young’S Modulus ◽  
Filter Cake ◽  
Young's Modulus ◽  
Raw Material ◽  
Cellulose Fibres ◽  
Elongation At Break ◽  
Intermediate States

Nanocellulose fibres can be hand-spun from different intermediate states, such as nanocellulose paper and filter cake, which are made from the BC suspension as well as wet pellicle (WP) and dry pellicle (DP) from BC pellicles. In this study, it can be concluded that increasing the hanging weight can increase the Young’s modulus and the tensile strength of fibres. Nanofibres produced from BC pellicles as raw material have better performance than those made from BC suspension. The best properties obtained from the fibres produced from wet pellicles and suspended to a 100g hanging weight upon drying are Young’s modulus (33.8 GPa), tensile strength (610 MPa) and elongation at break (3.6%).

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