Characterisation of Electrode Drying Effect on the Tungsten Carbide Hardfacing Microstructure

2020 ◽  
Vol 991 ◽  
pp. 77-85
Author(s):  
Muniandy Nagentrau ◽  
Abdul Latif Mohd Tobi ◽  
Saifulnizan Jamian ◽  
Mathan Sambu
Keyword(s):  
Major Part ◽  
Medium Carbon Steel ◽  
Medium Carbon ◽  
Scanning Electron Microscope Analysis ◽  
Hardness Tester ◽  
Carbide Distribution ◽  
Electron Microscope Analysis ◽  
Hardness Values ◽  
Scanning Electron

This study addresses characterization of ED (electrode drying) effect on WC hardfacing welding microstructure. Medium carbon steel blade which used as CD (continuous digester) blade to mix up sulphuric acid together with ilmenite ore in a digester tank as a major part of production. Microstructure of WC hardfacing, elemental composition alongside hardness analyses are executed to investigate the effect of ED (electrode drying). The ED (electrode drying) effect on microstructure and hardness values of WC hardafcing coating are characterized by SEM (scanning electron microscope) analysis and micro-Vickers hardness tester correspondingly. Results revealed that ED (electrode drying) effect less significant in the larger carbides at overall coating zone. However, the absence of ED (electrode drying) led to distribution of uniform smaller carbide in non-carbide zone. The uniform carbide distribution increases the hardness of the WC hardfacing coating.

scholarly journals Preparation and Characterization of Keratin/Alginate Blend Microparticles

2018 ◽  
Vol 2018 ◽  
pp. 1-8 ◽  
Author(s):  
Yaowalak Srisuwan ◽  
Prasong Srihanam
Keyword(s):  
Diffusion Method ◽  
Blend Ratio ◽  
Scanning Electron Microscope Analysis ◽  
Sheet Structure ◽  
Electron Microscope Analysis ◽  
Different Shapes ◽  
Thermal Stability Of ◽  
Scanning Electron ◽  
Main Factor

The water-in-oil (W/O) emulsification-diffusion method was used for construction of keratin (Ker), alginate (Alg), and Ker/Alg blend microparticles. The Ker, Alg, and Ker/Alg blend solutions were used as the water phase, while ethyl acetate was used as the oil phase. Firstly, different concentrations of Ker solution was used to find suitable content. 1.6% w/v Ker solution was blended with the same concentration of the Alg solution for further microparticle construction. Results from scanning electron microscope analysis show that the microparticles have different shapes: spherical, bowl-like, porous, and hollow, with several sizes depending on the blend ratio. FTIR and TG analyses indicated that the secondary structure and thermal stability of the microparticles were influenced by the Ker/Alg blend ratio. The interaction between functional groups of keratin and alginate was the main factor for both β-sheet structure and Td,max values of the microparticles. The results suggested that Ker/Alg blend microparticles might be applied in many fields by varying the Ker/Alg ratio.

scholarly journals Susceptibility Assessment of Multidrug Resistant Bacteria to Natural Products

Dose-Response ◽  
2020 ◽  
Vol 18 (3) ◽  
pp. 155932582093618
Author(s):  
Essam Hassan Mohamed ◽  
Youssef Saeed Alghamdi ◽  
Salama Mostafa Abdel-Hafez ◽  
Mohamed Mohamed Soliman ◽  
Saad H. Alotaibi ◽  
...  
Keyword(s):  
Inhibitory Concentration ◽  
Multidrug Resistant ◽  
Resistant Bacteria ◽  
Syzygium Aromaticum ◽  
Bacterial Strains ◽  
Multidrug Resistant Bacteria ◽  
Scanning Electron Microscope Analysis ◽  
Electron Microscope Analysis ◽  
Holothuria Atra ◽  
Scanning Electron

Objective: The aim of this study was to examine the effect of some natural compounds against multidrug-resistant bacteria. Methods: Forty-three bacterial strains were collected. Disc diffusion and minimum inhibitory concentration (MIC) tests were carried out for natural compounds including quercetin, Acacia nilotica, Syzygium aromaticum, and Holothuria atra. Scanning electron microscope analysis and bacterial DNA apoptosis assays were performed. Results: Staphylococcus aureus strains were resistant to imipenim, ampicillin, and penicillin. Most Escherichia coli strains were resistant to amoxicillin, clavulanat, and ampicillin. Finally, tigecycline was effective with Klebsiella pneumoniae and was resistant to all antibiotics. Only S aromaticum had an antibacterial effect on K pneumoniae. Most S aureus strains were sensitive to S aromaticum, A nilotica, and quercetin. All examined natural extracts had no effect on E coli. Holothuria atra had no effect on any of the strains tested. Minimum inhibitory concentration and minimum bactericidal concentration values for examined plants against S aureus were 6.25 to 12, 1.6 to 3.2, and 9.12 to 18.24 mg/mL, respectively. Syzygium aromaticum was active against K pneumoniae with an MIC of 12.5 mg/mL. Scanning electron microscope analysis performed after 24 and 48 hours of incubation showed bacterial strains with distorted shapes and severe cell wall damage. Syzygium aromaticum, quercetin, and A nilotica showed clear fragmentations of S aureus DNA. Conclusions: Current findings confirmed the beneficial effect of using natural products such as clove (S aromaticum), quercetin, and A nilotica as a promising therapy to overcome multidrug resistant bacteria.

scholarly journals Effect of Boron on Microstructure and Microhardness Properties of Mo-Si-B Based Coatings Produced Via TIG Process

2016 ◽  
Vol 61 (3) ◽  
pp. 1515-1520 ◽  
Author(s):  
S. Islak ◽  
C. Özorak ◽  
C. T. Sezgin ◽  
M. Akkaş
Keyword(s):  
Electron Microscopy ◽  
Boron Content ◽  
Medium Carbon Steel ◽  
Inert Gas ◽  
X Ray Diffraction ◽  
Medium Carbon ◽  
X Ray ◽  
Physical Chemical ◽  
Structural Applications ◽  
Scanning Electron

Abstract In this study, Mo-Si-B based coatings were produced using tungsten inert gas (TIG) process on the medium carbon steel because the physical, chemical, and mechanical properties of these alloys are particularly favourable for high-temperature structural applications. It is aimed to investigate of microstructure and microhardness properties of Mo-Si-B based coatings. Optical microscopy (OM), X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to characterize the microstructures of Mo-Si-B based coatings. The XRD results showed that microstructure of Mo–Si–B coating consists of α-Mo, α-Fe, Mo2B, Mo3Si and Mo5SiB2 phases. It was reported that the grains in the microstructure were finer with increasing amounts of boron which caused to occur phase precipitations in the grain boundary. Besides, the average microhardness of coatings changed between 735 HV0.3 and 1140 HV0.3 depending on boron content.

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