scholarly journals Biological and physico-chemical properties of new root canal sealers

Author(s):  
M Colombo ◽  
C Poggio ◽  
A Dagna ◽  
MV Meravini ◽  
P Riva ◽  
...  
Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7594
Author(s):  
Zhejun Wang ◽  
Ya Shen ◽  
Markus Haapasalo

Microbes are prevalent in the root canals of necrotic teeth, and they are the cause of primary and post-treatment apical periodontitis. Bacteria can dwell within the infected root canal system as surface-adherent biofilm structures, which exhibit high resistance to antimicrobial agents. Bioceramic materials, with their biocompatible nature and excellent physico-chemical properties, have been widely used in dental applications, including endodontics. This review focuses on the application of bioceramic technology in endodontic disinfection and the antibiofilm effects of endodontic bioceramic materials. Different bioceramic materials have shown different levels of antibiofilm effects. New supplements have emerged to potentially enhance the antibiofilm properties of bioceramics aiming to achieve the goal of microbial elimination in the root canal system.


2018 ◽  
Vol 17 ◽  
pp. e181207
Author(s):  
Clauber Romagnoli ◽  
Klíssia Romero Felizardo ◽  
Ricardo Danil Guiraldo ◽  
Alcides Gonini Júnior ◽  
Renan Hideki Kaneshima ◽  
...  

Aim: The aim of this study was to evaluate and compare the setting times (ST), flow (FW), radiopacity (RP), dimensional stability (DS), solubility (SB), and polymerization stress (PS) of the MTA Fillapex and AH Plus root canal sealers. Methods: The above qualities were tested according to ISO 6876/2001 standardization. The water used in the dimensional stability test was evaluated to verify the presence of released materials. For the photoelastic analysis, 20 photoelastic resin rings were prepared, and the root canal sealers were inserted. After 24 hours, the specimens were analyzed in a Polariscope. Data of the setting times, flow tests, radiopacity, dimensional stability, and solubility tests were submitted to a Kolgomorov–Smirnov test and then to a Student’s t-test at the 5% significance level. Results: The data derived from photoelastic analyses were submitted to an ANOVA and Tukey’s test with a significance level of 5%. MTA Fillapex and AH Plus complied with ISO 6876/2001. However, there were significant differences (p < 0.05) between the two cements for ST, FW, RP, DS, and SB. MTA Fillapex showed higher FW, SB, and PS when compared with AH Plus. Conclusions: MTA Fillapex and AH Plus complied with ISO 6876/2001 in terms of ST, FW, RP, DS, and SB. MTA Fillapex showed higher PS when compared to AH Plus.


2022 ◽  
Vol 12 (2) ◽  
pp. 873
Author(s):  
Sawsan T. Abu Abu Zeid ◽  
Ruaa A. Alamoudi ◽  
Abeer A. Mokeem Mokeem Saleh

Aimed to evaluate the effect of water solubility on chemical properties and surface structure of bioceramic-based (BC-HiFlow and BC-EndoSeqence) compared with resin-based (Adseal) root canal sealers. Fresh mix was inserted into polyethylene mold (n = 10) and subjected to Vicat needle to evaluate the setting time. The set discs were analyzed by Fourier transform infrared (FTIR) spectroscopy then immersed in deionized water for 1, 7, 14 and 28 days. The solubility%, pH changes, released calcium (Ca2+), phosphate (PO43−) and silicon (Si4+) ions were evaluated after each immersion period. The discs were analyzed by scanning electron microscopy/Energy dispersed X-ray (SEM/EDX) before and after solubility test. Although FTIR detected similar composition of both bioceramic-sealers, BC-EndoSequence determined the prolonged setting times. At the end of solubility test, both bioceramic-sealers exhibited significant greater solubility (>3%), alkaline pH (>11) at p < 0.001. Adseal displayed the significant greatest Ca2+ and PO43− released, while BC-HiFlow displayed the significant greatest Si4+ release (p < 0.001). SEM revealed voids and pores on the surface of all tested sealers with the greatest value on Adseal surface. In conclusion, although both bioceramic-sealers had high solubility, BC-Hiflow complied the ISO standard regarding setting time and least surface micropores better than that of BC-EndoSequence.


Author(s):  
H. Gross ◽  
H. Moor

Fracturing under ultrahigh vacuum (UHV, p ≤ 10-9 Torr) produces membrane fracture faces devoid of contamination. Such clean surfaces are a prerequisite foe studies of interactions between condensing molecules is possible and surface forces are unequally distributed, the condensate will accumulate at places with high binding forces; crystallites will arise which may be useful a probes for surface sites with specific physico-chemical properties. Specific “decoration” with crystallites can be achieved nby exposing membrane fracture faces to water vopour. A device was developed which enables the production of pure water vapour and the controlled variation of its partial pressure in an UHV freeze-fracture apparatus (Fig.1a). Under vaccum (≤ 10-3 Torr), small container filled with copper-sulfate-pentahydrate is heated with a heating coil, with the temperature controlled by means of a thermocouple. The water of hydration thereby released enters a storage vessel.


1990 ◽  
Vol 63 (03) ◽  
pp. 499-504 ◽  
Author(s):  
A Electricwala ◽  
L Irons ◽  
R Wait ◽  
R J G Carr ◽  
R J Ling ◽  
...  

SummaryPhysico-chemical properties of recombinant desulphatohirudin expressed in yeast (CIBA GEIGY code No. CGP 39393) were reinvestigated. As previously reported for natural hirudin, the recombinant molecule exhibited abnormal behaviour by gel filtration with an apparent molecular weight greater than that based on the primary structure. However, molecular weight estimation by SDS gel electrophoresis, FAB-mass spectrometry and Photon Correlation Spectroscopy were in agreement with the theoretical molecular weight, with little suggestion of dimer or aggregate formation. Circular dichroism studies of the recombinant molecule show similar spectra at different pH values but are markedly different from that reported by Konno et al. (13) for a natural hirudin-variant. Our CD studies indicate the presence of about 60% beta sheet and the absence of alpha helix in the secondary structure of recombinant hirudin, in agreement with the conformation determined by NMR studies (17)


1963 ◽  
Vol 79 (2) ◽  
pp. 263-293 ◽  
Author(s):  
E.M. Savitskii ◽  
V.F. Terekhova ◽  
O.P. Naumkin

1990 ◽  
Vol 39 (442) ◽  
pp. 996-1000 ◽  
Author(s):  
Ayao TAKASAKA ◽  
Hideyuki NEMOTO ◽  
Hirohiko KONO ◽  
Yoshihiro MATSUDA

Food Biology ◽  
1970 ◽  
pp. 19-23
Author(s):  
Nawal Abdel-Gayoum Abdel-Rahman

The aim of this study is to use of karkede (Hibiscus sabdariffa L.) byproduct as raw material to make ketchup instead of tomato. Ketchup is making of various pulps, but the best type made from tomatoes. Roselle having adequate amounts of macro and micro elements, and it is rich in source of anthocyanine. The ketchup made from pulped of waste of soaked karkede, and homogenized with starch, salt, sugar, ginger (Zingiber officinale), kusbara (Coriandrum sativum) and gum Arabic. Then processed and filled in glass bottles and stored at two different temperatures, ambient and refrigeration. The total solids, total soluble solids, pH, ash, total titratable acidity and vitamin C of ketchup were determined. As well as, total sugars, reducing sugars, colour density, and sodium chloride percentage were evaluated. The sensory quality of developed product was determined immediately and after processing, which included colour, taste, odour, consistency and overall acceptability. The suitability during storage included microbial growth, physico-chemical properties and sensory quality. The karkede ketchup was found free of contaminants throughout storage period at both storage temperatures. Physico-chemical properties were found to be significantly differences at p?0.05 level during storage. There were no differences between karkade ketchup and market tomato ketchup concerning odour, taste, odour, consistency and overall acceptability. These results are encouraging for use of roselle cycle as a raw material to make acceptable karkade ketchup.


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