scholarly journals Empirical relations of rock properties of outcrop and core samples from the Northwest German Basin for geothermal drilling

2014 ◽  
Vol 2 (1) ◽  
pp. 21-37 ◽  
Author(s):  
D. Reyer ◽  
S. L. Philipp

<p><strong>Abstract.</strong> Information about geomechanical and physical rock properties, particularly uniaxial compressive strength (UCS), are needed for geomechanical model development and updating with logging-while-drilling methods to minimise costs and risks of the drilling process. The following parameters with importance at different stages of geothermal exploitation and drilling are presented for typical sedimentary and volcanic rocks of the Northwest German Basin (NWGB): physical (<i>P</i> wave velocities, porosity, and bulk and grain density) and geomechanical parameters (UCS, static Young's modulus, destruction work and indirect tensile strength both perpendicular and parallel to bedding) for 35 rock samples from quarries and 14 core samples of sandstones and carbonate rocks. <br><br> With regression analyses (linear- and non-linear) empirical relations are developed to predict UCS values from all other parameters. Analyses focus on sedimentary rocks and were repeated separately for clastic rock samples or carbonate rock samples as well as for outcrop samples or core samples. Empirical relations have high statistical significance for Young's modulus, tensile strength and destruction work; for physical properties, there is a wider scatter of data and prediction of UCS is less precise. For most relations, properties of core samples plot within the scatter of outcrop samples and lie within the 90% prediction bands of developed regression functions. The results indicate the applicability of empirical relations that are based on outcrop data on questions related to drilling operations when the database contains a sufficient number of samples with varying rock properties. The presented equations may help to predict UCS values for sedimentary rocks at depth, and thus develop suitable geomechanical models for the adaptation of the drilling strategy on rock mechanical conditions in the NWGB.</p>

Geophysics ◽  
2014 ◽  
Vol 79 (4) ◽  
pp. D227-D233 ◽  
Author(s):  
Mohsen Farrokhrouz ◽  
Mohammad Reza Asef ◽  
Riyaz Kharrat

The uniaxial compressive strength of rock ([Formula: see text]) is an important parameter for petroleum engineers, drilling operations, and all related activities from exploration through to production and abandonment. A thorough understanding of the parameters affecting [Formula: see text] is a basic prerequisite for accurate geomechanical modeling of the reservoir and overburden properties. Uniaxial compressive strength plays a significant role in mud weight determination while drilling, especially for a troublesome lithology such as shale. However, standard geomechanical practice requires well-preserved core samples for measurement of [Formula: see text] in the lab. Because core samples are not often available, there is a need for alternative methods to obtain fit-for-purpose values of [Formula: see text], based on other related rock parameters. Our primary objective was to identify a minimum set of related rock properties that could be used to predict [Formula: see text]. From a review of existing data in the literature, supplemented by laboratory measurements on Iranian samples, we established a database and accomplished extensive statistic analysis. Also, a normality test was executed to make sure a statistically acceptable set of data was collected. We suggested that two parameters of Young’s modulus ([Formula: see text]) and porosity ([Formula: see text]), which might be estimated from geophysical log data, were sufficient for a reliable prediction of [Formula: see text] in shale formations, and the overall contribution of [Formula: see text] was more than [Formula: see text]. We obtained a prediction equation with improved accuracy compared to previous investigations. Furthermore, we determined that the relative sensitivity of shale strength to porosity and Young’s modulus very much depended on the range of porosity.


2011 ◽  
Vol 695 ◽  
pp. 170-173 ◽  
Author(s):  
Voravadee Suchaiya ◽  
Duangdao Aht-Ong

This work focused on the preparation of the biocomposite films of polylactic acid (PLA) reinforced with microcrystalline cellulose (MCC) prepared from agricultural waste, banana stem fiber, and commercial microcrystalline cellulose, Avicel PH 101. Banana stem microcrystalline cellulose (BS MCC) was prepared by three steps, delignification, bleaching, and acid hydrolysis. PLA and two types of MCC were processed using twin screw extruder and fabricated into film by a compression molding. The mechanical and crystalline behaviors of the biocomopsite films were investigated as a function of type and amount of MCC. The tensile strength and Young’s modulus of PLA composites were increased when concentration of MCC increased. Particularly, banana stem (BS MCC) can enhance tensile strength and Young’s modulus of PLA composites than the commercial MCC (Avicel PH 101) because BS MCC had better dispersion in PLA matrix than Avicel PH 101. This result was confirmed by SEM image of fractured surface of PLA composites. In addition, XRD patterns of BS MCC/PLA composites exhibited higher crystalline peak than that of Avicel PH 101/PLA composites


2012 ◽  
Vol 3 (1) ◽  
pp. 13-26
Author(s):  
Myrtha Karina ◽  
Lucia Indrarti ◽  
Rike Yudianti ◽  
Indriyati

The effect of castor oil on the physical and mechanical properties of bacterial cellulose is described. Bacterial cellulose (BC) was impregnated with 0.5–2% (w/v) castor oil (CO) in acetone–water, providing BCCO films. Scanning electron micrographs revealed that the castor oil penetrated the pores of the bacterial cellulose, resulting in a smoother morphology and enhanced hydrophilicity. Castor oil caused a slight change in crystallinity indices and resulted in reduced tensile strength and Young's modulus but increased elongation at break. A significant reduction in tensile strength and Young's modulus was achieved in BCCO films with 2% castor oil, and there was an improvement in elongation at break and hydrophilicity. Impregnation with castor oil, a biodegradable and safe plasticiser, resulted in less rigid and more ductile composites.


2011 ◽  
Vol 264-265 ◽  
pp. 819-824 ◽  
Author(s):  
Md. Rezaur Rahman ◽  
Sinin Hamdan ◽  
M. Saiful Islam ◽  
Md. Shahjahan Mondol

In Malaysia, especially Borneo Island Sarawak has a large scale of tropical wood species. In this study, selected raw tropical wood species namely Artocarpus Elasticus, Artocarpus Rigidus, Xylopia Spp, Koompassia Malaccensis and Eugenia Spp were chemically treated with sodium meta periodate to convert them into wood polymer composites. Manufactured wood polymer composites were characterized using mechanical testing (modulus of elasticity (MOE), modulus of rupture (MOR), static Young’s modulus) and decay resistance test. Modulus of elasticity and modulus of rupture were calculated using three point bending test. Static Young’s modulus and decay resistance were calculated using compression parallel to gain test and natural laboratory decay test respectively. The manufactured wood polymer composites yielded higher modulus of elasticity, modulus of rupture and static Young’s modulus. Wood polymer composite had high resistant to decay exposure, while Eugenia Spp wood polymer composite had highly resistant compared to the other ones.


2021 ◽  
Author(s):  
MICHAEL N. OLAYA ◽  
SAGAR PATIL ◽  
GREGORY M. ODEGARD ◽  
MARIANNA MAIARÙ

A novel approach for characterization of thermosetting epoxy resins as a function of the degree of cure is presented. Density, cure kinetics, tensile strength, and Young’s modulus are experimentally characterized across four mixing ratios of DGEBF/DETDA epoxy. Dynamic differential scanning calorimetry (DSC) is used to characterize parameters for a Prout-Thompkins kinetic model unique to each mixing ratio case through a data fitting procedure. Tensile strength and Young’s modulus are then characterized using stress-strain data extracted from quasi-static, uniaxial tension tests at room temperature. Strains are measured with the 2-D digital image correlation (DIC) optical strain measurement technique. Strength tends to increase as amine content use in the formulation increases. The converse trend is observed for Young’s modulus. Density measurements also reveal an inverse relationship with amine content.


2018 ◽  
Vol 33 (3) ◽  
pp. 289-304 ◽  
Author(s):  
Kuhananthan Nanthakumar ◽  
Chan Ming Yeng ◽  
Koay Seong Chun

This research covers the preparation of poly(lactic acid) (PLA)/sugarcane leaves fibre (SLF) biofilms via a solvent-casting method. The results showed that the tensile strength and Young’s modulus of PLA/SLF biofilms increased with the increasing of SLF content. Nevertheless, the elongation at break showed an opposite trend as compared to tensile strength and Young’s modulus of biofilms. Moreover, water absorption properties of PLA/SLF biofilms increased with the increasing of SLF content. In contrast, the tensile strength and Young’s modulus of biofilms were enhanced after bleaching treatment with hydrogen peroxide on SLF, but the elongation at break and water absorption properties of bleached biofilms were reduced due to the improvement of filler–matrix adhesion in biofilms. The tensile and water properties were further discussed using B-factor and Fick’s law, respectively. Furthermore, the functional groups of unbleached and bleached SLF were characterized by Fourier transform infrared analysis.


2018 ◽  
Vol 29 (1) ◽  
pp. 48-53
Author(s):  
Manuela Gonçalves de Souza e Silva ◽  
Eliseu Aldrighi Münchow ◽  
Rafael Pino Vitti ◽  
Mário Alexandre Coelho Sinhoreti ◽  
Evandro Piva ◽  
...  

Abstract The aim of this study was to synthesize and evaluate physicochemical properties of a new salicylate derivative in experimental calcium-based root canal sealers. Two salicylate derivatives were synthesized for the transesterification reaction of methyl salicylate with two different alcohols (1,3-butylenoglicol disalicylate-BD and pentaerythritol tetrasalicylate -PT) in molar ratio 1:3 and 1:6, respectively. The products (BD and PT), were characterized by Fourier Transform Infrared Spectroscopy (FTIR) and Nuclear Magnetic Resonance spectroscopy (RMN). Calcium-based experimental sealers were prepared with the same catalyst paste (60% of MTA, 39% of n-ethyl-o-toluenesulfonamide, and 1% titanium dioxide) and four different concentrations of BD and PT in the base pastes (40/0 - control, 35/5, 30/10 and 20/20) with 60% of bismuth oxide. The experimental sealers were evaluated for setting time, solubility (24 h, 7, 14 and 30 days), diametral tensile strength and Young’s Modulus. Data were analyzed by one- or two-way ANOVA with Tukey’s test (p<0.05). The addition of PT reduced the materials setting time. After 24 h the sealer 40/0 and 35/5 had higher solubility, and after 14 and 28 days the sealer 20/20 showed the lowest solubility (p<0.05). After 7 days the sealer 20/20 stabilized its solubility. The sealer 40/0 presented the highest values and the 20/20 presented the lowest values of diametral tensile strength and Young’s modulus (p<0.05). The addition of PT to calcium-based root canal sealers provides benefits to the setting time and solubility.


2018 ◽  
Vol 10 (7) ◽  
pp. 168781401878528 ◽  
Author(s):  
Zirong Luo ◽  
Xin Li ◽  
Jianzhong Shang ◽  
Hong Zhu ◽  
Delei Fang

A modified rule of mixtures is required to account for the experimentally observed nonlinear variation of tensile strength. A modified Halpin–Tsai model was presented to predict the Young’s modulus of multiscale reinforced composites with both micron-sized and nano-sized reinforcements. In the composites, both micron-sized fillers—carbon fibers—and nano-sized fillers—rubber nanoparticles and carbon nanotubes—are added into the epoxy resin matrix. Carbon fibers can help epoxy resins increase both the tensile strength and Young’s modulus, while rubber nanoparticles and carbon nanotubes can improve the toughness without sacrificing other properties. Mechanical experiments and scanning electron microscopy observations were used to study the effects of the micron-sized and nano-sized reinforcements and their combination on tensile and toughness properties of the composites. The results showed that the combined use of multiscale reinforcements had synergetic effects on both the strength and the toughness of the composites.


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