coating layer
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2022 ◽  
Vol 12 (1) ◽  
Author(s):  
Yi-Yun Tsai ◽  
Yi-Chen Pan ◽  
Jui-Chao Kuo

AbstractA raw electron backscatter diffraction (EBSD) signal can be empirically decomposed into a Kikuchi diffraction pattern and a smooth background. For pattern indexing, the latter is generally undesirable but can reveal topographical, compositional, or diffraction contrast. In this study, we proposed a new background correction method using polynomial fitting (PF) algorithm to obtain clear Kikuchi diffraction patterns for some applications in nonconductive materials due to coating problems, at low accelerated voltage and at rough sample surfaces and for the requirement of high pattern quality in HR-EBSD. To evaluate the quality metrics of the Kikuchi patterns, we initially used three indices, namely, pattern quality, Tenengrad variance, and spatial–spectral entropy-based quality to detect the clarity, contrast, and noise of Kikuchi patterns obtained at 5 and 15 kV. Then, we examined the performance of PF method by comparing it with pattern averaging and Fourier transform-based methods. Finally, this PF background correction is demonstrated to extract the background images from the blurred diffraction patterns of EBSD measurements at low kV accelerating voltage and with coating layer, and to provide clear Kikuchi patterns successfully.


Small ◽  
2022 ◽  
pp. 2106337
Author(s):  
Jiuding Liu ◽  
Zhonghan Wu ◽  
Meng Yu ◽  
Honglu Hu ◽  
Yudong Zhang ◽  
...  

Ionics ◽  
2022 ◽  
Author(s):  
Mengzhao Ding ◽  
Jianguang Zhai ◽  
Panjing Zeng ◽  
Chaomin Zhang ◽  
Yunxia Ping

2022 ◽  
pp. 110066
Author(s):  
Jiankang Huang ◽  
Yanqin Huang ◽  
Xiaoquan Yu ◽  
Guangyin Liu ◽  
Shurong Yu ◽  
...  

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