No Sample Preparation

Author(s):  
Yang Liu ◽  
George L. Reid ◽  
Zhongli Zhang
Molecules ◽  
2021 ◽  
Vol 26 (2) ◽  
pp. 382
Author(s):  
Barbara Pacholczyk-Sienicka ◽  
Grzegorz Ciepielowski ◽  
Łukasz Albrecht

Spices and herbs are among the most commonly adulterated food types. This is because spices are widely used to process food. Spices not only enhance the flavor and taste of food, but they are also sources of numerous bioactive compounds that are significantly beneficial for health. The healing effects of spices are connected with their antimicrobial, anti-inflammatory and carminative properties. However, regular consumption of adulterated spices may cause fatal damage to our system because adulterants in most cases are unhealthy. For that reason, the appropriate analytical methods are necessary for quality assurance and to ensure the authenticity of spices. Spectroscopic methods are gaining interest as they are fast, require little or no sample preparation, and provide rich structural information. This review provides an overview of the application of NMR spectroscopy combined with chemometric analysis to determine the quality and adulteration of spices.


2017 ◽  
Vol 1061-1062 ◽  
pp. 438-444 ◽  
Author(s):  
Sten Ohlson ◽  
Jagjit Kaur ◽  
Manfred Raida ◽  
Ulf Niss ◽  
Tim Bengala ◽  
...  

Molecules ◽  
2020 ◽  
Vol 25 (7) ◽  
pp. 1719 ◽  
Author(s):  
Alshymaa Aly ◽  
Tadeusz Górecki

Preparing a sample for analysis is a crucial step of many analytical procedures. The goal of sample preparation is to provide a representative, homogenous sample that is free of interferences and compatible with the intended analytical method. Green approaches to sample preparation require that the consumption of hazardous organic solvents and energy be minimized or even eliminated in the analytical process. While no sample preparation is clearly the most environmentally friendly approach, complete elimination of this step is not always practical. In such cases, the extraction techniques which use low amounts of solvents or no solvents are considered ideal alternatives. This paper presents an overview of green extraction procedures and sample preparation methodologies, briefly introduces their theoretical principles, and describes the recent developments in food, pharmaceutical, environmental and bioanalytical chemistry applications.


1978 ◽  
Vol 24 (7) ◽  
pp. 1182-1185 ◽  
Author(s):  
B L Therrell ◽  
J M Drosche ◽  
T W Dziuk

Abstract We describe a modified tantalum ribbon atomic absorption procedure for determining lead in undiluted whole blood. An instrumentation Laboratory (I.L.) Model 151 atomic absorption spectrophotometer equipped with an I.L. Model 355 Flameless Sampler was used. The Flameless Sampler was slightly modified to include three-cycle operation instead of the normal two cycles. This modified single-beam system, equipped with background correction, allows 5-microliter specimens of whole blood to be quickly and accurately analyzed. No sample preparation other than vortex mixing is involved and method reliability has been demonstrated during an extended period of successful participation in proficiency testing studies conducted by the Center for Disease Control. This tantalum ribbon methodology has further been demonstrated to be effective both as a primary screening procedure and as a confirmatory procedure, when coupled with erythrocyte protoporphyrin determinations, in screening over 300 000 clients during a three-year period of use in the Early and Periodic Screening, Diagnosis and Treatment (EPSDT) Program in Texas.


1999 ◽  
Vol 7 (2) ◽  
pp. 22-23
Author(s):  
Barbara Foster

Recently, a question surfaced on the Microscopy list server regarding preparation of insect eggs for EM evaluation. While the electron microscopy approach involved considerable sample preparation (mounting, coating, etc.), our experience indicated that, for some of these applications, a combination of reflected and fluorescent confocal microscopy provided valuable information with little or no sample preparation required, provided there are not other considerations such as the extended resolution provided by electron microscopy.In the biological arena, most confocal work is done in fluorescence mode, There have been some forays into imaging silver-stained structures using reflected light confocal but those applications have not been very prevalent in the literature. With the judicious addition of a quarter wave plate (a polarizing accessory) in the light path, the disruptive artifact from the laser beam can be removed from the image, converting any confocal into a dual purpose instrument.


1995 ◽  
Vol 78 (3) ◽  
pp. 730-735 ◽  
Author(s):  
Jeffrey N Leebowitz ◽  
Rafael Sarmiento ◽  
Sumer M Dugar ◽  
Michael W Ethridge

Abstract Two direct sample injection methods using liquid chromatography (LC) and gas chromatography coupled with mass spectrometry (GC/MS) were used to determine phthalate residues in grain neutral spirits and vodka. Six reported phthalates were quantitated at concentrations as low as 20 μg/L (20 ppb) with no sample preparation or sample enrichment.


2006 ◽  
Vol 1 (1) ◽  
Author(s):  
G. Gruber ◽  
J.-L. Bertrand-Krajewski ◽  
J. De Beneditis ◽  
M. Hochedlinger ◽  
W. Lettl

An explosion-proof UV/VIS sensor has been available even in sewer systems for some years for simultaneous measurement of CODeq, filtered CODeq, TSSeq and nitrateeq. This sensor allows in-situ real-time measurements with no sampling, no sample preparation and no reagents. Three case studies are presented in this paper using this UV/VIS sensor for long-term sewer monitoring issues whereby two different installation strategies are applied. The pros and cons of both different installation solutions are compared and different calibration results during dry and wet weather conditions and long-term operational sewer monitoring experiences are given in this paper.


Sensors ◽  
2021 ◽  
Vol 21 (4) ◽  
pp. 1373
Author(s):  
Leonardo Franceschelli ◽  
Annachiara Berardinelli ◽  
Sihem Dabbou ◽  
Luigi Ragni ◽  
Marco Tartagni

Standard analytical methods for fish freshness assessment are based on the measurement of chemical and physical attributes related to fish appearance, color, meat elasticity or texture, odor, and taste. These methods have plenty of disadvantages, such as being destructive, expensive, and time consuming. All these techniques require highly skilled operators. In the last decade, rapid advances in the development of novel techniques for evaluating food quality attributes have led to the development of non-invasive and non-destructive instrumental techniques, such as biosensors, e-sensors, and spectroscopic methods. The available scientific reports demonstrate that all these new techniques provide a great deal of information with only one test, making them suitable for on-line and/or at-line process control. Moreover, these techniques often require little or no sample preparation and allow sample destruction to be avoided.


1992 ◽  
Vol 46 (2) ◽  
pp. 246-248 ◽  
Author(s):  
Michael A. Friese ◽  
Sujit Banerjee

The lignin content of pulp is determined from its diffuse reflectance infrared spectrum by an algorithm that calculates the degree of overlap between two spectra. The lignin:cellulose fraction correlates with kappa number, a titrimetric measure of lignin. Essentially no sample preparation is required, and the procedure is insensitive to variations in moisture content. The algorithm is able to detect changes induced by exposure of pulp to NO2.


1982 ◽  
Vol 36 (5) ◽  
pp. 582-584 ◽  
Author(s):  
M. J. D. Low ◽  
M. Lacroix ◽  
C. Morterra

Infrared spectra were recorded of organic and inorganic solids with a Fourier transform spectrometer built to operate with a photothermal beam deflection detector. No sample preparation or cells per se is needed to examine milligram quantities of powder. The total absence of sample-containing devices makes it possible to examine portions of the surfaces of objects which are very large in size. Sample heating may occur, so that care must be taken with heat-sensitive materials.


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