Qualitative Phase Analysis Using an X-Ray Powder Diffractometer

1981 ◽  
pp. 91-97 ◽  
Author(s):  
W. N. Schreiner ◽  
C. Surdukowski ◽  
R. Jenkins
Keyword(s):  
Phase Analysis ◽  
X Ray ◽  
Powder Diffractometer ◽  
Qualitative Phase

Qualitative phase analysis system for crystalline mixtures based on X-ray powder diffraction file

2004 ◽  
Vol 19 (4) ◽  
pp. 340-346
Author(s):  
YuanYuan Qiao ◽  
YunFei Xi ◽  
DongTao Zhuo ◽  
Ji Jun Wang ◽  
ShaoFan Lin
Keyword(s):  
Phase Analysis ◽  
Powder Diffraction ◽  
Identification System ◽  
Phase Identification ◽  
Powder Diffraction File ◽  
X Ray ◽  
Analysis System ◽  
Qualitative Phase ◽  
Full Peak

A qualitative phase identification system for crystalline mixtures is presented. The system provides up to five-phase qualitative identification using up to nine-peak filtration, and additive full peak matching based on the powder diffraction file of ICDD. It was implemented using Microsoft Visual C++, and runs under most common Windows systems. Screenshots and examples are included.

Qualitative Phase Analysis Using an X-Ray Powder Diffractometer

1980 ◽  
Vol 24 ◽  
pp. 91-97
Author(s):  
W. N. Schreiner ◽  
C. Surdukowski ◽  
R. Jenkins
Keyword(s):  
Qualitative Analysis ◽  
Phase Analysis ◽  
Powder Diffraction ◽  
X Ray ◽  
Qualitative And Quantitative ◽  
The Past ◽  
Quantitative Analyses ◽  
Improved Performance ◽  
Qualitative Phase ◽  
Self Consistency

During the past three years we have undertaken the development of a complete X-Ray Powder Diffraction, facility with the goal of fully integrating experimental and analytical procedures. Such an approach potentially offers substantially improved performance over previously existing systems by virtue of its internal self-consistency and it opens the possibility of significantly extending analytic procedures for both qualitative and quantitative analyses. Our work to date has resulted in improved performance and significant extensions in both areas, and today I will report on those advances in the area of qualitative analysis.

Qualitative and quantitative phase analyses of Pingguo bauxite mineral using X-ray powder diffraction and the Rietveld method

2007 ◽  
Vol 22 (4) ◽  
pp. 300-302 ◽  
Author(s):  
Liangqin Nong ◽  
Xiying Yang ◽  
Lingmin Zeng ◽  
Jingping Liu
Keyword(s):  
Rietveld Refinement ◽  
Phase Analysis ◽  
Powder Diffraction ◽  
Rietveld Method ◽  
X Ray ◽  
Quantitative Phase ◽  
Qualitative And Quantitative ◽  
Refinement Method ◽  
Quantitative Analyses ◽  
Qualitative Phase

X-ray powder diffraction technique and the Rietveld refinement method have been used successfully for the qualitative and quantitative analyses of Pingguo bauxite from Guangxi, China. Qualitative phase analysis shows that the Pingguo bauxite contains diaspore (AlOOH), hematite (Fe2O3), goethite (FeOOH), anatase (TiO2), and kaolinite (Al2(Si2O5)(OH)4). Quantitative Rietveld refinement shows that the weight concentrations of diaspore, goethite, hematite, anatase, and kaolinite for the Pingguo bauxite are 71.9(4)%, 7.0(8)%, 11.3(7)%, 6.5(6)%, and 3.3(9)%, respectively.

Determination of the qualitative phase composition of a ceramic by x-ray phase analysis

1992 ◽  
Vol 49 (9) ◽  
pp. 435-437
Author(s):  
E. M. Dyatlova ◽  
N. M. Bobkova ◽  
T. N. Yurkevich ◽  
E. M. Kurpan
Keyword(s):  
Phase Composition ◽  
Phase Analysis ◽  
X Ray ◽  
Qualitative Phase

Quantitative Phase Analyses of a Slag Using X-Ray Powder Diffraction

2014 ◽  
Vol 881-883 ◽  
pp. 1241-1244
Author(s):  
Wei Jin Zeng ◽  
Chao Zeng ◽  
Wei He
Keyword(s):  
Quantitative Analysis ◽  
Phase Analysis ◽  
Powder Diffraction ◽  
Rietveld Method ◽  
Quantitative Phase Analysis ◽  
Powder Diffraction Data ◽  
X Ray ◽  
Quantitative Phase ◽  
Full Profile ◽  
Qualitative Phase

The quantitative phase analyses of a slag have been successfully carried out by using both of the full-profile Rietveld and RIR methods from X-ray powder diffraction data. The qualitative phase analysis indicates that the slag contains mayenite (CaO)12(Al2O3)7, olivine Ca2(SiO4), gehlenite Ca2Al (AlSiO7), lemite Ca2(SiO4) and hibonite CaO(Al2O3)6. The quantitative analysis from Rietveld refinement shows that the weight concentrations of mayenite, olivine, gehlenite, lemite and hibonite for the slag are 48.8(4) wt.%, 32.2(5) wt.%, 11.0(9) wt.%, 6.2(1.1) wt.% and 1.8 (1.2) wt.%, respectively. The quantitative phase analysis results obtained by Rietveld method are more precise then those by RIR method.

Composition of pigments of Santorini frescoes: The Rietveld method as an aid in qualitative phase analysis

2004 ◽  
Vol 19 (2) ◽  
pp. 145-148 ◽  
Author(s):  
Svend Erik Rasmussen ◽  
Sidsel Grundvig ◽  
Walter L. Friedrich
Keyword(s):  
Bronze Age ◽  
Phase Analysis ◽  
Rietveld Method ◽  
X Ray Diffraction ◽  
X Ray ◽  
On Line ◽  
Volcanic Islands ◽  
Line Positions ◽  
Qualitative Phase

Ten fragments of bronze age frescoes from the Greek group of volcanic islands known as Santorini have been examined by powder X-ray diffraction. A qualitative phase analysis based on line positions only was supplemented by the Rietveld method which uses complete diffraction profiles to increase the credibility of the phase analysis.

Rapid qualitative phase analysis in highly textured thin films by x-ray diffraction

2008 ◽  
Vol 79 (4) ◽  
pp. 043904 ◽  
Author(s):  
Cesare Borgia ◽  
Sven Olliges ◽  
Ralph Spolenak
Keyword(s):  
Thin Films ◽  
Phase Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Qualitative Phase

Texture Correction in Phase Analysis and Thin Film Studies

1986 ◽  
Vol 1 (2) ◽  
pp. 28-32 ◽  
Author(s):  
V. Valvoda
Keyword(s):  
Thin Film ◽  
Phase Analysis ◽  
Film Studies ◽  
Preferred Orientation ◽  
Crystallographic Plane ◽  
Direct Integration ◽  
Surface Layers ◽  
X Ray ◽  
Powder Diffractometer ◽  
Special Cases

AbstractA method is presented for correction of integrated X-ray intensities for preferred orientation of crystallites in a spinning specimen. It is based upon direct integration of the data obtainable from pole distribution of a single crystallographic plane. This pole distribution can be determined from measurements on a texture goniometer or, in special cases, from an ω-scan or from intensities of all reflections measured on a powder diffractometer only. The method was tested on four samples of magnesium and magnesium cadmium alloys and applied to hexagonal BN and α-Ti(N) surface layers. The method was developed with regard to application in phase analysis and thin film studies.

X-ray phase analysis in leucite systems

2007 ◽  
Vol 2007 (suppl_26) ◽  
pp. 531-536 ◽  
Author(s):  
J. Maixner ◽  
A. Kloužková ◽  
M. Mrázová ◽  
M. Kohoutková
Keyword(s):  
Phase Analysis ◽  
X Ray
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