Effects of Plastic Deformation and Aging Treatment on Phase Precipitation in Ti2AlNb Alloy

Author(s):  
Yanqi Fu ◽  
Zhenshan Cui
Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2742
Author(s):  
Furong Chen ◽  
Chenghao Liu

To improve the loose structure and serious porosity of (Al–Zn–Mg–Cu) 7075 aluminum alloy laser-welded joints, aging treatment, double-sided ultrasonic impact treatment (DSUIT), and a combination of aging and DSUIT (A–DSUIT) were used to treat joints. In this experiment, the mechanism of A–DSUIT on the microstructure and properties of welded joints was analyzed. The microstructure of the welded joints was observed using optical microscopy, scanning electron microscopy, and electron backscatter diffraction (EBSD). The hardness and tensile properties of the welded components under the different processes were examined via Vickers hardness test and a universal tensile testing machine. The results showed that, after the aging treatment, the dendritic structure of the welded joints transformed into an equiaxed crystal structure. Moreover, the residual tensile stress generated in the welding process was weakened, and the hardness and tensile strength were significantly improved. After DSUIT, a plastic deformation layer of a certain thickness was generated from the surface downward, and the residual compressive stress was introduced to a certain depth of the joint. However, the weld zone unaffected by DSUIT still exhibited residual tensile stress. The inner microhardness of the joint surface improved; the impact surface hardness was the largest and gradually decreased inward to the weld zone base metal hardness, with a small improvement in the tensile strength. Compared with the single treatment process, the microstructural and mechanical properties of the welded joint after A–DSUIT were comprehensively improved. The microhardness and tensile strength of the welded joint reached 200 HV and 615 MPa, respectively, for an increase of 45.8% and 61.8%, respectively. Observation of the fractures of the tensile specimens under the different treatment processes showed that the fractures before the aging treatment were mainly ductile fractures while those after were mainly brittle fractures. After DSUIT of the welded joints, a clear and dense plastic deformation layer was observed in the fracture of the tensile specimens and effectively improved the tensile properties of the welded joints. Under the EBSD characterization, the larger the residual compressive stress near the ultrasonic impact surface, the smaller the grain diameter and misorientation angle, and the lower the texture strength. Finally, after A–DSUIT, the hardness and tensile properties improved the most.


2013 ◽  
Vol 738-739 ◽  
pp. 189-194 ◽  
Author(s):  
Vladimir Brailovski ◽  
Sergey Prokoshkin ◽  
Karine Inaekyan ◽  
Sergey Dubinskiy

The influence of thermomechanical processing on the Ti-21.8Nb-6Zr (TNZ) and Ti-19.7Nb-5.8Ta (TNT) (at%) alloys’ structure, phase composition, mechanical and functional properties is studied. Both alloys possess polygonized dislocation substructure (average subgrain size  100 nm), and manifest superelastic behavior at room temperature and recovery stress generation during constant-strain temperature scanning experiments. After aging treatment, both alloys were -phase precipitation hardened, but their mechanical behavior was impacted differently -- it was detrimental for TNZ and beneficial for TNT. The different impact of aging heat treatment on the mechanical behavior of these alloys is explained by the differences in the -phase nucleation rate, precipitates’ size, shape, volume fraction and distribution, and by their effect on the alloys’ critical stresses and transformation temperatures.


Author(s):  
Lin Wang ◽  
Qiao-Yun Qin ◽  
Fan Zhang ◽  
Cheng-Wen Tan

Abstract Magnesium alloy is very attractive in many industrial applications due to its low density. The structure-property relationships of the magnesium alloy under quasi-static loading have been extensively investigated. However, the dynamic behavior, particularly the mechanism of high-rate plastic deformation, of the magnesium alloy requires more in-depth investigations. In this paper, the effect of aging treatment on the quasi-static and dynamic properties of a typical rare earth Mg-Gd-Y magnesium alloy is investigated. In particular, the plastic deformation mechanism under dynamic compression loading is discussed. Split Hopkinson Pressure Bar (SHPB) was used to carry out dynamic compression tests with controllable plastic deformation by using stopper rings. The experimental results demonstrate that both static and dynamic properties of the Mg-Gd-Y alloy vary under various aging treatment conditions (under-aged, peak-aged and over-aged conditions), due to two different kinds of second phases: remnant micro size phase from solid solution treatment and nano precipitation from aging treatment. The results of microstructure characterization and statistic analysis of the metallographic phase are presented. The area fraction of the twinned grains increases due to aging treatment and dynamic loading. The main plastic deformation mechanism of the rare earth Mg-Gd-Y magnesium alloy is possibly dislocation slip, rather than twinning for the conventional AZ31 magnesium alloy under high strain rate loading.


2019 ◽  
Vol 11 (11) ◽  
pp. 1489-1501
Author(s):  
Wenjing He ◽  
Caihe Fan ◽  
Shu Wang ◽  
Junhong Wang ◽  
Su Chen ◽  
...  

The evolution of nanoprecipitated phases in Al–Cu alloys under severe plastic deformation (SPD) is summarized in this study. SPD at room temperature induces the precipitation of Al–Cu alloys to dissolve, leading to the reformation of supersaturated solid solution in the aluminum matrix. In the process of SPD or aging treatment after the SPD, the reprecipitated phases are precipitated from the aluminum matrix and the mechanical properties of the alloys are remarkably improved. The mechanism and system of the redissolution of the precipitation phases and the effects of redissolution and reprecipitation on the microstructure and properties of Al–Cu alloys are comprehensively analyzed. The development and future of redissolution and reprecipitation of nanoprecipitated phases in Al–Cu alloys are also described.


2010 ◽  
Vol 667-669 ◽  
pp. 599-604
Author(s):  
Dai Hong Xiao ◽  
Min Song ◽  
Kang Hua Chen

The Al-Cu-Mg-Ag heat-resistant alloy were prepared by ingot metallurgy technology. Effects of serve plastic deformation on microstructure and mechanical properties of the alloy were investigated by microscopy, differential scanning calorimetry and hardness tester. It has been shown that serve plastic deformation in the solid solution and quenching state with aging treatment was found to be quite effective in refining the grains to 2 μm, and improving the mechanical properties and heat-resistant properties of the extruded Al-Cu-Mg-Ag alloy. Serve plastic deformation treatment accelerates the aging hardening process of the extruded alloys, increases the density of precipitate phase.


Author(s):  
Lin Wang ◽  
Qiao-Yun Qin ◽  
Fan Zhang ◽  
Cheng-Wen Tan

AbstractMagnesium alloy is very attractive in many industrial applications due to its low density. The structure-property relationships of the magnesium alloy under quasi-static loading have been extensively investigated. However, the dynamic behavior, particularly the mechanism of high-rate plastic deformation, of the magnesium alloy requires more in-depth investigations. In this paper, the effect of aging treatment on the quasi-static and dynamic properties of a typical rare earth Mg-Gd-Y magnesium alloy is investigated. In particular, the plastic deformation mechanism under dynamic compression loading is discussed. Split Hopkinson Pressure Bar (SHPB) was used to carry out dynamic compression tests with controllable plastic deformation by using stopper rings. The experimental results demonstrate that both static and dynamic properties of the Mg-Gd-Y alloy vary under various aging treatment conditions (under-aged, peak-aged and over-aged conditions), due to two different kinds of second phases: remnant micro size phase from solid solution treatment and nano precipitation from aging treatment. The results of microstructure characterization and statistic analysis of the metallographic phase are presented. The area fraction of the twinned grains increases due to aging treatment and dynamic loading. The main plastic deformation mechanism of the rare earth Mg-Gd-Y magnesium alloy is possibly dislocation slip, rather than twinning for the conventional AZ31 magnesium alloy under high strain rate loading.


Author(s):  
Jože Pirš ◽  
Marija Pavlin

In most age-hardening aluminum alloys, metallographic studies have shown that the extent of precipitation adjacent to grain boundaries is much less than that which occurs in the interior of the grains. The width of these almost precipitate-free regions, which are sometimes called denuded zones, and the extent of solute depletion with them are dependent upon the particular alloy and its aging treatment. It has been observed that these zones are relatively soft with the result that plastic deformation takes place preferentially within them. It has been shown 2-4 that there exists a tendency for intercrystalline cracking in fatigue when such zones are present. It is of interest to note that Broom et al. were able to reduce the incidence of this type of failure in an Al- 4 wt pct Cu alloy by stretching the material 10 pct prior to aging. This was later confirmed also on Al - 10 wt pct Mg alloy.


2015 ◽  
Vol 812 ◽  
pp. 239-245
Author(s):  
Judit Pázmán ◽  
Péter Bereczki ◽  
Balázs Verő ◽  
Ibolya Kardos ◽  
Jánosné Fehér

The AlMgSi1 alloy is generally used in automotive industry owing to its excellent mechanical properties, which can be further improved by applying severe plastic deformation and heat treatment. The dislocation density in the material increases significantly during severe plastic deformation due to the characteristic intensive shear strain. Therefore the motion of dislocations becomes more and more retarded, consequently the strength improves. In addition, the motion of dislocations can be prevented by aging due to formation of coherent precipitations in the metal matrix in order to realize further increasing in strength. In this paper the combined effect of severe plastic deformation and artificial aging treatment on the evolution of mechanical properties was investigated. The samples were subjected to multiple forging (MF) process at room and enhanced temperature. One part of the deformed samples were heat treated at 150°C for different times. The deformed as well as deformed and heat treated samples were investigated by micro hardness testing and X-ray profile analysis.


2006 ◽  
Vol 118 ◽  
pp. 431-436
Author(s):  
Il Ho Kim ◽  
S.I. Kwun

The formation behavior of γ″(Ni3Nb) precipitates in IN 718 alloy before and after ECAP(equal channel angular pressing) was investigated by microstructural observation and the hardness test. For the alloy examined before ECAP, the γ″ precipitates were formed only after aging treatment at 720, whereas after ECAP, the γ″ precipitates were formed at the aging temperatures of both 600 and 720. 600 is normally too low a temperature for γ″ precipitates to be formed in commercial IN 718 alloy, however, they were able to be formed due to severe plastic deformation by ECAP. It was found that the ECAP process changed the formation behavior of the γ″ precipitates in IN 718 alloy.


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