Multivariate analysis to select chemical compounds and rheological parameters as predictors of bread quality: interaction of wheat genotype and particle size of fine bran

Author(s):  
Ofelia Rouzaud-Sández ◽  
Alán Pavlovich-Abril ◽  
María Guadalupe Salazar-García ◽  
Rosario Maribel Robles-Sánchez ◽  
Reyna Luz Vidal-Quintanar
2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Fatemeh Ahmadi ◽  
Abbas Samadi ◽  
Ebrahim Sepehr ◽  
Amir Rahimi ◽  
Sergey Shabala

AbstractMedicinal plants are considered as one of the most important sources of chemical compounds, so preparing a suitable culture media for medicinal plant growth is a critical factor. The present study is aimed to improve the caffeic acid derivatives and alkylamides percentages of Echinacea purpurea root extract in hydroponic culture media with different perlite particle size and NO3−/NH4+ ratios. Perlite particle size in the growing media was varied as very coarse perlite (more than 2 mm), coarse perlite (1.5–2 mm), medium perlite (1–1.5 mm), fine perlite (0.5–1 mm), and very fine perlite (less than 0.5 mm) in different ratios to peat moss (including pure perlite, 50:50 v/v, 30:70 v/v, and pure peat moss). Two NO3−/NH4+ ratios (90:10 and 70:30) were tested in each growing media. All phytochemical analyses were performed according to standard methods using high performance liquid chromatography (HPLC). It was found that the E. purpurea grown in the medium containing very fine-grade perlite with 50:50 v/v perlite to peat moss ratio had the maximum caffeic acid derivatives, including chicoric acid (17 mg g−1 DW), caftaric acid (6.3 mg g−1 DW), chlorogenic acid (0.93 mg g−1 DW), cynarin (0.84 mg g−1 DW), and echinacoside (0.73 mg g−1 DW), as well as, alkylamides (54.21%). The percentages of these phytochemical compounds increased by decreasing perlite particle size and increasing of NO3−/NH4+ ratio. The major alkylamide in the E. purpurea root extract was dodeca-2E, 4E, 8Z-10 (E/Z)-tetraenoic acid isobutylamide in all treatments, ranging from 31.12 to 54.21% of total dry weight. It can be concluded that optimizing hydroponic culture media and nutrient solution has significant effects on E. purpurea chemical compounds.


2001 ◽  
Vol 15 (06n07) ◽  
pp. 649-656 ◽  
Author(s):  
H. J. CHOI ◽  
J. W. KIM ◽  
M. S. SUH ◽  
M. J. SHIN ◽  
K. TO

Copolyanilines are synthesized by a chemical oxidation of aniline and o-ethoxyaniline with various molar ratios in an acidic media, and then characteristics of these polymers such as chemical structure, particle size and the particle size distribution were examined by using FT-IR, SEM and particle size analyzer, respectively. Suspensions of copolyaniline containing ethoxy group, namely poly(aniline-co-o-ethoxyaniline), in silicone oil have been investigated as one of many potential candidates for dry-base electrorheological (ER) fluid systems. Rotational rheometer (Physica) equipped with a high voltage generator was used to characterize the rheological properties of ER fluids from both steady shear and dynamic tests. From the steady shear experiment, we obtained flow properties and found that ER fluids exhibited the yield phenomenon. On the other hand, viscoelastic property was also obtained from the dynamic experiment. Since viscoelastic properties for ER fluids are mainly dominated by the particle chain structure, the state at different time scale was analyzed from the rheological parameters such as storage modulus (G'), loss modulus (G'') and tan δ. We conducted a strain amplitude sweep at 1 Hz under an applied electric field to determine a linear viscoelastic region first. The G' and G'' were then measured by a frequency sweep from 0.1 to 100 Hz in the linear viscoelastic region.


2020 ◽  
Vol 11 (4) ◽  
pp. 3610-3620 ◽  
Author(s):  
Suyun Lin ◽  
Jing Gao ◽  
Xiaoxuan Jin ◽  
Yong Wang ◽  
Zhizhong Dong ◽  
...  

Whole-wheat flour (WWF) particle size is critical to dough properties, bread quality, and in vitro starch digestibility of bread.


2012 ◽  
Vol 89 (5) ◽  
pp. 223-229 ◽  
Author(s):  
Juan Mario Sanz-Penella ◽  
José Moisés Laparra ◽  
Yolanda Sanz ◽  
Monika Haros

1965 ◽  
Vol 5 (01) ◽  
pp. 6-14 ◽  
Author(s):  
R.F. Burdyn

Abstract The inadequate use of centrifugation to economically recover solids from weighted drilling fluids reflects the need for better equipment and techniques for this purpose. Laboratory studies in the development of an improved separator are described in which an operating equation is derived and tested. Results show that the concentric cylinder geometry employed effectively separates barite from a suspension and that the operating equation provides a good approximation for scale-up. Introduction Our current drilling technology frequently requires a high-density drilling fluid obtained by addition of barite. In the course of drilling, formation solids which are too fine to be removed either by screening or settling become suspended in the drilling fluid and gradually the volume of solids in the mud increases. The volume fraction of solids must be limited (if a satisfactory set of rheological parameters are to be maintained). A centrifugal separator provides an economical way of accomplishing this. The barite recovery process can be considered as a separation of two solids. One, the light solids, composed of formation and added solids, has a specific gravity of 2.6 to 2.7; the other, barite, has a specific gravity of 4.2 to 4.3. This density difference, plus the fact that the average light-solids particle size is much smaller than the average barite particle size, permits separation by a centrifuge. In drilling fluids some of the coarse particles of the light-solids-range will settle faster than fine particles of the barite-particle range. As a result a complete separation of the two species is not possible. Since the object of the process is not merely recovering the maximum amount of barite but includes as well removing the maximum amount of light solids, an optimum barite recovery efficiency exists. From a practical standpoint this optimum cannot be determined in the field for each drilling fluid system, and in practice the separation is less than optimum, with some sacrifice of barite. Drilling technology has included centrifugal separators for barite recovery for more than a decade. Results have been reported by a number of investigators indicating that the process is practical and economical. The decision to use a centrifuge is based on economics in which direct cost savings and the indirect benefits in rig time derived from improvement of the drilling fluid are important factors. One would expect that centrifugal separation of barite from drilling fluids would significantly affect barite consumption; however, this is not the case. The Minerals Yearbook shows an annual domestic barite consumption in the drilling industry of nearly I million tons. By rough estimate there are perhaps 80 separators presently in field use. Assuming half of these in use at any one time, operating an, average of four hours per day, at recovery rates averaging 3,000 lb of barite per hour, total annual recovery is about 90,000 tons. This is less than 10 per cent of the total barite used. I conservatively estimate that barite consumption in drilling operations can be reduced by 30 per cent through greater utilization of centrifugal separators. To encourage more wide- spread acceptance of centrifugal separators in the drilling industry, improved equipment and techniques would be very desirable. The present paper, covering theory and results obtained from a laboratory model, is the first in a series on the development of an improved mud separator for field use. THE CONCENTRIC CYLINDER GEOMETRY AS A SEPARATING DEVICE Consider the geometry shown in Fig. 1, consisting of two concentric cylinders separated by an annular space. These are arranged so that the outer cylinder is fixed and the inner one can be rotated about its axis on shafts sealed against the ends of the outer cylinder. SPEJ P. 6ˆ


2010 ◽  
Vol 52 (1) ◽  
pp. 59-64 ◽  
Author(s):  
Martijn W.J. Noort ◽  
Daan van Haaster ◽  
Youna Hemery ◽  
Henk A. Schols ◽  
Rob J. Hamer

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