Determination of lipophilic metabolites for species discrimination and quality assessment of nine leafy vegetables

2015 ◽  
Vol 58 (6) ◽  
pp. 909-918 ◽  
Author(s):  
Tae Jin Kim ◽  
Kyoung Bok Lee ◽  
Seung-A Baek ◽  
Jaehyuk Choi ◽  
Sun-Hwa Ha ◽  
...  
Keyword(s):  
Quality Assessment ◽  
Leafy Vegetables ◽  
Species Discrimination

The Development of a Turbidimetric Method for the Quantitative Determination of Antibiotics of the Aminoglycoside Group in Medications

2020 ◽  
Vol 65 (7-8) ◽  
pp. 37-41
Author(s):  
E. N. Semenova ◽  
S. I. Kuleshova ◽  
E. I. Sakanyan
Keyword(s):  
Quantitative Determination ◽  
Quality Assessment ◽  
Aminoglycoside Antibiotics ◽  
Metrological Characteristics ◽  
Streptomycin Sulfate ◽  
Turbidimetric Method ◽  
Validation Criteria ◽  
Validation Parameters ◽  
Validation Tests

A method for the quantitative determination of streptomycin sulfate in medicines by the turbidimetric method has been developedand validated. Based on the results of the experiments, it was found that the metrological characteristics of such validation parameters of the method as linearity, precision, and correctness do not exceed the validation criteria. Linearity was noted in the range of streptomycin concentrations from 3.75 to 8.43 μg/ml. The results of validation tests of the method for the quantitative determination of streptomycin indicate the prospects and feasibility of introducing the turbidimetric method into the domestic system for standardization and quality assessment of aminoglycoside antibiotics.

scholarly journals External Quality Assessment for the Determination of Diphtheria Antitoxin in Human Serum

2010 ◽  
Vol 17 (8) ◽  
pp. 1282-1290 ◽  
Author(s):  
Paolo Di Giovine ◽  
Antonella Pinto ◽  
Rose-Marie Ölander ◽  
Dorothea Sesardic ◽  
Paul Stickings ◽  
...  
Keyword(s):  
Quality Assessment ◽  
External Quality Assessment ◽  
Accurate Determination ◽  
Enzyme Linked Immunosorbent Assay ◽  
Reference Laboratory ◽  
Routine Method ◽  
External Quality ◽  
Passive Hemagglutination

ABSTRACT Accurate determination of diphtheria toxin antibodies is of value in determining the rates of immunity within broad populations or the immune status of individuals who may be at risk of infection, by assessing responses to vaccination and immunization schedule efficacy. Here we report the results of an external quality assessment (EQA) study for diphtheria serology, performed within the dedicated surveillance network DIPNET. Twelve national laboratories from 11 European countries participated by testing a standard panel of 150 sera using their current routine method: Vero cell neutralization test (NT), double-antigen enzyme-linked immunosorbent assay (ELISA; DAE), dual double-antigen time-resolved fluorescence immunoassay (dDA-DELFIA), passive hemagglutination assay (PHA), toxin binding inhibition assay (ToBI), and in-house or commercial ELISAs. The objective of the study was not to identify the best assay, as the advantages and drawbacks of methods used were known, but to verify if laboratories using their routine method would have categorized (as negative, equivocal, or positive) a serum sample in the same way. The performance of each laboratory was determined by comparing its results on a quantitative and qualitative basis to NT results from a single reference laboratory, as this test is considered the in vitro “gold standard.” The performance of laboratories using NT was generally very good, while the laboratories’ performance using other in vitro methods was variable. Laboratories using ELISA and PHA performed less well than those using DAE, dDA-DELFIA, or ToBI. EQA is important for both laboratories that use in vitro nonstandardized methods and those that use commercial ELISA kits.

scholarly journals Representative commodity for six leafy vegetables based on the determination of six pesticide residues by gas chromatography

2019 ◽  
Vol 31 (1) ◽  
pp. 49-56 ◽  
Author(s):  
Shiming Song ◽  
Huili Huang ◽  
Zhaojie Chen ◽  
Jie Wei ◽  
Cheng Deng ◽  
...  
Keyword(s):  
Gas Chromatography ◽  
Pesticide Residues ◽  
Leafy Vegetables

scholarly journals A simple and fast multiclass method for determination of steroid hormones in berry fruits, root and leafy vegetables

Talanta Open ◽  
2021 ◽  
pp. 100081
Author(s):  
Francesca Merlo ◽  
Sara Suppini ◽  
Federica Maraschi ◽  
Antonella Profumo ◽  
Andrea Speltini
Keyword(s):  
Steroid Hormones ◽  
Leafy Vegetables ◽  
Berry Fruits

scholarly journals Plant of Lamiaceae family for cultivation at the vertical hydroponic installation

2020 ◽  
pp. 72-75
Author(s):  
I. T. Balashova ◽  
L. V. Bespalko ◽  
A. V. Molchanova ◽  
E. V. Pinchuk ◽  
N. E. Maschenko
Keyword(s):  
Ascorbic Acid ◽  
Secondary Metabolites ◽  
Dry Matter ◽  
Matter Content ◽  
Leafy Vegetables ◽  
Dry Matter Content ◽  
Monarda Fistulosa ◽  
Vertical Farming ◽  
Content Determination

Relevance. Vertical farming – is a new and advanced direction in greenhouse vegetable cultivation. Expansion biodiversity of plants for vertical farming occur with help of green leafy vegetables. Plants of Lamiaceae family are well known as aromatic and medicinal plants with high content of substances with antioxidant activity. It allows use these plants as a base for the functional nutrition. Leafy parts the plants of Lamiaceae family may be used as aromatic and healthy additions to traditional foods, such as salads, soups and sauces.  Goal of the study: analysis the biochemical composition of leafy parts plants of Lamiaceaefamily, cultivated at the multi circle hydroponic construction. Materials and methods. 1) Plants: Monarda fistulosa L. (the breeding sample №5 U.P.), Monarda citriodora Cerv. ex Lag. (Simka variety), Melissa officinalisL. (Zhemchuzhina variety). 2) secondary metabolites: flavonoid glycoside linarozid and steroid glycoside moldstim. Methods. 1) cultivation of plants Lamiaceae family at the 5 circles hydroponic construction; 2) analytic methods: determination of dry matter content, determination of ascorbic acid content, determination sum of chlorophylls and carotenoids, determination sum of antioxidants; 3) statistical methods. Results. First experiment the cultivation of plants Lamiaceae family at the multi circle hydroponic construction was successful. Location of plants at different circles of hydroponic installation didn’t influence the content of dry matter, ascorbic acid and sum of chlorophylls in leafy parts of plants Monarda fistulosaL. The content of dry matter and sum of antioxidants in leafy parts of Monarda fistulosaL. plants of the first cutting is significantly higher than of other cuttings. So, we can recommend the leaves of Monarda fistulosa L. plants of the first cutting for the healthy additions in the scheme of the functional nutrition. Seed treatment with water solutions of secondary metabolites changed significantly the weight of leaves: it was increased in Monarda citriodoraCerv. ex Lag. and in Melissa officinalisL. 

scholarly journals Determination of Fe and Zn Accumulation in Leafy Vegetables and Mushrooms Using Energy Dispersive X-Ray Fluorescence Technique

2011 ◽  
Vol 68 (2) ◽  
Author(s):  
Claudia STIHI ◽  
Gabriela BUSUIOC ◽  
Cristiana RADULESCU ◽  
Carmen ELEKES ◽  
Sorin CIULEI
Keyword(s):  
Leafy Vegetables ◽  
Energy Dispersive ◽  
Wild Edible Mushrooms ◽  
X Ray ◽  
Zn Uptake ◽  
Edxrf Technique ◽  
Armillariella Mellea ◽  
Relationship Of ◽  
The Relationship

The aim of this study was to determine the Fe and Zn concentrations in some leafy vegetables (cabbage, spinach, celery and lettuce) and in their growing soil collected from sites with different industrial activity; in fruiting body of wild edible mushrooms (Armillariella mellea) and in their substrate (soil) collected at different distances by a metal smelter, by using energy dispersive X-ray fluorescence (EDXRF) technique. A quantitative evaluation of the relationship of Fe and Zn uptake by the vegetables and mushrooms from soil was made by calculating the coefficient accumulation Ka. The results reveal that lettuce is a accumulator of Fe and Armillariella mellea is a accumulator of Zn.

Development and Validation of an HPLC Method for the Determination of Thiamine and Riboflavin in Green Leafy Vegetables Using Clara-Diastase

2011 ◽  
Vol 76 (4) ◽  
pp. C639-C642 ◽  
Author(s):  
Alicia del Carmen Mondragón-Portocarrero ◽  
Lourdes Vázquez-Odériz ◽  
MaÁngeles Romero-Rodríguez
Keyword(s):  
Hplc Method ◽  
Leafy Vegetables ◽  
Green Leafy Vegetables ◽  
Development And Validation
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