scholarly journals Fabrication of porous TiO2 foams by powder metallurgy technique and study of bulk crushing strength for biomedical application

Author(s):  
Farida Ahmed Koly ◽  
Md. Arafat Rahman ◽  
Md. Saiful Islam ◽  
Md. Mizanur Rahman
2021 ◽  
Vol 18 (23) ◽  
pp. 683
Author(s):  
Bappi Sarker ◽  
Md. Arafat Rahman ◽  
Md. Mizanur Rahman ◽  
Md. Saiful Islam

Despite the importance of Nickel Oxide (NiO) in diverse functional applications, very little information is available on the mechanical properties of bulk or porous NiO or, mostly unnoticed. In this study, porous Ni-NiO foam was synthesized using space holding-powder metallurgy and sintering methods to produce opened-cell structure with macrogravel and Neolamarckia cadamba (Cadamba flower) like surface morphology. Four different types of porous Ni-NiO with different pore diameter of 35.65 ± 12.77, 36.10 ± 8.85, 68.20 ±7.36 and 62.45 ± 17.48 µm were fabricated for evaluating the effect of porosity on the mechanical properties of bulk porous Ni-NiO foam. The mechanical properties such as bulk crushing force of as synthesized Ni-NiO foam with various porosities such as 20.55, 27.35, 27.85 and 28.82 % exhibited the average crushing load of 115.40, 39.95, 138.10 and 151.20 N, respectively. This study suggests that crushing load of Ni-NiO foam is not only depending on the porosity but also on the sintering temperature and crystallite sizes of NiO. HIGHLIGHTS Ni-NiO foam is synthesized using space holding-powder metallurgy and sintering methods Different pore diameter is fabricated for evaluating the effect of porosity on the mechanical properties of bulk porous Ni-NiO foam Crushing strength of Ni-NiO foam is not only depending on the porosity but also on the sintering temperature and crystallite sizes of NiO GRAPHICAL ABSTRACT


2021 ◽  
Vol 30 (2) ◽  
pp. 1207-1220
Author(s):  
Amarjit Singh ◽  
Jarnail Singh ◽  
Manoj Kumar Sinha ◽  
Ravi Kumar ◽  
Vikram Verma

Crystals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 540
Author(s):  
Mohamed Ali Hassan ◽  
Hossam M. Yehia ◽  
Ahmed S. A. Mohamed ◽  
Ahmed Essa El-Nikhaily ◽  
Omayma A. Elkady

To improve the AlCoCrFeNi high entropy alloys’ (HEAs’) toughness, it was coated with different amounts of Cu then fabricated by the powder metallurgy technique. Mechanical alloying of equiatomic AlCoCrFeNi HEAs for 25 h preceded the coating process. The established powder samples were sintered at different temperatures in a vacuum furnace. The HEAs samples sintered at 950˚C exhibit the highest relative density. The AlCoCrFeNi HEAs model sample was not successfully produced by the applied method due to the low melting point of aluminum. The Al element’s problem disappeared due to encapsulating it with a copper layer during the coating process. Because the atomic radius of the copper metal (0.1278 nm) is less than the atomic radius of the aluminum metal (0.1431 nm) and nearly equal to the rest of the other elements (Co, Cr, Fe, and Ni), the crystal size powder and fabricated samples decreased by increasing the content of the Cu wt%. On the other hand, the lattice strain increased. The microstructure revealed that the complete diffusion between the different elements to form high entropy alloy material was not achieved. A dramatic decrease in the produced samples’ hardness was observed where it decreased from 403 HV at 5 wt% Cu to 191 HV at 20 wt% Cu. On the contrary, the compressive strength increased from 400.034 MPa at 5 wt% Cu to 599.527 MPa at 15 wt% Cu with a 49.86% increment. This increment in the compressive strength may be due to precipitating the copper metal on the particles’ surface in the nano-size, reducing the dislocations’ motion, increasing the stiffness of produced materials. The formability and toughness of the fabricated materials improved by increasing the copper’s content. The thermal expansion has increased gradually by increasing the Cu wt%.


2020 ◽  
Vol 38 (3) ◽  
pp. 273-286 ◽  
Author(s):  
Cristina Garcia-Cabezon ◽  
Celia Garcia-Hernandez ◽  
Maria L. Rodriguez-Mendez ◽  
Gemma Herranz ◽  
Fernando Martin-Pedrosa

AbstractMicrostructural changes that result in relevant improvements in mechanical properties and electrochemical behavior can be induced using different sintering conditions of ASTM F75 cobalt alloys during their processing using powder metallurgy technique. It has been observed that the increase in carbon and nitrogen content improves corrosion resistance and mechanical properties as long as the precipitation of carbides and nitrides is avoided, thanks to the use of rapid cooling in water after the sintering stage. In addition, the reduction of the particle size of the powder improves hardness and resistance to corrosion in both acid medium with chlorides and phosphate-buffered medium that simulates the physiological conditions for its use as a biomaterial. These results lead to increased knowledge of the role of carbon and nitrogen content in the behavior displayed by the different alloys studied.


Author(s):  
Luana Marotta Reis de Vasconcellos ◽  
Yasmin Rodarte ◽  
Renata Falchete do Prado ◽  
Luis Gustavo Oliveira de Vasconcellos ◽  
Mrio Lima de Alencastro Graa ◽  
...  

2017 ◽  
Vol 69 (2) ◽  
pp. 241-247 ◽  
Author(s):  
H. Siddhi Jailani ◽  
A. Rajadurai ◽  
B. Mohan ◽  
T. Sornakumar

Purpose Metal matrix composites (MMCs) are commonly used in many aerospace and industrial applications. MMCs possess significantly improved properties including high specific strength, specific modulus, damping capacity and good wear resistance compared to unreinforced alloys. The purpose of this paper is to describe the tribological studies of Al-Si alloy–fly ash composites manufactured using powder metallurgy technique. Design/methodology/approach Al-Si (12 Wt.%) alloy–fly ash composites were developed using powder metallurgy technique. Al-Si alloy powder was used as matrix material, and the fly ash was used as reinforcement. The particle size of Al-Si alloy powder was in the range of 75-300 μm, and the fly ash was in the range of 1-15 μm. The friction and wear characteristics of the composites were studied using a pin-on-disc set up. The test specimen was mated against cast iron disc, and the tests were conducted with the loads of 10, 20 and 30 N, sliding speeds of 0.5, 1 and 1.5 m/s for a sliding distance of 2,000 m. Findings The effects of load and sliding speed on tribological properties of the base alloy and Al-Si alloy–fly ash composites pins on sliding with cast iron disc are evaluated. The wear rate of Al-Si alloy–fly ash composites is lower than that of base alloy, and it increases with increasing load and sliding speed. The coefficient of friction of Al-Si alloy–fly ash composites is increased as compared with base alloy. Practical implications The development of Al-Si alloy–fly ash composites produced by powder metallurgy technique will modernize the automobile and other industries because near net shape at low cost and good mechanical properties are obtained. Originality/value There are few papers available on the development and tribological studies of Al-Si alloy–fly ash composites produced by powder metallurgy technique.


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