Determination of average domain size on permalloy and perminvar by means of complex permeability measurements

1983 ◽  
Vol 37 (3) ◽  
pp. 309-314 ◽  
Author(s):  
G. Bán ◽  
P. Arató ◽  
L. Szentmiklósi
1996 ◽  
Vol 69 (5) ◽  
pp. 769-780 ◽  
Author(s):  
R. H. Schuster ◽  
H. M. Issel ◽  
V. Peterseim

Abstract This paper describes the determination of accurate solubility parameters for nonpolar rubbers according to a GLC-method developed by Guillet. The data obtained provide a simple but meaningful thermodynamic characterization of the contribution of microstructure units and comonomers (styrene) in polydienes. On this basis quantitative expressions are derived for δ2-parameters of BR and SBR as a function of the vinyl and the styrene content respectively. The consequences on morphology development and miscibility are presented for blends of NR, SBR, BR and EPDM. Furthermore, it is shown for the first time that the method is able to describe the temperature dependence of the δ2-parameter so that temperature induced phase transitions (UCST and LCST) can be predicted. On this basis morphological predictions are made on average domain size and size distribution as well as on the phase inversion region. The contribution of intermolecular interactions to flow-induced phase morphology is discussed in relation to the influence of rheological factors. An extension to polymer—filler systems is made.


2013 ◽  
Vol 28 (S2) ◽  
pp. S51-S64 ◽  
Author(s):  
U.V. Ancharova ◽  
S.V. Cherepanova

Monte Carlo domain structure simulation and Debye equation calculation of XRD patterns were used to confirm the formation of domain structure and investigate its peculiarities. Correspondence of simulated XRD patterns with synchrotron powder diffraction experiments is achieved on the conditions that beside of 90o rotations of brownmillerite-like domains inside perovskite-like matrix each domain contains areas with perpendicularly oriented tetrahedral chains. Influence of such parameters as stoichiometry, average domain size, orthorhombic distortion degree on the XRD patterns is considered.


2015 ◽  
Vol 1761 ◽  
Author(s):  
Takatoshi Yamada ◽  
Nayuta Shimada ◽  
Kazuki Uekusa ◽  
Masataka Hasegawa

ABSTRACTWrinkle-less graphene films are obtained through roll-to-roll microwave plasma chemical vapor deposition by using flexible copper/polyimide (Cu/PI) webs. Raman spectra suggests that the average domain size of the obtained graphene on the flexible Cu/PI is almost the same compared to the graphene on a Cu web that includes wrinkles. Also, by utilizing the flexible Cu/PI webs, the compressive strains decreased. The sheet resistances of graphene deposited on the Cu/PI are (1∼5)×104Ω, which is two orders of magnitude lower than those of graphene deposited on the Cu webs. Our results suggest that the controlling the expansion of web material an important technology to improve graphene transparent conductive properties.


1994 ◽  
Vol 366 ◽  
Author(s):  
Mohamed Laradji ◽  
Ole G. Mouritsen ◽  
Søren Toxvaerd ◽  
Martin J. Zuckermann

ABSTRACTThe dynamics of phase separation of binary fluid mixtures in the presence of surfactants is studied via molecular dynamics simulations. In contrast to phase separation in pure binary fluid mixtures, which is characterized by an algebraic time dependence of the average domain size, mixtures containing surfactants exhibit nonalgebraic slow dynamics. At very late times, the average domain size saturates at a value inversely proportional to the surfactant concentration. Despite the fact that these systems only microphase separate, a dynamical scaling was observed at late times.


2009 ◽  
Vol 615-617 ◽  
pp. 181-184 ◽  
Author(s):  
Milena Beshkova ◽  
Mikael Syväjärvi ◽  
Remigijus Vasiliauskas ◽  
Jens Birch ◽  
Rositza Yakimova

The present paper deals with morphological and structural investigation of 3C-SiC layers grown by sublimation epitaxy on on axis 6H-SiC(0001) at source temperature 2000 °C, under vacuum conditions (<10-5 mbar) and different temperature gradients in the range of 5-8 °C/mm. The layer grown at a temperature gradient 6 °C/mm has the largest average domain size of 0.4 mm2 assessed by optical microscope in transmission mode. The rocking curve full width at half maximum (FWHM) of (111) reflection is 43 arcsec which suggests good crystalline quality. The AFM image of the same layer shows steps with height 0.25 nm and 0.75 nm which are characteristic of a stacking fault free 3C-SiC surface and c-axis repeat height, respectively.


1983 ◽  
Vol 36 (1) ◽  
pp. 130-136 ◽  
Author(s):  
W. G. P. Lamb

Efforts to determine the mean size of ship ‘domains’ from measurements of the distribution of ships in the vicinity of an individual ship have been made by several workers, particularly by Goodwin, who made extensive observations in the Sunk Lightship area of the North Sea. The work involved plotting the positions of vessels at time intervals of a few minutes to estimate the number of ships in an annulus about a central ship, or alternatively the number per unit area at various distances from a central ship. These figures were used to obtain distribution curves from which the average domain could be estimated. The work of Curtis and Barratt on the validation of simulator studies of passing manoeuvres in fog, in which the nearest point of approach of ship's tracks was determined, serves to illustrate an alternative method based on the distribution of the density of tracks. In both procedures use is made of the point at which the distribution function first returns to the value which would obtain if the distribution were uniform, that is, if ship domains were absent. Some doubts have been expressed as to the validity of using the position of the cross-over point as a measure of the average domain size, and also whether it would be more appropriate to employ the position of the maximum value of the functions.


2013 ◽  
Vol 740-742 ◽  
pp. 125-128
Author(s):  
Dang Chao Wang ◽  
Yu Ming Zhang ◽  
Yi Men Zhang ◽  
Hui Guo ◽  
Yue Hu Wang

This paper investigated a feasible process of growing epitaxial graphene on 4H hexagonal poly-type of silicon carbide Si-faced polar surface (0001) under an argon pressure of 900 mbar conditions. Using Raman Spectroscopy, Scanning Electron Microscopy and X-ray Photoelectron Spectroscopy, epitaxial graphene grown at temperature 1600°C is confirmed to take shape weakly on 4H-SiC (0001) with an average domain size of several tens of nanometers, and this can be seen as the characteristic of initial formation of epitaxial graphene on substrate.


1994 ◽  
Vol 351 ◽  
Author(s):  
A. Moet ◽  
A. Akelah ◽  
N. Salahuddin ◽  
A. Hiltner ◽  
E. Baer

ABSTRACTComposites of amine terminated butadieneacrylonitrile (ATBN) and montmorillonite (MMT) were prepared by ion exchange between the onium salt of the polymer and the interlamellar cation of the mineral following two different preparation approaches. The first carried out the ion exchange in situ and used dioxane, a better solvent for the polymer, and the second administered the onium salt to MMT using dimethylsulfoxide (DMSO). Elemental analysis and IR spectroscopy indicated that all the ionic sites of the mineral have been occupied by polymer end groups. The d (001) spacing and the span between the internal lamelar surface were only expanded to about 14 Å and 5 Å, respectively, suggesting horizontal packing of the polymer molecules. TEM of microtome sections prepared from compression molded composites revealed that the lamellae, laminated with polymers assembled into multiplets of about 5 nm for both preparations. The multiplets clustered into mineral rich domains whose average size was 250 nm for the DMSO preparation. Finer clusters (70 nm) were obtained by the first method. This three fold decrease in the average domain size was attributed to the strong solvation power of dioxane in the binary solvent and to the locale of ion exchange.


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