scholarly journals Microstructure, shear properties and corrosion resistance of Cu/Cu-In/Cu solder joints

Author(s):  
Li Liu ◽  
Bo Zhao ◽  
Bang Jiang ◽  
Zhiwen Chen ◽  
Wei Huang ◽  
...  
2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Jianguo Cui ◽  
Keke Zhang ◽  
Di Zhao ◽  
Yibo Pan

AbstractThrough ultrasonic wave assisted Sn2.5Ag0.7Cu0.1RExNi/Cu (x = 0, 0.05, 0.1) soldering test and − 40 to 125 °C thermal shock test, the microstructure and shear properties of Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints under thermal cycling were studied by the SEM, EDS and XRD. The results show that the Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints with high quality and high reliability can be obtained by ultrasonic assistance. When the ultrasonic vibration power is 88 W, the ultrasonic-assisted Sn2.5Ag0.7Cu0.1RE0.05Ni/Cu solder joints exhibits the optimized performance. During the thermal cycling process, the shear strength of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints had a linear relationship with the thickness of interfacial intermetallic compound (IMC). Under the thermal cycling, the interfacial IMC layer of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints consisted of (Cu,Ni)6Sn5 and Cu3Sn. The thickness of interfacial IMC of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints was linearly related to the square root of equivalent time. The growth of interfacial IMC of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints had an incubation period, and the growth of IMC was slow within 300 cycles. And after 300 cycles, the IMC grew rapidly, the granular IMC began to merge, and the thickness and roughness of IMC increased obviously, which led to a sharp decrease in the shear strength of the solder joints. The 0.05 wt% Ni could inhibit the excessive growth of IMC, improve the shear strength of solder joints and improve the reliability of solder joints. The fracture mechanism of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints changed from the ductile–brittle mixed fracture in the solder/IMC transition zone to the brittle fracture in the interfacial IMC.


2010 ◽  
Vol 26 (8) ◽  
pp. 737-742 ◽  
Author(s):  
X.J. Wang ◽  
Q.L. Zeng ◽  
Q.S. Zhu ◽  
Z.G. Wang ◽  
J.K. Shang

Author(s):  
Nan Jiang ◽  
Liang Zhang ◽  
Kai-Kai Xu ◽  
Mu-Lan Li ◽  
Feng-Jiang Wang

In this work, SiC nanowires (SiC NWs) reinforced SBG (Sn-58Bi-0.05GNSs) composite solder was prepared using powder metallurgy route. The effect of SiC NWs on melting temperature, wetting behavior, shear properties, microstructure of the prepared solder joints and interfacial reaction were studied in detail. Results reveal that incorporating SiC NWs can develop the wetting behavior and shear properties of solder joint but has a little effect on melting temperature. The microstructure of solder is refined markedly with the addition of SiC NWs, which is one of the reasons for the increase in the shear strength of the solder joints. Additionally, the dimension of Cu6Sn5 IMC grains diminishes with the doping of SiC NWs, which resulted in the thinning of Cu6Sn5 IMC layer. Thence, the addition of SiC NWs may be an effective way to improve the reliability of solder joints.


1988 ◽  
Vol 4 (5) ◽  
pp. 255-260 ◽  
Author(s):  
E. Angelini ◽  
P. Bonino ◽  
M. Pezzoli

Metals ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 2027
Author(s):  
Zhimin Liang ◽  
Fei Shen ◽  
Zongyuan Yang ◽  
Da Xu ◽  
Shaowei Wei ◽  
...  

Sn–Sb system solders and ENIG/ENEPIG surface finish layers are commonly used in electronic products. To illustrate the thermal reliability evaluation of such solder joints, we studied the interfacial microstructure and shear properties of Sn-4.5Sb-3.5Bi-0.1Ag/ENIG and Sn-4.5Sb-3.5Bi-0.1Ag/ENEPIG solder joints after aging at 150 °C for 250, 500 and 1000 h. The results show that the intermetallic compound of Sn-4.5Sb-3.5Bi-0.1Ag/ENIG interface was more continuous and uniform compared with that of Sn-4.5Sb-3.5Bi-0.1Ag/ENEPIG interface after reflow. The thickness of the interfacial intermetallic compounds of the former was significantly thinner than that of the latter before and after aging. With extension of aging time, the former interface was stable, while obvious voids appeared at the interface of the latter after 500 h aging and significant fracture occurred after 1000 h aging. The shear tests proved that shear strength of solder joints decreased with increasing aging time. For the Sn-4.5Sb-3.5Bi-0.1Ag/ENEPIG joint after 1000 h aging, the fracture mode is ductile-brittle mixed type, which means fracture could occur at the solder matrix or the solder/IMC interface. For other samples of these two types of joints, ductile fracture occurred inside of the solder. The Sn-4.5Sb-3.5Bi-0.1Ag/ENIG solder joint was thermally more reliable than Sn-4.5Sb-3.5Bi-0.1Ag/ENEPIG.


2015 ◽  
Vol 27 (1) ◽  
pp. 45-51 ◽  
Author(s):  
Wei Liu ◽  
Rong An ◽  
Chunqing Wang ◽  
Yanhong Tian

Purpose – The purpose of this paper is to investigate the effect of typical morphologies of Au-Sn IMCs (intermetallic compounds) at the interfaces of solder and pads on shear properties of laser reflowed micro-solder joints. Design/methodology/approach – Sn-2.0Ag-0.75Cu-3.0Bi (SnAgCuBi) solder balls (120 μm in diameter), pads with 0.1, 0.5, 0.9 or 4.0 μm thickness of Au surface finish, and different laser input energies were utilized to fabricate micro-solder joints with Au-Sn IMCs having different typical morphologies. The joints were performed by a shear test through a DAGE bond test system. Fracture surfaces of the joints were analyzed by scanning electron microscopy and energy-dispersive X-ray spectrometry to identify fracture modes and locations. Findings – Morphologies of Au-Sn IMCs would affect shear properties of the joints remarkably. When needle-like AuSn4 IMCs formed at the interfaces of solder and pads, almost entire surfaces presented the manner of ductile fracture. Moreover, shear forces of this kind of solder joints were higher than those of joints without Au-Sn IMCs or with a nearly continuous/continuous Au-Sn IMCs layer. The reason was that the shear performance of the solder joints with needle-like AuSn4 IMCs was enhanced by an interlocking effect between solder and needle-like AuSn4 IMCs. As a nearly continuous or continuous Au-Sn IMCs layer formed, the fracture surfaces presented more character of brittle than ductile fracture. However, if an Au layer still remained under Au-Sn IMCs, the shear performance of the joints would be enhanced. Originality/value – The results in this study can be used to optimize microstructures and shear properties of laser reflowed micro-solder joints.


2012 ◽  
Vol 560-561 ◽  
pp. 694-697
Author(s):  
Gyun Lee ◽  
Hyo Sun Yu ◽  
Sung Mo Yang ◽  
Hee Yong Kang ◽  
Dong Pyo Hong ◽  
...  

The use of Pb-free solder alloys are just newly developed materials and their properties are not well established and documented yet. So, the research to substitute the critical problem of the Pb solder alloy are increasing widely. To evaluate the shear property of solder joints according to temperature condition was predicted through the Shear-Punch test and FEM. By using the database according to this, the reliability evaluation technology of the solder joints tries to be formulated. In this paper, the solder used the Sn37Pb, Sn-4Ag and the Sn4Ag0.5Cu. When solder melted in the copper interface, the solder joints according to reflow times, each modeling required for the Shear- Punch was made in consideration of the IMC layer thickness. And the micro shear punch test was performed to obtain material properties of solder according to temperature condition. The shear properties of specimen which was modeled was predicted through FEM. It compared with the test value in which it obtains from Shear-Punch. Also, a method which can obtain shear properties of Pb-free solder joints easily and quickly using FEM was proposed.


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