Mechanical properties and thermal conductivity of a temperature resistance hollow glass microspheres/borosilicate glass buoyance material

2016 ◽  
Vol 674 ◽  
pp. 604-614 ◽  
Author(s):  
Sue Ren ◽  
Jiachen Liu ◽  
Anran Guo ◽  
Wenjie Zang ◽  
Haitao Geng ◽  
...  
2018 ◽  
Vol 772 ◽  
pp. 33-37
Author(s):  
Nattakarn Hongsriphan ◽  
Pajaera Patanathabutr ◽  
Kanyakarn Lappokachai

Recycled poly (ethylene terephthalate) or R-PET is conventionally melt blended with polycarbonate with the presence of chain extender in order to produce polymer blend that provides good mechanical properties and cost effectiveness. This research was carried out to improve properties of such a blend by compounding them with silane treated hollow glass microspheres (HGMs), which mixing procedure was emphasized how it could affect mechanical properties. R-PET/PC/HGM composites of a fixed composition were melt compounded with three different mixing procedures. It was found that the compounding HGMs with PC and then R-PET obtained the most rigidity specimens than the all-in-one compounding or the compounding HGMs with R-PET and then PC. Silane treated HGMs were well distributed in the polymer matrix presenting good interfacial adhesion. However, the notched impact strength of all composites were inspected to be in the same range.


2013 ◽  
Vol 467 ◽  
pp. 247-252 ◽  
Author(s):  
Semenov Vyacheslav ◽  
Oreshkin Dmitriy ◽  
Rozovskaya Tamara

In the paper the research results of light-weight masonry mortars with hollow glass microspheres (HGMS) and antifreeze admixtures (AFA) for masonry walling of the efficient small items at the low temperatures are given. One has chosen the antifreeze admixtures for the mortars and their rate has been justified. The main properties of the masonry mortars with HGMS and the antifreeze admixtures have been determined. The standard research methods are used. Main attention was paid to the analysis of strength of the mortar with HGMS and the antifreeze admixtures formed at the positive and negative temperatures. The optimal mixtures for the temperature down to 10 °C were developed. A priority direction of development of construction science currently is energy saving and the improvement of energy efficiency of buildings and structures. A part of the solution to this problem is the development of efficient building materials and fencing structures. The use of multi-layer fencing structures is known to lead to a decrease in the coefficient of their thermal uniformity [. In this regard, the most promising is the development of single-wall exterior fencing structures, which answer the requirements of the standards for thermal protection. However, single-wall fencing structures answering the requirements for thermal protection must have an average density value not greater than 500 kg/m3. The materials from cellular concrete, polystyrene concrete, foam ceramics concrete and others satisfy the aforesaid requirements. The monolith unity of similar structures is provided through the use of mortars on the basis of mineral, mineral-and-polymer and polymer binders [2-. Such mortars with high average density and a high coefficient of thermal conductivity are the bridges of cold in the construction; they do not provide the thermal homogeneity of the fencing structure and reduce its thermal resistance. A solution to this problem is the use of light-weight masonry mortars (warm mortars). Such mortars with traditional light-weight fillers (e.g. expanded perlite and vermiculite mortar sands) have an increased water requirement, and, as a consequence, the extremely low strength value. Recently, hollow glass (HGMS) or ceramics (CMS) microspheres are used as light-weight fillers for masonry mortars [. Thus, in [ the scientific principles of the use of such compositions with HGMS have been developed. The masonry mortar has been obtained with the following properties: average density of dried mortar is 450 kg/m3 with a coefficient of thermal conductivity equal to 0.17 W/m·°C and a compressive strength equal to 3.2 MPa at the age of 28 days, water-retention capacity over 90% and with optimal technological and rheological characteristics [.


2013 ◽  
Vol 678 ◽  
pp. 37-41 ◽  
Author(s):  
Sridhar Dalai ◽  
Savithri Vijayalakshmi ◽  
Pratibha Sharma

Hollow glass microspheres (HGMs) are a unique class of materials with interconnected pores in the microsphere walls, which can adsorb, retain and release hydrogen and other gases. In this study, HGMs was prepared from amber coloured and borosilicate glass frits. The glass frits after the preliminary washing and drying was sized to particles below 120 μm. The hollow glass microspheres were successfully fabricated from the glass powder by flame spheroidisation using air-acetylene flame. Effect of glass feed particle size as well as feed rate, in the formation of HGMs was studied. Glass feed particle size >75 μm and that <45 μm were found to give very poor yield of HGMs, whereas particles 50-75 μm gave very good yield for HGMs. Further study of the process parameters and constant monitoring to regulate the process are being carried out in our laboratory to arrive at a correct figure for the yield of HGMs. Characterisation of the HGMs prepared was done using Image analysing system, SEM, and XRD. The composition of the raw material and the product HGMs were determined using ICP-AES.


Polymers ◽  
2019 ◽  
Vol 11 (4) ◽  
pp. 624 ◽  
Author(s):  
Adriano Vignali ◽  
Salvatore Iannace ◽  
Giulio Falcone ◽  
Roberto Utzeri ◽  
Paola Stagnaro ◽  
...  

In this work, novel composites based on poly(ε-caprolactone) (PCL) were prepared and characterized in terms of morphological, thermal, rheological and mechanical properties. Hollow glass microspheres (HGM), alone or surface modified by treatment with (3-aminopropyl)triethoxysilane (APTES) in order to enhance the compatibility between the inorganic particles and the polymer matrix, were used to obtain lightweight composites with improved properties. The silanization treatment implies a good dispersion of filler particles in the matrix and an enhanced filler–polymer adhesion. The addition of HGM to PCL has relevant implications on the rheological and mechanical properties enhancing the stiffness of the material. Furthermore, the presence of HGM strongly interferes with the crystallization behavior and thermo-oxidative degradation of PCL. The increase of PCL crystallization rate was observed as a function of the HGM amount in the composites. Finally, rotational molding tests demonstrated the possibility of successfully producing manufactured goods in PCL and PCL-based composites on both a laboratory and industrial scale.


2015 ◽  
Vol 820 ◽  
pp. 509-514
Author(s):  
Cindy Yuri Ueki Peres ◽  
Antonio Hortêncio Munhoz ◽  
L.F. Miranda ◽  
A. Cabral Neto ◽  
A.R. Zandonadi ◽  
...  

The addition of hollow glass spheres is interesting to reduce the thermal conductivity of the concrete pieces. This work aims to evaluate the concrete with addition of hollow glass microsphere with different combinations of dosage in concrete concerning strength and workability. Slump tests were performed in each dosage of concrete in order to evaluate the effect of glass microspheres in concrete mix. In each age of curing concrete, bodies-specimens underwent ultrasound to estimate the homogeneity of concrete with hollow glass microspheres, and testing of compressive strength. The analysis of the results shows that for some formulations, the addition of hollow glass microspheres imparts high mechanical strength to compressive strength above 30MPa at all analyzed cure periods. The workability of the concrete had to be substantially reduced, showing no workability improvement due to the addition of hollow glass microsphere.


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