Critical resolved shear stress of activated slips measured by micropillar compression tests for single-crystals of Cr-based Laves phases

2021 ◽  
Vol 806 ◽  
pp. 140861
Author(s):  
Yunlong Xue ◽  
Naoki Takata ◽  
Hongmei Li ◽  
Makoto Kobashi ◽  
Liang Yuan
1998 ◽  
Vol 552 ◽  
Author(s):  
Kouji Hagihara ◽  
Takayoshi Nakano ◽  
Yukichi Umakoshi

ABSTRACTTemperature dependence of yield stress and operative slip system in Ni3Nb single crystals with the DOa structure was investigated in comparison with that in an analogous L12 structure. Compression tests were performed at temperatures between 20 °C and 1200 °C for specimens with loading axes perpendicular to (110), (331) and (270).(010)[100] slip was operative for three orientations, while (010)[001] slip for (331) and {211} <10 7 13> twin for (270) orientations were observed, depending on deformation temperature. The critical resolved shear stress (CRSS) for the (010)[100] slip anomaly increased with increasing temperature showing a maximum peak between 400 °C and 800 °C depending on crystal orientation. The CRSS showed orientation dependence and no significant strain rate dependence in the temperature range for anomalous strengthening. The [100] dislocations with a screw character were aligned on the straight when the anomalous strengthening occurred. The anomalous strengthening mechanism for (010)[100] slip in Ni3Nb single crystals is discussed on the basis of a cross slip model which has been widely accepted for some L12-type compounds.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Zhenghao Chen ◽  
Bhaskar Paul ◽  
Sanjib Majumdar ◽  
Norihiko L. Okamoto ◽  
Kyosuke Kishida ◽  
...  

AbstractThe plastic deformation behavior of single crystals of two transition-metal diborides, ZrB2 and TiB2 with the AlB2 structure has been investigated at room temperature as a function of crystal orientation and specimen size by micropillar compression tests. Although plastic flow is not observed at all for their bulk single crystals at room temperature, plastic flow is successfully observed at room temperature by the operation of slip on {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 3> in ZrB2 and by the operation of slip on {1$${\bar{1}}$$ 1 ¯ 00}<0001> and {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 0> in TiB2. Critical resolve shear stress values at room temperature are very high, exceeding 1 GPa for all observed slip systems; 3.01 GPa for {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 3> slip in ZrB2 and 1.72 GPa and 5.17 GPa, respectively for {1$${\bar{1}}$$ 1 ¯ 00}<0001> and {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 0> slip in TiB2. The identified operative slip systems and their CRSS values are discussed in comparison with those identified in the corresponding bulk single crystals at high temperatures and those inferred from micro-hardness anisotropy in the early studies.


2000 ◽  
Vol 46 (152) ◽  
pp. 41-44 ◽  
Author(s):  
Y. L. Trickett ◽  
I. Baker ◽  
P. M. S. Pradhan

AbstractSingle crystals with a wide variety of orientations were cut from large pucks of laboratory-grown ice. Constant-strain-rate compression tests were performed on the crystals either at an axial strain rate of 1 × 10−5 s−1at –20°C or at axial strain rates from 1 × 10−6 s−1 to 1 × 10−4 s−1 at –10°C. In agreement with previous studies of ice flow, the compression tests showed a linearly rising stress with increasing strain, followed by a sharply declining stress after reaching a peak. With further strain, the sharp decline in stress slowed and the flow stress approached a plateau that was only weakly dependent on strain. For all crystallographic orientations, it was found that Schmid’s (critical resolved shear stress) law was obeyed by the peak stress. Slip lines clearly showed that basal slip was the deformation mode.


2007 ◽  
Vol 561-565 ◽  
pp. 459-462
Author(s):  
Katsushi Tanaka ◽  
Hiromitsu Ide ◽  
Yoshinori Sumi ◽  
Kyosuke Kishida ◽  
Haruyuki Inui

Compressive deformation of L10-ordered single crystals of FePd whose c/a ratio less than unity have been investigated from room temperature to 823 K. The results show that the critical resolved shear stress (CRSS) for octahedral glide of ordinary dislocations is smaller than that of super-lattice dislocations in all the temperature range investigated, that is the opposite sense to the case of Ti-56 mol% Al. The CRSS for ordinary dislocations virtually independent to the temperature. On the other hand, the CRSS for super dislocations exhibits a weak positive temperature dependence from room temperature up to 573 K and decreases in higher temperatures.


1990 ◽  
Vol 213 ◽  
Author(s):  
R.D. Field ◽  
D.F. Lahrman ◽  
R. Darolia

ABSTRACTA detailed study of deformation of NiAl single crystals in two soft orientations, <110> and <111>, has been conducted. The Schmid factor favors {100} slip in the former and {110} slip in the latter. Detailed dislocation analysis, critical resolved shear stress measurements, and slip trace analysis have been performed to determine the nature of dislocation motion and interactions in this material. Particular attention is given to prismatic loops formed during deformation, since the shapes of these loops reveal the active slip planes. Similar loop morphologies observed in elevated temperature [001] oriented tensile specimens are also discussed.


The problem of accommodation of constrained deformation by slip and twinning has been analysed. The analysis is based on Taylor’s least work hypothesis. In this analysis, the operative combination of slip and twinning systems is found by minimizing the orientation factor M = (∑ i s i +α∑ i t i )/ ε , where s i and t i are the simple shears resulting from slip and twinning respectively, α is the ratio of the critical resolved shear stress for twinning against slip, and Ɛ is the external strain. Detailed calculations have been made for face-centred cubic crystals deformed by plane strain compression. Experimental observations on deformed single crystals of a Co–8% Fe alloy indicate good agreement with the analysis. Implications of the present study to the twinning observations of Heye & Wassermann on rolled Ag crystals are discussed.


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