Reactive sputtering deposition of photocatalytic TiO2 thin films on glass substrates

2007 ◽  
Vol 138 (2) ◽  
pp. 139-143 ◽  
Author(s):  
C.J. Tavares ◽  
J. Vieira ◽  
L. Rebouta ◽  
G. Hungerford ◽  
P. Coutinho ◽  
...  
2012 ◽  
Vol 2 (1) ◽  
Author(s):  
Marek Nocuń ◽  
Sławomir Kwaśny

AbstractIn our investigation, V doped SiO2/TiO2 thin films were prepared on glass substrates by dip coating sol-gel technique. Chemical composition of the samples was studied by X-ray photoelectron spectroscopy (XPS). Transmittance of the samples was characterized using UV-VIS spectrophotometry. Subsequently band-gap energy (Eg) was estimated for these films. Powders obtained from sols were characterized by FTIR spectroscopy. It was found that vanadium decreases optical band gap of SSiO2/TiO2 films.


2008 ◽  
Vol 73 (1) ◽  
pp. 121-126
Author(s):  
Ivan Radovic ◽  
Yves Serruys ◽  
Yves Limoge ◽  
Natasa Bibic

SiO2 layers were deposited in a UHV chamber by 1 keV Ar+ ion sputtering from a high purity silicon target, using different values of the oxygen partial pressure (5?10-6-2?10-4 mbar) and of the ion beam current on the target (1.67-6.85 mA). The argon partial pressure during operation of the ion gun was 1?10-3 mbar. The substrate temperature was held at 550?C and the films were deposited to a thickness of 12.5-150 nm, at a rate from 0.0018-0.035 nm s-1. Structural characterization of the deposited thin films was performed by Rutherford backscattering spectrometry (RBS analysis). Reactive sputtering was proved to be efficient for the deposition of silica at 550?C, an oxygen partial pressure of 2?10-4 mbar (ion beam current on the target of 5 mA) or, at a lower deposition rate, ion beam current of 1.67 mA and an oxygen partial pressure of 6?10-5 mbar. One aspect of these investigations was to study the consumption of oxygen from the gas cylinder, which was found to be lower for higher deposition rates.


2014 ◽  
Vol 552 ◽  
pp. 10-17 ◽  
Author(s):  
M.A. Baker ◽  
H. Fakhouri ◽  
R. Grilli ◽  
J. Pulpytel ◽  
W. Smith ◽  
...  

2013 ◽  
Vol 699 ◽  
pp. 789-794 ◽  
Author(s):  
Laith Rabih ◽  
Sudjatmoko ◽  
Kuwat Triyana ◽  
Pekik Nurwantoro

Titanium dioxide (TiO2 ) thin films have been deposited on glass substrates under various conditions by using a homemade reactive DC sputtering technique. The TiO2 has unique characteristics and economical alternative material for transparent conductivity oxide thin films compared with other materials. In this study, titanium (Ti) has been used as a target while argon (Ar) and oxygen (O22</subthin films has been measured by using a calibrated I-V meter. On the other hand, the transparency, microstructure and component of TiO2 thin films have been investigated respectively by using UV-VIS spectrophotometer, XRD and SEM (EDX). The thickness of TiO2 films, the grain size and the band gap have been also successfully estimated. As a result, the conductivity of films increased for Dt at 1 hour to 3.5 hours and decreased for Dt at 4 hours. It means that the optimum Dt was at about 3.5 hours. It may be related to the thickness (structures) of the films. In addition, the thickness and grain size increased by increasing Dt, while the band gap decreased when the film structure changed from non-crystalline structure to crystalizing structure.


2011 ◽  
Vol 694 ◽  
pp. 466-470
Author(s):  
Wen Dong Liang ◽  
Xian Kun Wang ◽  
Yong Ping Yang

Anatase TiO2 thin films were prepared on glass substrates by dip-coating method with TiCl4 as the Ti precursor hydrolysis in a mixed solvent of alcohol and water. The effects of preparation parameters such as the alcohol species, the alcohol/water (A/W) ratio, and the dosage of TiCl4 (the volume ratio of TiCl4 and mixed solution) were investigated. The best preparation condition was optimized that with the isopropanol / H2O volume ratio of 65:35, the dosage of TiCl4 at 3%. XRD, SEM, TEM and UV–Vis photospectroscopy were used to analyze the characteristics of the solution and films. The films have a high hydrophilicity after illuminating with ultraviolet light, it have a good adherence and can be used as an efficient photocatalyst.


2016 ◽  
Vol 289 ◽  
pp. 172-178 ◽  
Author(s):  
Stéphanie Collette ◽  
Julie Hubert ◽  
Abdelkrim Batan ◽  
Kitty Baert ◽  
Marc Raes ◽  
...  

2002 ◽  
Vol 17 (3) ◽  
pp. 21-23 ◽  
Author(s):  
Wei Jian-hong ◽  
Zhao Xiu-jian ◽  
Gan Jian-guo ◽  
Yuan Run-zhang ◽  
Shi Jing

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