Automatic acquisition of particle orientation by interferometric out-of-focus image

2021 ◽  
Vol 486 ◽  
pp. 126795
Author(s):  
Jinlu Sun ◽  
Hongxia Zhang ◽  
Wenbo Fan ◽  
Shengyong Chen
Author(s):  
R. J. Horylev ◽  
L. E. Murr

Smith has shown by dark-field electron microscopy of extracted ThO2 particles from TD-nickel (2% ThO2) that they possess single crystal characteristics. It is generally assumed that these particle dispersions are incoherent. However, some diffraction effects associated with the particle images appeared to be similar to coherency strain fields. The present work will demonstrate conclusively that ThO2 dispersed particles in TD-nickel (2% ThO2) and TD-NiCr (2% ThO2, 20% Cr, Ni) are single crystals. Moreover, the diffraction contrast effects are extinction fringes. That is, these effects arise because of the particle orientation with respect to the electron beam and the extinction conditions for various operating reflections The particles are in fact incoherent.


Author(s):  
O. E. Bradfute

Electron microscopy is frequently used in preliminary diagnosis of plant virus diseases by surveying negatively stained preparations of crude extracts of leaf samples. A major limitation of this method is the time required to survey grids when the concentration of virus particles (VPs) is low. A rapid survey of grids for VPs is reported here; the method employs a low magnification, out-of-focus Search Mode similar to that used for low dose electron microscopy of radiation sensitive specimens. A higher magnification, in-focus Confirm Mode is used to photograph or confirm the detection of VPs. Setting up the Search Mode by obtaining an out-of-focus image of the specimen in diffraction (K. H. Downing and W. Chiu, private communications) and pre-aligning the image in Search Mode with the image in Confirm Mode facilitates rapid switching between Modes.


Author(s):  
Joachim Frank

Compared with images of negatively stained single particle specimens, those obtained by cryo-electron microscopy have the following new features: (a) higher “signal” variability due to a higher variability of particle orientation; (b) reduced signal/noise ratio (S/N); (c) virtual absence of low-spatial-frequency information related to elastic scattering, due to the properties of the phase contrast transfer function (PCTF); and (d) reduced resolution due to the efforts of the microscopist to boost the PCTF at low spatial frequencies, in his attempt to obtain recognizable particle images.


2009 ◽  
Vol 29 (3) ◽  
pp. 846-848 ◽  
Author(s):  
Yong-wen HUANG ◽  
Zhong-shi HE ◽  
Xing WU

2019 ◽  
Vol 92 ◽  
pp. 01004
Author(s):  
Christopher Ibeh ◽  
Matteo Pedrotti ◽  
Alessandro Tarantino ◽  
Rebecca Lunn

The quality and reliability of cohesive soil laboratory test data can be significantlyaffected by sample disturbance during sampling or sample preparation. Sample disturbance may affect key design and modelling parameters such as stiffness, preconsolidation stress, compressibility and undrained shear strength, and ultimately determine particle mobilization and shear plane development. The use of X-ray computed tomography (X-CT) in the study of soil is restricted by the inverse relationship of specimen size and obtainable image resolution. This has led to the testing of miniature specimen sizes which are far less than conventional laboratory sample size in a bid to obtain high resolution images and detailed particle-scale soil properties; however, these miniature soil specimens are more prone to sample disturbance. In this work 2% muscovite was mixed with speswhite kaolin clay as a strain marker for use in X-CT. The clay soil sample was prepared from slurry and either consolidated using an oedometer or a gypsum mould. Specimens obtained from a 7 mm tube sampler were compared to lathe trimmed specimens with a diameter (Ø) of 7 mm. Results from X-CT imaging were used to study the influence of sampler type on specimen disturbance, by analysing the muscovite particle orientation of the obtained 3D images. The results show that; for samples subjected to large consolidation stress (>200kpa) lathe trimmed specimens may be subject to lesser disturbance compared to tube sampled specimens.


1963 ◽  
Vol 3 (01) ◽  
pp. 1-8 ◽  
Author(s):  
N.T. Burdine

BURDINE, N.T., SOCONY MOBIL OIL CO., INC., DALLAS, TEX Abstract The present investigation is concerned with the cumulative damage to rock samples when exposed to cyclic stresses under various loading conditions. Information on the response of rocks to repetitive deformational forces is an essential prerequisite to an understanding of the fundamentals of drilling. Using a laboratory designed and constructed dynamic-stress apparatus, preliminary data were obtained on cylindrical rock samples. The experiments consist of measuring the number of cycles to failure for a given axial load ( static plus dynamic). Data were obtained for various confining and pore pressures, pore fluids (air and water), frequencies of stress application and loading procedures. The results are related to failure theories and dynamic fatigue properties of other materials. Introduction In most conventional and new drilling processes, repetitive forces are applied to the bottom of the borehole. Furthermore, in hard-rock drilling the number of applications of the forces to a particular section of rock may become excessively large. The present investigation is concerned with the cumulative damage to rocks when exposed to cyclic stresses under various loading conditions. It is believed that the experiments will lead to a better understanding of the mechanical response of rocks to particular deformational forces and to a more efficient drillingprocedure.Thepresent investigation is the initial part of a general study of the behavior of inelastic materials under static and dynamic conditions, including both theoretical and experimental studies. SURVEY OF FAILURE THEORIES OF MATERIALS Few, even phenomenological, theories on rock deformation have been established because the state of knowledge of flow, fracture and strength of rocks is largely empirical. Most of the theories that do exist were originally formulated for other materials. HOOKE'S LAW The state of stress in continuous media is completely determined by the stress tensor and the state of deformation by the strain tensor . In the linear theory of elasticity the generalized Hooke's law is ..........................(1) where the coefficients are the components of the elasticity tensor. For homogeneous and isotropic conditions the number of independent coefficients reduce to two, and Eq. 1 becomes ..................(2) in which and are Lame's constants; is the kronecker delta; and is the dilation. This simplified version of Hooke's law has been used quite extensively in geophysical research where most of the information about the mechanical properties of the earth have been obtained. However, it has only limited application in rock fatigue studies. MATERIAL BEHAVIOR Many solids obey Hooke's law at small stresses, but for higher stresses a hysteretic effect occurs due to temporary or permanent residual deformation of the solid (inelastic deformation). Such deviations in mechanical behavior exist in varying degrees in different classes of materials. Most elastic materials have a microscopic heterogeneity due either to random distribution of anisotropic particles, or due to some preferred particle orientation, or both. Other materials are quite grossly heterogeneous. And the method of formation, particularly in rocks, oftentimes creates residual stress concentrations which have complicated states of imperfect equilibrium. Also, the thermal effects resulting from structural behavior give rise to nonuniform temperature distributions and the degradation of mechanical energy. When such bodies are exposed to certain large loading conditions, the inelastic behavior is intensified so strongly that the deformation, normally brittle, becomes ductile. SPEJ P. 1^


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