Multiple phase transitions investigated by high-speed TEM

Author(s):  
Oleg Bostanjoglo ◽  
Peter Thomsen-Schmidt

Thin GexTe1-x (x = 0.15-0.8) were studied as a model substance of a composite semiconductor film, in addition being of interest for optical storage material. Two complementary modes of time-resolved TEM were used to trace the phase transitions, induced by an attached Q-switched (50 ns FWHM) and frequency doubled (532 nm) Nd:YAG laser. The laser radiation was focused onto the specimen within the TEM to a 20 μm spot (FWHM). Discrete intermediate states were visualized by short-exposure time doubleframe imaging /1,2/. The full history of a transformation was gained by tracking the electron image intensity with photomultiplier and storage oscilloscopes (space/time resolution 100 nm/3 ns) /3/. In order to avoid radiation damage by the probing electron beam to detector and specimen, the beam is pulsed in this continuous mode of time-resolved TEM,too.Short events ( <2 μs) are followed by illuminating with an extended single electron pulse (fig. 1c)

1999 ◽  
Vol os-8 (1) ◽  
pp. 1558925099OS-80 ◽  
Author(s):  
Hong Yin ◽  
Zanyao Yan ◽  
Randall R. Bresee

High-speed digital imaging techniques and web measurements were used to investigate the meltblowing (MB) process. We evaluated fiber diameter, fiber orientation, fiber entanglement, fiber velocity and fiber acceleration between the die and collector. Three processing variables were studied: primary air pressure, die-to-collector distance and collector surface speed. Although results of this investigation are somewhat preliminary, they provide fundamental information about the MB process and increase our understanding of it. Introduction Meltblowing (MB) is a fast, chaotic and complicated process. These features make it difficult to study the MB process theoretically as well as experimentally and most researchers have simply studied the effects of resin and process variables on web structure or web properties. Some researchers, however, have reported on-line measurements during MB [1–9]. Bansal and Shambaugh measured fiber temperature during single-hole MB using an infrared camera [1]. Wu and Shambaugh measured fiber velocity using laser Doppler velocimetry during single-hole MB [2]. Shambaugh and others reported experimental measurements of fiber motion and fiber diameter using a single-hole die [1–7]. Multiple-exposed photographs using conventional film were produced with a strobe light in a dark room to study fiber motion and single-exposed photographs were used to estimate fiber diameter. The exposure duration of the strobe light (50 μs), however, was not short enough to eliminate image blur and obtain sharp images so the primary air velocity used during MB was low (17–55 m/s). Milligan and Utsman used a similar film-based photographic technique to investigate MB using a 30-hole die [8]. Bresee and Yan used a video imaging technique to investigate the dynamics of web formation at the collector of a 600-hole MB line [9]. Measurements of the dynamics between the die and collector of a high-speed commercial-like MB process would be expected to be especially desirable for understanding MB. To directly observe dynamic motions during this fast process, it is necessary to use a short exposure time to freeze motion in each image and a high framing rate to resolve fast fiber motions. We used a high-speed digital camera from Vision Research Inc. to acquire images as rapidly as 1,000 frames/s. The camera produced image frames with a spatial resolution as great as 512×512 pixels and 8-bit gray level resolution (256 gray levels). Electronic shuttering of the camera provided exposure times as short as 50 μs/frame. To obtain exposure times shorter than 50 μs or to obtain multiple-exposed images, a high-speed pulsed laser from Oxford Lasers, Inc. was used for illumination. The laser produced 100 watt peak power at 805 nm and pulse durations as short as 1 μs were synchronized with the camera.


2016 ◽  
Vol 23 (4) ◽  
pp. 1046-1053 ◽  
Author(s):  
Tao Sun ◽  
Kamel Fezzaa

A high-speed X-ray diffraction technique was recently developed at the 32-ID-B beamline of the Advanced Photon Source for studying highly dynamic, yet non-repeatable and irreversible, materials processes. In experiments, the microstructure evolution in a single material event is probed by recording a series of diffraction patterns with extremely short exposure time and high frame rate. Owing to the limited flux in a short pulse and the polychromatic nature of the incident X-rays, analysis of the diffraction data is challenging. Here,HiSPoD, a stand-alone Matlab-based software for analyzing the polychromatic X-ray diffraction data from polycrystalline samples, is described. WithHiSPoD, researchers are able to perform diffraction peak indexing, extraction of one-dimensional intensity profiles by integrating a two-dimensional diffraction pattern, and, more importantly, quantitative numerical simulations to obtain precise sample structure information.


Author(s):  
Farzaneh Shahini ◽  
Maryam Zahabi ◽  
Ben Patranella ◽  
Ashiq Mohammed Abdul Razak

Police motor vehicle crashes are a leading cause of officers’ fatalities in line of duty. These crashes have been attributed not only to driving at high speed in emergency situations but more importantly to interaction with different in-vehicle technologies. Prior studies in this domain have been limited to specific equipment and short exposure time and were typically conducted in laboratory settings with simulated environment or tasks which limit their generalizability to actual police operations. The objective of this study was to identify the most frequently used and cognitively demanding in-vehicle technologies for police officers while driving. Ten officers participated in a three-hour ride-along study. Findings suggested that the mobile computer terminal is the most frequently used and visually and cognitively demanding in-vehicle technology for police officers. Other factors such as work shift, duration, and average time spent in the vehicle per shift can also affect workload. The results indicated the need for improvements in in-vehicle technology design and implementation, officer training protocols, and departmental policies in order to reduce officers’ mental workload and improve safety in police operations.


Sensors ◽  
2019 ◽  
Vol 19 (7) ◽  
pp. 1606 ◽  
Author(s):  
Kazuki Yamato ◽  
Toshihiko Yamashita ◽  
Hiroyuki Chiba ◽  
Hiromasa Oku

We developed a temporally coded exposure (TeCE) camera that can cope with high-speed focus variations of a tunable acoustic gradient index (TAG) lens. The TeCE camera can execute a very short exposure multiple times at an arbitrary timing during one shot. Furthermore, by accumulating the photoelectrons generated by each exposure, it is possible to maintain the brightness even with a short exposure time. By synchronously driving the TeCE camera and the TAG lens, different focal planes of an observation target can be acquired at high speed. As a result, high-speed three-dimensional measurement becomes possible, and this can be used for feedback of three-dimensional information. In the work described in this paper, we conducted a focus tracking experiment to evaluate the feedback performance of the TeCE camera. From the experimental results, we confirmed the feedback capability of the TeCE camera.


1967 ◽  
Vol 21 (6) ◽  
pp. 360-364 ◽  
Author(s):  
Esther C. Cassidy ◽  
Stanley Abramowitz

A spectroscopic technique for continuous and time-resolved study of the atomic and molecular species produced by electrically exploded wires is described. A high-speed drum camera is utilized to record the time history of the explosion spectrum. More detailed studies (from photographic plates) of the spectrum at selected times are then conducted by use of a rotating shutter. Results are presented from experiments with aluminum wires exploded in various controlled atmospheres.


Author(s):  
P Eriksson ◽  
V Wikström ◽  
R Larsson

Using optical interferometry in a standard ball-and-disc apparatus and a high-speed video camera with light enhancer, thickener particles entering a grease-lubricated elastohydrodynamic (EHD) contact were traced as they passed through the contact in pure rolling. In previous studies, it has not been possible to track specific particles but, due to the short exposure time and high recording rates used here, sharp images of a passing particle could be captured. Two greases, based on the same synthetic poly(α-olefin) but thickened with Li-12-OH and lithium complex respectively were studied and for a freshly lubricated track it could be documented that the lithium complex thickener causes fewer, but larger, particles to pass the contact. The influence of the base oil bleeding on film formation is also discussed in the paper.


2020 ◽  
Vol 4 (2) ◽  
pp. 722-729
Author(s):  
Usman Sani ◽  
Bashir Gide Muhammad ◽  
Dimas Skam Joseph ◽  
D. Z. Joseph

Poor implementation of quality assurance programs in the radiation industry has been a major setback in our locality. Several studies revealed that occupational workers are exposed to many potential hazards of ionizing radiation during radio-diagnostic procedures, yet radiation workers are often not monitored. This study aims to evaluate the occupational exposure of the radiation workers in Federal Medical Centre Katsina, and to compare the exposure with recommended occupational radiation dose limits. The quarterly readings of 20 thermo-luminescent dosimeters (TLDs') used by the radiation workers from January to December, 2019 were collected from the facility's radiation monitoring archive, and subsequently assessed and analyzed. The results indicate that the average annual equivalent dose per occupational worker range from 0.74 to 1.20 mSv and 1.28 to 2.21 mSv for skin surface and deep skin dose, measured at 10 mm and 0.07 mm tissue depth respectively. The occupational dose was within the recommended national and international limits of 5 mSv per annum or an average of 20 mSv in 5 years. Therefore, there was no significant radiation exposure to all the occupational workers in the study area. Though, the occupational radiation dose is within recommended limit, this does not eliminate stochastic effect of radiation. The study recommended that the occupational workers should adhere and strictly comply with the principles of radiation protection which includes distance, short exposure time, shielding and proper monitoring of dose limits. Furthermore, continuous training of the radiation workers is advised.


2021 ◽  
Vol 10 (1) ◽  
Author(s):  
Sicong Wang ◽  
Chen Wei ◽  
Yuanhua Feng ◽  
Hongkun Cao ◽  
Wenzhe Li ◽  
...  

AbstractAlthough photonics presents the fastest and most energy-efficient method of data transfer, magnetism still offers the cheapest and most natural way to store data. The ultrafast and energy-efficient optical control of magnetism is presently a missing technological link that prevents us from reaching the next evolution in information processing. The discovery of all-optical magnetization reversal in GdFeCo with the help of 100 fs laser pulses has further aroused intense interest in this compelling problem. Although the applicability of this approach to high-speed data processing depends vitally on the maximum repetition rate of the switching, the latter remains virtually unknown. Here we experimentally unveil the ultimate frequency of repetitive all-optical magnetization reversal through time-resolved studies of the dual-shot magnetization dynamics in Gd27Fe63.87Co9.13. Varying the intensities of the shots and the shot-to-shot separation, we reveal the conditions for ultrafast writing and the fastest possible restoration of magnetic bits. It is shown that although magnetic writing launched by the first shot is completed after 100 ps, a reliable rewriting of the bit by the second shot requires separating the shots by at least 300 ps. Using two shots partially overlapping in space and minimally separated by 300 ps, we demonstrate an approach for GHz magnetic writing that can be scaled down to sizes below the diffraction limit.


1988 ◽  
Author(s):  
H. W. Tom ◽  
G. D. Aumiller ◽  
C. H. Brito-Cruz

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