Simple and fast determination of catecholamines in pharmaceutical samples using Ag+–3,3′,5,5′-tetramethylbenzidine as a colorimetric probe

2015 ◽  
Vol 7 (16) ◽  
pp. 6785-6790 ◽  
Author(s):  
Shuyun Zhu ◽  
Jing Yang ◽  
Xian-en Zhao ◽  
Rongmei Kong ◽  
Hua Wang ◽  
...  

For the first time, a colorimetric method for the detection of catecholamines is developed based on their reducibility towards blue oxidized 3,3′,5,5′-tetramethylbenzidine oxidized by Ag+.

Author(s):  
Monica HARMANESCU

Principal Components and Classification Analysis (PC&CA) represents one of the most utilised multivariate chemometric techniques, having the advantage to use many measurements for a single sample in the same time, being recommended for understanding better the complexity of one phenomenon. The aim of this paper was to use PC&CA to study the effects of different types of fertilizers on polyphenols content of forages harvested in autumn from permanent grassland. Gravimetrically was established the matrix of floristic composition. The experimental field was fertilized first time in 2003, organic and/or NPK mineral. The determination of polyphenols contents was made using UV-VIS SPECORD 205 spectrophotometer, in conformity to chemical Folin and Ciocalteu colorimetric method. The highest polyphenols content was identified in forages from unfertilized variant (108 µM gallic acid/g). PC&CA can be a useful tool in describing the modification of polyphenols contents of forages under the effects of organic and/or mineral fertilisation of permanent grassland.


2017 ◽  
Vol 9 (21) ◽  
pp. 3151-3158 ◽  
Author(s):  
Thangarasu Sasikumar ◽  
Malaichamy Ilanchelian

In this work, we have developed a simple, rapid, sensitive and selective colorimetric method for the quantitative determination of hypochlorite (ClO−) ions by using triangular silver nanoprisms (AgNPRs) as a colorimetric probe.


2017 ◽  
Vol 29 (10) ◽  
pp. 2340-2347 ◽  
Author(s):  
Tiago de Jesus Guedes ◽  
Glauber Antônio Reis Andrade ◽  
Amanda Barbosa Lima ◽  
Rodrigo Amorim Bezerra da Silva ◽  
Wallans Torres Pio dos Santos

RSC Advances ◽  
2016 ◽  
Vol 6 (70) ◽  
pp. 65588-65593 ◽  
Author(s):  
Hui-Jun Fu ◽  
Yu Wang ◽  
Xiu-Xiu Dong ◽  
Yi-Xin Liu ◽  
Zi-Jian Chen ◽  
...  

In this work, a nickel cobalt oxide (Ni/Co oxide) nanoflake based electrochemical sensor for the fast determination of estriol in milk is presented for the first time.


RSC Advances ◽  
2015 ◽  
Vol 5 (69) ◽  
pp. 56255-56261 ◽  
Author(s):  
Mehdi Shabani-Nooshabadi ◽  
Fahimeh Tahernejad-Javazmi

In this study, we describe the simultaneous determination of glutathione and vitamin B6in pharmaceutical and biological samples for the first time.


2018 ◽  
Vol 90 (5) ◽  
pp. 3550-3555 ◽  
Author(s):  
Sabir Khan ◽  
Matthieu Tubino ◽  
Marta M. D. C. Vila ◽  
Flavio A. Bastos

2016 ◽  
Vol 45 (28) ◽  
pp. 11540-11553 ◽  
Author(s):  
Anupam Ghorai ◽  
Jahangir Mondal ◽  
Shubhamoy Chowdhury ◽  
Goutam K. Patra

A solvent-dependent reversible fluorescent-colorimetric bis-iminopyridyl Schiff base receptor (N1E,N4E)-N1,N4-bis(quinolin-4-ylmethylene)benzene-1,4-diamine (L) has been developed for the first time for sensitive and selective determination of Al3+ and Cu2+ in aqueous solution.


2019 ◽  
Vol 147 ◽  
pp. 319-323 ◽  
Author(s):  
Mengling Lin ◽  
Yingjie Guo ◽  
Zhiyong Liang ◽  
Xuesong Zhao ◽  
Jianan Chen ◽  
...  

2017 ◽  
Vol 41 (22) ◽  
pp. 13881-13888 ◽  
Author(s):  
Javad Tashkhourian ◽  
Mina Afsharinejad

A simple and reliable colorimetric method for visual differentiation between the S-citalopram and R-citalopram enantiomers in aqueous solution based on the inherent chirality of silver nanoparticles as a colorimetric probe was presented.


2020 ◽  
pp. 22-38
Author(s):  
Natalia Guseva ◽  
Vitaliy Berdutin

At present, the problem of establishing disability is a point at issue in Russia. Despite the fact that medical criteria for disability are being developed very actively, high-quality methods for assessing social hallmarks are still lacking. Since disability is a phenomenon inherent in any society, each state forms a social and economic policy for people with disabilities in accordance with its level of development, priorities and opportunities. We have proposed a three-stage model, which includes a system for the consistent solution of the main tasks aimed at studying the causes and consequences of the problems encountered today in the social protection of citizens with health problems. The article shows why the existing approaches to the determination of disability and rehabilitation programs do not correspond to the current state of Russian society and why a decrease in the rate of persons recognized as disabled for the first time does not indicate an improvement in the health of the population. The authors proposed a number of measures with a view to correcting the situation according to the results of the study.


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