scholarly journals Automated SEM and TEM sample preparation applied to copper/low k materials

2001 ◽  
Author(s):  
R. Reyes
Keyword(s):  
2004 ◽  
Vol 812 ◽  
Author(s):  
Mikhail R. Baklanov ◽  
Konstantin P. Mogilnikov ◽  
Jin-Heong Yim

AbstractEvaluation of quasi-closed cavities connected with air through narrow necks is discussed. These cavities behave as closed pores when they are studied by Positron Annihilation Lifetime Spectroscopy (PALS). The reason is a short lifetime of o-positronium (Ps) and energy barrier that exist for Ps diffusion from large pores (d>3 nm) to small ones (d<3 nm). It is shown that more comprehensive information can be obtained using adsorption porosimetry. Standard adsorptives used in adsorption porosimetry have infinite lifetime allowing complete penetration and filling all the cavities during the measurement. Calculation of the neck and cavity sizes is based on the theory of metastable adsorption phases developed by Derjagin, Broekhoff and de Boer (DBdB). Results of evaluation are in good agreement with data obtained by SEM and TEM.


Author(s):  
R. R. Cerchiara ◽  
H. A. Cook ◽  
P. E. Fischione ◽  
J. J. Gronsky ◽  
J. M. Matesa ◽  
...  

Abstract The SiLK resins, composed of aromatic hydrocarbons, are a family of highly cross-linked thermoset polymers with isotropic dielectric properties. Patterning of SiLK for high aspect ratio copper interconnects has depended on reactive ion etching with oxygen/nitrogen gas mixtures. Reactive ion etching is therefore also accomplished with reducing plasmas such as nitrogen/hydrogen. An additional plasma cleaning step can be inserted after the reactive ion etching (RIE) step, so that any residual contamination is removed prior to imaging or final sputter coating. Automated sample preparation of microelectronic materials containing high and low-k dielectrics for FESEM is accomplished in this article by combining these techniques: plasma cleaning, ion beam etching, and reactive ion etching. A single RIE chemistry was effective in etching both dielectrics as well as delineating the other phases present.


1999 ◽  
Vol 7 (7) ◽  
pp. 34-35
Author(s):  
Janet Teshima

A large part of the preparation of semiconductor samples for SEM and TEM observations involves the creation of cross sections to expose subsurface defects and three-dimensional structure. A powerful new combination of FIB (FEI Company, Hillsboro, Oregon, http://www.feic.com ) with automated microcleaving technology (SELA, Santa Clara, California, http://www. sela.com ) now offers a comprehensive solution for fast, easy and accurate sample preparation.


2021 ◽  
pp. 113365
Author(s):  
Ankur Sinha ◽  
Gloria Ischia ◽  
Giovanni Straffelini ◽  
Stefano Gialanella

Author(s):  
Liu Binghai ◽  
Chen Ye ◽  
Mo Zhiqiang ◽  
Zhao Si Ping ◽  
Wang Chue Yuin ◽  
...  

Abstract Electron-beam induced radiation damage can give rise to large structural collapse and deformation of low k and ultra low k IMD in semiconductor devices, posing great challenges for failure analysis by electron microscopes. Such radiation damage has been frequently observed during both sample preparation by dual-beam FIB and TEM imaging. To minimize radiation damage, in this work we performed systematic studies on every possible failure analysis step that could introduce radiation damage, i.e., pre-FIB sample preparation, FIB milling, and TEM imaging. Based on these studies, we utilized comprehensive technical solutions to radiation damage by each failure analysis step, i.e., low-dose/low-kV FIB and low-dose TEM techniques. We propose and utilize the low-dose TEM imaging techniques on conventional TEM tools without using low-dose imaging control interface/software. With these new methodologies or techniques, the electron-beam induced radiation damage to ultra low k IMD has been successfully minimized, and the combination of single-beam FIB milling and low-dose TEM imaging techniques can reduce structure collapse and shrinkage to almost zero.


Author(s):  
Kuang-Tse Ho ◽  
Chien-Wei Wu ◽  
Te-Fu Chang ◽  
Chia-Hsiang Yen ◽  
Ching-Hsiang Chan

Abstract This research sets up failure analysis flow to verify failure mechanisms and root causes of different kinds of contact leakage. This flow mainly uses EBIC, C-AFM and nano-probing to do fault isolation and confirm electrical failure mechanisms. Appropriate sample preparation is also mandatory for FIB, SEM and TEM inspection.


Author(s):  
Wei-Ming Yang ◽  
Shu-Qing Duan ◽  
Yu-Ke Wang ◽  
Qiang Guo ◽  
Wei-Ting Kary Chien
Keyword(s):  

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