Wetting properties of AFM probes by means of contact angle measurement

2006 ◽  
Vol 39 (17) ◽  
pp. 3858-3862 ◽  
Author(s):  
Zhenhua Tao ◽  
Bharat Bhushan
2011 ◽  
Vol 306-307 ◽  
pp. 25-30 ◽  
Author(s):  
Ping Luo ◽  
Zhan Yun Huang ◽  
Di Hu Chen

In this work, titanium oxide nanorod arrays were fabricated by using the hydrothermal method on fluorine-doped tin oxide (FTO) coated glass. The diameter of the nanorods could be controlled from 150 nm to 30 nm by changing the growth parameters. The surface morphology and the structure of the samples were characterized by SEM and XRD. The wetting properties were identified by contact angle measurement. Platelet attachment was investigated to evaluate the blood compatibility of the samples with different nanoscale topographies. Results show that the nanotopographical surfaces perform outstanding blood compatibility, and the adhering platelet decreased with the increasing diameter of the nanorods.


2000 ◽  
Vol 6 (S2) ◽  
pp. 780-781
Author(s):  
J.P. Craven ◽  
N.A. Stelmashenko ◽  
E.M. Terentjev ◽  
B. L. Thiel

The ESEM uses a novel differential pumping system combined with a pressure-limiting aperture to achieve relatively high pressures of up to 10 torr in the specimen chamber. Using this system allows samples to be imaged in the presence of water vapour or other gases. Conveniently the saturated water pressure at 275K lies within this range, allowing the stabilisation of hydrated samples, condensation from water vapour and evaporation to be performed in situ within the microscope chamber.Wetting of surfaces is of fundamental importance in many different areas of science, from textiles to petroleum engineering. The ESEM now provides an opening for high-resolution studies of these phenomena without the problematic depth-of-field limitations that optical methods present. The contact angle, θ, is defined as the angle between the tangent to the liquid-fluid interface and the tangent to the solid interface. It provides a ready indication to the wetting properties of a system.


2013 ◽  
Vol 8 (4) ◽  
pp. 155892501300800 ◽  
Author(s):  
Yatinkumar Rane ◽  
Aleksey Altecor ◽  
Nelson S. Bell ◽  
Karen Lozano

Superhydrophobic materials combined with manufacturing processes that can increase surface roughness of the material, offer an opportunity to effectively control wetting properties. Rapid formation of Teflon® AF (TAF) fibrous mats with sub-micron fiber diameter using the Forcespinning™ technique is presented. The fiber formation technique is based on the use of centrifugal forces. SEM analysis shows uniform formation of TAF 1600 fibers with average diameter of 362±58nm. Contact angle measurement confirms the superhydrophobic nature of the mats with contact angles as high as 169° ± 3° and rolling angles of 2°. TAF 1600 mats were forcespun at a rate of 1gr/min. The relationship between the contact angle and hierarchical surface roughness of the TAF mat is also discussed. TAF yarns were also manufactured and characterized. Yarns with diameters of 156 microns withstood 17.5 MPa of engineering stress with a Young's modulus of 348 MPa in the elastic region and excellent thermal stability.


2016 ◽  
Vol 5 (1) ◽  
Author(s):  
Jose L. Ocaña ◽  
R. Jagdheesh ◽  
J.J. García-Ballesteros

AbstractThe current availability of new advanced fiber and DPSS lasers with characteristic pulse lengths ranging from ns to fs has provided a unique frame in which the development of laser-generated microstructures has been made possible for very diverse kinds of materials and applications. At the same time, the development of the appropriate laser-processing workstations granting the appropriate precision and repeatability of the respective laser interaction processes in line with the characteristic dimension features required in the microstructured samples has definitively consolidated laser surface microstructuring as a reference domain, nowadays, unavoidable for the design and manufacturing of current use microsystem: MEMSs, fluidic devices, advanced sensors, biomedical devices and instruments, etc., are all among the most well-known developments of the micromanufacturing technology. Completing the broad spectrum of applications developed mostly involving the generation of geometrical features on a subtrate with specific functional purposes, a relatively new, emerging class of laser-microstructuring techniques is finding an important niche of application in the generation of physically structured surfaces (particularly of metallic materials) with specific contact, friction, and wear functionalities, for whose generation the concourse of different types of laser sources is being found as an appropriate tool. In this paper, the application of laser sources with emission in the UV and at ns time regime to the surface structuration of metal surfaces (specifically Al) for the modification of their wettability properties is described as an attractive application basis for the generation of self-cleaning properties of extended functional surfaces. Flat aluminum sheets of thickness 100 μm were laser machined with ultraviolet laser pulses of 30 ns with different laser parameters to optimize the process parameters. The samples produced at the optimum conditions with respect to contact angle measurement were subjected to microstructure and chemical analysis. The wetting properties were evaluated by static contact angle measurements on the laser-patterned surface. The laser-patterned microstructures exhibited superhydrophobicity with a maximum contact angle of 180° for the droplet volumes in the range of 8–12 μl.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Ahmed S. Belal ◽  
Jehan El Nady ◽  
Azza Shokry ◽  
Shaker Ebrahim ◽  
Moataz Soliman ◽  
...  

AbstractOily water contamination has been sighted as one of the most global environmental pollution. Herein, copper hydroxide nanorods layer was constructed onto cellulosic filter paper surface cured with polydopamine, Ag nanoparticles, and Cu NPs through immersion method. This work has been aimed to produce a superhydrophobic and superoleophilic cellulosic filter paper. The structure, crystalline, and morphological properties of these modified cellulosic filter paper were investigated. Scanning electron microscope images confirmed that the modified surface was rougher compared with the pristine surface. The contact angle measurement confirmed the hydrophobic nature of these modified surfaces with a water contact angle of 169.7°. The absorption capacity was 8.2 g/g for diesel oil and the separation efficiency was higher than 99%. It was noted that the flux in the case of low viscosity solvent as n-hexane was 9663.5 Lm−2 h−1, while for the viscous oil as diesel was 1452.7 Lm−2 h−1.


Author(s):  
He Xu ◽  
Yan Xu ◽  
Peiyuan Wang ◽  
Hongpeng Yu ◽  
Ozoemena Anthony Ani ◽  
...  

Purpose The purpose of this paper is to explore a novel measurement approach for wheel-terrain contact angle using laser scanning sensors based on near-terrain perception. Laser scanning sensors have rarely been applied to the measurement of wheel-terrain contact angle for wheeled mobile robots (WMRs) in previous studies; however, it is an effective way to measure wheel-terrain contact angle directly with the advantages of simple, fast and high accuracy. Design/methodology/approach First, kinematics model for a WMR moving on rough terrain was developed, taking into consideration wheel slip and wheel-terrain contact angle. Second, the measurement principles of wheel-terrain contact angle using laser scanning sensors was presented, including “rigid wheel - rigid terrain” model and “rigid wheel - deformable terrain” model. Findings In the proposed approach, the measurement of wheel-terrain contact angle using laser scanning sensors was successfully demonstrated. The rationality of the approach was verified by experiments on rigid and sandy terrains with satisfactory results. Originality/value This paper proposes a novel, fast and effective wheel-terrain contact angle measurement approach for WMRs moving on both rigid and deformable terrains, using laser scanning sensors.


Author(s):  
Lixin Wang ◽  
Pan Pan ◽  
Shixing Yan ◽  
Shiyun Dong

The slippery zone of Nepenthes alata depends on its highly evolved morphology and structure to show remarkable superhydrophobicity, which has gradually become a biomimetic prototype for developing superhydrophobic materials. However, the mechanism governing this phenomenon has not been fully revealed through model analysis. In this paper, the superhydrophobicity of slippery zone is studied by contact angle measurement, morphology/structure examination and model analysis. The slippery zone causes ultrapure water droplet to produce a considerably high contact angle (155.11–158.30°), and has a micro-nano scale hierarchical structures consisting of lunate cells and wax coverings. According to the Cassie-Baxter equation and a self-defined infiltration coefficient, a model was established to analyze the effect of structure characteristic on the contact angle. Analysis result showed that the calculated contact angle (154.67–159.49°) was highly consistent with the measured contact angle, indicating that the established model can quantitatively characterize the relationship between the contact angle and the structure characteristic. Our study provides some evidences to further reveal the superhydrophobic mechanism of Nepenthes alata slippery zone, as well as inspires the biomimetic development of superhydrophobic surfaces.


2004 ◽  
Vol 274 (2) ◽  
pp. 637-644 ◽  
Author(s):  
Tammar S. Meiron ◽  
Abraham Marmur ◽  
I.Sam Saguy

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